ATE413918T1 - Verfahren zur herstellung von monosilan - Google Patents
Verfahren zur herstellung von monosilanInfo
- Publication number
- ATE413918T1 ATE413918T1 AT06763774T AT06763774T ATE413918T1 AT E413918 T1 ATE413918 T1 AT E413918T1 AT 06763774 T AT06763774 T AT 06763774T AT 06763774 T AT06763774 T AT 06763774T AT E413918 T1 ATE413918 T1 AT E413918T1
- Authority
- AT
- Austria
- Prior art keywords
- countercurrent reactor
- trichlorosilane
- heat exchanger
- double wall
- monosilane
- Prior art date
Links
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 abstract 4
- 239000005052 trichlorosilane Substances 0.000 abstract 4
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000006200 vaporizer Substances 0.000 abstract 2
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- 238000007323 disproportionation reaction Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- FDNAPBUWERUEDA-UHFFFAOYSA-N silicon tetrachloride Chemical compound Cl[Si](Cl)(Cl)Cl FDNAPBUWERUEDA-UHFFFAOYSA-N 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/04—Hydrides of silicon
- C01B33/043—Monosilane
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/04—Hydrides of silicon
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
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- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/30—Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
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- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
- B01J8/0085—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer
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- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
- B01J8/009—Membranes, e.g. feeding or removing reactants or products to or from the catalyst bed through a membrane
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/06—Reactor-distillation
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Inorganic Chemistry (AREA)
- Thermal Sciences (AREA)
- Silicon Compounds (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005046105A DE102005046105B3 (de) | 2005-09-27 | 2005-09-27 | Verfahren zur Herstellung von Monosilan |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE413918T1 true ATE413918T1 (de) | 2008-11-15 |
Family
ID=36950933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT06763774T ATE413918T1 (de) | 2005-09-27 | 2006-06-19 | Verfahren zur herstellung von monosilan |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US8105564B2 (de) |
| EP (1) | EP1928591B1 (de) |
| JP (1) | JP4922303B2 (de) |
| KR (1) | KR20080065971A (de) |
| CN (1) | CN101466463B (de) |
| AT (1) | ATE413918T1 (de) |
| BR (1) | BRPI0616443A2 (de) |
| CA (1) | CA2624534C (de) |
| DE (2) | DE102005046105B3 (de) |
| ES (1) | ES2317557T3 (de) |
| NO (1) | NO20081913L (de) |
| RU (1) | RU2403964C2 (de) |
| UA (1) | UA89438C2 (de) |
| WO (1) | WO2007039326A1 (de) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006003464A1 (de) * | 2006-01-25 | 2007-07-26 | Degussa Gmbh | Verfahren zur Erzeugung einer Siliciumschicht auf einer Substratoberfläche durch Gasphasenabscheidung |
| DE102007007874A1 (de) | 2007-02-14 | 2008-08-21 | Evonik Degussa Gmbh | Verfahren zur Herstellung höherer Silane |
| DE102007052325A1 (de) * | 2007-03-29 | 2009-05-07 | Erk Eckrohrkessel Gmbh | Verfahren zum gleitenden Temperieren chemischer Substanzen mit definierten Ein- und Ausgangstemperaturen in einem Erhitzer und Einrichtung zur Durchführung des Verfahrens |
| DE102007050199A1 (de) * | 2007-10-20 | 2009-04-23 | Evonik Degussa Gmbh | Entfernung von Fremdmetallen aus anorganischen Silanen |
| DE102008017304A1 (de) * | 2008-03-31 | 2009-10-01 | Schmid Silicon Technology Gmbh | Verfahren und Anlage zur Herstellung von Reinstsilizium |
| CN102092720B (zh) * | 2009-02-13 | 2013-03-27 | 李明成 | 高纯硅烷气体连续制备装置 |
