ATE39471T1 - Verfahren zur herstellung eines zeolithen durch kontinuierliches mischen. - Google Patents
Verfahren zur herstellung eines zeolithen durch kontinuierliches mischen.Info
- Publication number
- ATE39471T1 ATE39471T1 AT84401830T AT84401830T ATE39471T1 AT E39471 T1 ATE39471 T1 AT E39471T1 AT 84401830 T AT84401830 T AT 84401830T AT 84401830 T AT84401830 T AT 84401830T AT E39471 T1 ATE39471 T1 AT E39471T1
- Authority
- AT
- Austria
- Prior art keywords
- reaction zone
- zeolite
- intimate admixture
- gelation
- continuous
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000010457 zeolite Substances 0.000 abstract 3
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 238000001879 gelation Methods 0.000 abstract 2
- 239000004115 Sodium Silicate Substances 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 230000014759 maintenance of location Effects 0.000 abstract 1
- 229910001388 sodium aluminate Inorganic materials 0.000 abstract 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052911 sodium silicate Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/32—Alkali metal silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
- C01B33/28—Base exchange silicates, e.g. zeolites
- C01B33/2807—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures
- C01B33/2815—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L)
- C01B33/2823—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L) from aqueous solutions of an alkali metal aluminate and an alkali metal silicate excluding any other source of alumina or silica
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/21—Faujasite, e.g. X, Y, CZS-3, ECR-4, Z-14HS, VHP-R
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/24—LTA, e.g. A, alpha, ZK-4, ZK-21, ZK-22
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8314985A FR2552070B1 (fr) | 1983-09-21 | 1983-09-21 | Procede d'obtention d'une zeolite par alimentation en continu d'une solution aqueuse de silicate de sodium et d'une solution aqueuse d'aluminate de sodium, produit obtenu et application du produit a la detergence |
| EP84401830A EP0149929B2 (de) | 1983-09-21 | 1984-09-14 | Verfahren zur Herstellung eines Zeolithen durch kontinuierliches Mischen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE39471T1 true ATE39471T1 (de) | 1989-01-15 |
Family
ID=9292392
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT84401830T ATE39471T1 (de) | 1983-09-21 | 1984-09-14 | Verfahren zur herstellung eines zeolithen durch kontinuierliches mischen. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4661334A (de) |
| EP (1) | EP0149929B2 (de) |
| KR (1) | KR890004801B1 (de) |
| AT (1) | ATE39471T1 (de) |
| BR (1) | BR8404722A (de) |
| CA (1) | CA1244813A (de) |
| DE (1) | DE3475774D1 (de) |
| ES (1) | ES8602537A1 (de) |
| FR (1) | FR2552070B1 (de) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5474753A (en) * | 1990-11-09 | 1995-12-12 | Laviosa Rhone-Poulenc | Preparation of crystalline 4A zeolites |
| FR2669017B1 (fr) * | 1990-11-09 | 1993-09-10 | Rhone Poulenc Chimie | Procede de preparation de zeolithe 4a cristallisee. |
| US5672390A (en) * | 1990-11-13 | 1997-09-30 | Dancor, Inc. | Process for protecting a surface using silicate compounds |
| ES2024361A6 (es) * | 1990-12-14 | 1992-02-16 | Foret Sa | Procedimiento de obtencion de zeolita 4a. |
| US5487882A (en) * | 1994-07-19 | 1996-01-30 | Albemarle Corporation | Process for preparation of zeolite "X" |
| IT1284078B1 (it) * | 1996-06-27 | 1998-05-08 | Condea Augusta Spa | Materiale cristallino microporoso, procedimento per la preparazione e uso in composizioni detergenti |
| US6036939A (en) * | 1996-08-30 | 2000-03-14 | Tosoh Corporation | Heat-resistant low-silica zeolite, and process for production and application thereof |
| US6831056B1 (en) | 1999-11-09 | 2004-12-14 | Kao Corporation | Process for preparing fine alkaline earth metal zeolite particles |
| JP3611185B2 (ja) * | 1999-11-09 | 2005-01-19 | 花王株式会社 | 微粒子ゼオライトの製造方法 |
| US6358616B1 (en) | 2000-02-18 | 2002-03-19 | Dancor, Inc. | Protective coating for metals |
| US6432380B1 (en) | 2000-09-08 | 2002-08-13 | Albemarle Corporation | Synthesis of aluminosilicates via cofeeding an alkali metal aluminate and sodium silicate and cofeeding apparatus therefor |
| US6632415B2 (en) * | 2001-04-09 | 2003-10-14 | Chevron U.S.A. Inc. | Methods for making molecular sieves |
| KR100483181B1 (ko) * | 2002-05-27 | 2005-04-14 | 김익진 | 연속결정화 방법에 의한 NaX 제올라이트의 제조방법 |
| US7528201B2 (en) * | 2004-12-22 | 2009-05-05 | Exxonmobil Chemical Patents Inc. | Synthesis of silicoaluminophosphate molecular sieves |
| CN101745365B (zh) * | 2009-12-30 | 2012-07-25 | 郑州雪山实业有限公司 | 高吸附性能13x分子筛的制备方法 |
| WO2013003728A1 (en) | 2011-06-29 | 2013-01-03 | Pq Corporation | Zeolite impregnated with titanium dioxide |
| CN106276959B (zh) * | 2016-08-16 | 2018-01-23 | 中国铝业股份有限公司 | 球形4a沸石,其制备方法、制备装置和用途 |
| FR3063993B1 (fr) * | 2017-03-17 | 2022-02-04 | Arkema France | Procede de synthese en continu de cristaux de zeolithe |
| FR3063996B1 (fr) | 2017-03-17 | 2022-01-14 | Arkema France | Procede de synthese de cristaux de zeolithe avec agent d'ensemencement |
| FR3076828A1 (fr) | 2018-01-15 | 2019-07-19 | Arkema France | Procede de preparation de zeolithes en continu au moyen d'ultrasons |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4160011A (en) * | 1974-12-26 | 1979-07-03 | Texaco Inc. | Crystalline aluminosilicate percursor |
| DE2705088C2 (de) * | 1977-02-08 | 1986-05-22 | Kali-Chemie Ag, 3000 Hannover | Verfahren zur Herstellung von überwiegend kristallinen Natriumaluminiumsilikaten |
| DE2856278A1 (de) * | 1978-12-27 | 1980-07-10 | Degussa | Verfahren zur herstellung feinstteiliger natriumaluminiumsilikate |
| DE2910152A1 (de) * | 1979-03-15 | 1980-10-16 | Degussa | Verfahren zur herstellung von amorphen natriumaluminiumsilikaten |
| JPS5917048B2 (ja) * | 1980-06-04 | 1984-04-19 | 日本化学工業株式会社 | A型ゼオライトの製造法 |
| JPS6049130B2 (ja) * | 1980-12-27 | 1985-10-31 | 日本化学工業株式会社 | A型ゼオライトの製造法 |
| JPS57129819A (en) * | 1981-01-28 | 1982-08-12 | Nippon Chem Ind Co Ltd:The | Manufacture of a-type zeolite |
| JPS57166311A (en) * | 1981-04-02 | 1982-10-13 | Nippon Chem Ind Co Ltd:The | Production of x-type zeolite |
| FR2528722A1 (fr) * | 1982-06-18 | 1983-12-23 | Rhone Poulenc Chim Base | Zeolite comme auxiliaire de detergence |
-
1983
- 1983-09-21 FR FR8314985A patent/FR2552070B1/fr not_active Expired
-
1984
- 1984-09-14 EP EP84401830A patent/EP0149929B2/de not_active Expired - Lifetime
- 1984-09-14 DE DE8484401830T patent/DE3475774D1/de not_active Expired
- 1984-09-14 AT AT84401830T patent/ATE39471T1/de not_active IP Right Cessation
- 1984-09-20 BR BR8404722A patent/BR8404722A/pt not_active IP Right Cessation
- 1984-09-20 ES ES536089A patent/ES8602537A1/es not_active Expired
- 1984-09-20 CA CA000463658A patent/CA1244813A/fr not_active Expired
- 1984-09-20 KR KR1019840005767A patent/KR890004801B1/ko not_active Expired
- 1984-09-21 US US06/653,084 patent/US4661334A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FR2552070A1 (fr) | 1985-03-22 |
| EP0149929A1 (de) | 1985-07-31 |
| EP0149929B1 (de) | 1988-12-28 |
| DE3475774D1 (en) | 1989-02-02 |
| US4661334A (en) | 1987-04-28 |
| BR8404722A (pt) | 1985-08-13 |
| FR2552070B1 (fr) | 1987-09-11 |
| ES536089A0 (es) | 1985-12-01 |
| ES8602537A1 (es) | 1985-12-01 |
| CA1244813A (fr) | 1988-11-15 |
| KR890004801B1 (ko) | 1989-11-27 |
| KR850002242A (ko) | 1985-05-10 |
| EP0149929B2 (de) | 1993-09-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification | ||
| EEIH | Change in the person of patent owner | ||
| UEP | Publication of translation of european patent specification | ||
| REN | Ceased due to non-payment of the annual fee |