| ES2350559B1 (es) * | 2009-05-28 | 2011-11-18 | Centro De Tecnologia Del Silicio Solar, S.L. (Centesil) | Procedimiento de aprovechamiento de residuos ligeros en una planta de producción de silicio de alta pureza. |
| DE102009027730A1 (de) | 2009-07-15 | 2011-01-27 | Evonik Degussa Gmbh | Verahren und Verwendung von aminofunktionellen Harzen zur Dismutierung von Halogensilanen und zur Entfernung von Fremdmetallen |
| DE102009037154B3 (de) * | 2009-08-04 | 2010-12-09 | Schmid Silicon Technology Gmbh | Verfahren zur Herstellung von Monosilan |
| KR101159674B1 (ko) * | 2009-11-16 | 2012-06-25 | 주식회사 케이씨씨 | 모노실란의 정제방법 |
| DE102009053804B3 (de) | 2009-11-18 | 2011-03-17 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Hydridosilanen |
| DE102010034469A1 (de) * | 2010-08-06 | 2012-02-09 | Schmid Silicon Technology Gmbh | Anlage zur Herstellung von Monosilan |
| CN101920178B (zh) * | 2010-08-30 | 2012-04-25 | 哈尔滨工业大学 | 制备甲硅烷气体的管式反应器系统及使用其制备甲硅烷的方法 |
| EP2426089A1 (de) * | 2010-09-03 | 2012-03-07 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Verfahren zur Spaltung von Monosilan aus einer chlorsilanreichen Mischung |
| DE102010043648A1 (de) | 2010-11-09 | 2012-05-10 | Evonik Degussa Gmbh | Verfahren zur selektiven Spaltung höherer Silane |
| DE102011004058A1 (de) | 2011-02-14 | 2012-08-16 | Evonik Degussa Gmbh | Monochlorsilan, Verfahren und Vorrichtung zu dessen Herstellung |
| KR101978107B1 (ko) * | 2011-06-28 | 2019-05-13 | 코너 스타 리미티드 | 버블 컬럼에서 실란의 제조 방법 |
| CN103112860B (zh) * | 2013-02-26 | 2015-09-02 | 天津大学 | 改良西门子法联产制备高纯硅烷的方法 |
| CN106241813B (zh) * | 2016-08-16 | 2021-01-01 | 上海交通大学 | 一种由三氯氢硅生产高纯硅烷的系统及方法 |
| CN106397471B (zh) * | 2016-08-16 | 2018-09-28 | 湖北兴发化工集团股份有限公司 | 一种有机硅单体原料氯甲烷的汽化节能装置及工艺 |
| EP3659964A1 (de) | 2018-11-28 | 2020-06-03 | Hysilabs, SAS | Katalysiertes verfahren zur herstellung von wasserstoff aus silylierten derivaten als wasserstoffträgerverbindungen |
| JP7269761B2 (ja) * | 2019-03-15 | 2023-05-09 | 三菱重工業株式会社 | 原料流体の処理プラント、及び原料流体の処理方法 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3968199A (en) * | 1974-02-25 | 1976-07-06 | Union Carbide Corporation | Process for making silane |
| US4676967A (en) * | 1978-08-23 | 1987-06-30 | Union Carbide Corporation | High purity silane and silicon production |
| JPS59121110A (ja) * | 1982-12-24 | 1984-07-13 | Denki Kagaku Kogyo Kk | シラン化合物の連続的製法 |
| JPS61191513A (ja) * | 1985-02-19 | 1986-08-26 | Denki Kagaku Kogyo Kk | シラン化合物の連続的製造方法 |
| DE3711444A1 (de) | 1987-04-04 | 1988-10-13 | Huels Troisdorf | Verfahren und vorrichtung zur herstellung von dichlorsilan |
| JPH0218303A (ja) * | 1988-07-07 | 1990-01-22 | Mitsubishi Gas Chem Co Inc | 炭化水素の改質反応器および改質方法 |
| DE3925357C1 (de) | 1989-07-31 | 1991-04-25 | Degussa Ag, 6000 Frankfurt, De | |
| SE503793C2 (sv) * | 1995-02-01 | 1996-09-09 | Kvaerner Pulping Tech | Förfarande vid behandling av kondensat |
| DE19654516C1 (de) | 1996-12-27 | 1998-10-01 | Degussa | Verfahren zur Auftrennung des Produktgasgemisches der katalytischen Synthese von Methylmercaptan |
| RU2129984C1 (ru) * | 1998-06-25 | 1999-05-10 | Государственный научный центр Российской Федерации - Государственный научно-исследовательский институт химии и технологии элементоорганических соединений | Способ получения моносилана высокой чистоты |
| DE19860146A1 (de) * | 1998-12-24 | 2000-06-29 | Bayer Ag | Verfahren und Anlage zur Herstellung von Silan |
| SG85160A1 (en) * | 1999-03-02 | 2001-12-19 | Nippon Catalytic Chem Ind | Method for production of (meth) acrylic acid and/or (meth) acrylic esters |
| JP2001131188A (ja) * | 1999-10-29 | 2001-05-15 | Tokuyama Corp | クロロシラン類の不均化反応方法 |
| DE10017168A1 (de) | 2000-04-07 | 2001-10-11 | Bayer Ag | Verfahren und Anlage zur Herstellung von Silan |
| DE10034493C1 (de) | 2000-07-15 | 2001-11-29 | Degussa | Verfahren zur Herstellung von Organosilylalkylpolysulfanen |
| DE10061680A1 (de) | 2000-12-11 | 2002-06-20 | Solarworld Ag | Verfahren zur Herstellung von Silan |
| RU2214362C1 (ru) * | 2002-07-19 | 2003-10-20 | Федеральное государственное унитарное предприятие "Государственный научно-исследовательский институт химии и технологии элементоорганических соединений" | Способ получения моносилана высокой чистоты |
| DE10243022A1 (de) | 2002-09-17 | 2004-03-25 | Degussa Ag | Abscheidung eines Feststoffs durch thermische Zersetzung einer gasförmigen Substanz in einem Becherreaktor |
| DE10331952A1 (de) | 2003-07-15 | 2005-02-10 | Degussa Ag | Vorrichtung und Verfahren zur diskontinuierlichen Polykondensation |
| DE10357091A1 (de) | 2003-12-06 | 2005-07-07 | Degussa Ag | Vorrichtung und Verfahren zur Abscheidung feinster Partikel aus der Gasphase |
| DE102004008042A1 (de) | 2004-02-19 | 2005-09-01 | Goldschmidt Gmbh | Verfahren zur Herstellung von Aminosäureestern und deren Säure-Additions-Salzen |
| DE102004010055A1 (de) | 2004-03-02 | 2005-09-22 | Degussa Ag | Verfahren zur Herstellung von Silicium |
| DE102004027564A1 (de) | 2004-06-04 | 2005-12-22 | Joint Solar Silicon Gmbh & Co. Kg | Verdichtungs-Vorrichtung |
| DE102004038718A1 (de) | 2004-08-10 | 2006-02-23 | Joint Solar Silicon Gmbh & Co. Kg | Reaktor sowie Verfahren zur Herstellung von Silizium |
| CN101128393A (zh) * | 2005-03-05 | 2008-02-20 | 联合太阳能硅有限及两合公司 | 反应器和制备硅的方法 |
| DE102006003464A1 (de) * | 2006-01-25 | 2007-07-26 | Degussa Gmbh | Verfahren zur Erzeugung einer Siliciumschicht auf einer Substratoberfläche durch Gasphasenabscheidung |
| DE102007050199A1 (de) * | 2007-10-20 | 2009-04-23 | Evonik Degussa Gmbh | Entfernung von Fremdmetallen aus anorganischen Silanen |
-
2005
- 2005-09-27 DE DE102005046105A patent/DE102005046105B3/de not_active Expired - Fee Related
-
2006
- 2006-06-19 AT AT06763774T patent/ATE413918T1/de not_active IP Right Cessation
- 2006-06-19 EP EP06763774A patent/EP1928591B1/de not_active Not-in-force
- 2006-06-19 BR BRPI0616443-9A patent/BRPI0616443A2/pt not_active IP Right Cessation
- 2006-06-19 JP JP2008532688A patent/JP4922303B2/ja not_active Expired - Fee Related
- 2006-06-19 CA CA2624534A patent/CA2624534C/en not_active Expired - Fee Related
- 2006-06-19 ES ES06763774T patent/ES2317557T3/es active Active
- 2006-06-19 UA UAA200805472A patent/UA89438C2/ru unknown
- 2006-06-19 CN CN2006800356931A patent/CN101466463B/zh not_active Expired - Fee Related
- 2006-06-19 US US12/088,286 patent/US8105564B2/en not_active Expired - Fee Related
- 2006-06-19 DE DE602006003667T patent/DE602006003667D1/de active Active
- 2006-06-19 RU RU2008116147/12A patent/RU2403964C2/ru not_active IP Right Cessation
- 2006-06-19 KR KR1020087007312A patent/KR20080065971A/ko not_active Abandoned
- 2006-06-19 WO PCT/EP2006/063316 patent/WO2007039326A1/en not_active Ceased
-
2008
- 2008-04-22 NO NO20081913A patent/NO20081913L/no not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| CN101466463A (zh) | 2009-06-24 |
| US20090155156A1 (en) | 2009-06-18 |
| NO20081913L (no) | 2008-04-22 |
| WO2007039326A1 (en) | 2007-04-12 |
| JP4922303B2 (ja) | 2012-04-25 |
| DE102005046105B3 (de) | 2007-04-26 |
| JP2009509901A (ja) | 2009-03-12 |
| ES2317557T3 (es) | 2009-04-16 |
| CA2624534A1 (en) | 2007-04-12 |
| DE602006003667D1 (de) | 2008-12-24 |
| UA89438C2 (ru) | 2010-01-25 |
| KR20080065971A (ko) | 2008-07-15 |
| EP1928591B1 (de) | 2008-11-12 |
| CN101466463B (zh) | 2012-07-18 |
| BRPI0616443A2 (pt) | 2011-06-21 |
| CA2624534C (en) | 2012-11-27 |
| EP1928591A1 (de) | 2008-06-11 |
| US8105564B2 (en) | 2012-01-31 |
| RU2008116147A (ru) | 2009-11-10 |
| RU2403964C2 (ru) | 2010-11-20 |
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| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |