ATE456541T1 - Verfahren zur kontinuierlichen produktion von hydroxylammonium - Google Patents

Verfahren zur kontinuierlichen produktion von hydroxylammonium

Info

Publication number: ATE456541T1
Authority: AT; Austria
Prior art keywords: hydroxyl ammonium; zone; synthesis zone; cyclohexanone oxime; production
Prior art date: 2005-07-08

Application number

AT06754663T

Other languages

English (en)

Inventor

Hendrik Oevering

Olaf Poorter

Original Assignee

Dsm Ip Assets Bv

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2005-07-08

Filing date

2006-07-04

Publication date

2010-02-15

2006-07-04 Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv

2010-02-15 Application granted granted Critical

2010-02-15 Publication of ATE456541T1 publication Critical patent/ATE456541T1/de

Links

RBLWMQWAHONKNC-UHFFFAOYSA-N hydroxyazanium Chemical compound O[NH3+] RBLWMQWAHONKNC-UHFFFAOYSA-N 0.000 title abstract 9
238000000034 method Methods 0.000 title abstract 5
238000010924 continuous production Methods 0.000 title abstract 2
VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 abstract 8
MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 abstract 6
230000015572 biosynthetic process Effects 0.000 abstract 5
238000003786 synthesis reaction Methods 0.000 abstract 5
238000004519 manufacturing process Methods 0.000 abstract 3
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
229910002651 NO3 Inorganic materials 0.000 abstract 2
239000003054 catalyst Substances 0.000 abstract 2
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 2
239000001257 hydrogen Substances 0.000 abstract 2
229910052739 hydrogen Inorganic materials 0.000 abstract 2
-1 nitrate ions Chemical class 0.000 abstract 2
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
238000000605 extraction Methods 0.000 abstract 1
239000007788 liquid Substances 0.000 abstract 1
229910017604 nitric acid Inorganic materials 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/56—Platinum group metals
- B01J23/62—Platinum group metals with gallium, indium, thallium, germanium, tin or lead
- B01J23/622—Platinum group metals with gallium, indium, thallium, germanium, tin or lead with germanium, tin or lead
- B01J23/624—Platinum group metals with gallium, indium, thallium, germanium, tin or lead with germanium, tin or lead with germanium
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C239/00—Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Catalysts (AREA)
Pyrane Compounds (AREA)

AT06754663T 2005-07-08 2006-07-04 Verfahren zur kontinuierlichen produktion von hydroxylammonium ATE456541T1 (de)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL2005000491		2005-07-08
PCT/EP2006/006507 WO2007006458A1 (en)	2005-07-08	2006-07-04	Process for the continuous production of hydroxylammonium

Publications (1)

Publication Number	Publication Date
ATE456541T1 true ATE456541T1 (de)	2010-02-15

Family

ID=35229877

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT06754663T ATE456541T1 (de)	2005-07-08	2006-07-04	Verfahren zur kontinuierlichen produktion von hydroxylammonium

Country Status (15)

Country	Link
US (1)	US20090221854A1 (de)
EP (1)	EP1901994B1 (de)
JP (1)	JP5256031B2 (de)
KR (1)	KR101311626B1 (de)
CN (1)	CN101218171B (de)
AT (1)	ATE456541T1 (de)
BR (1)	BRPI0613171A2 (de)
DE (1)	DE602006012048D1 (de)
EA (1)	EA014243B1 (de)
MX (1)	MX2008000324A (de)
MY (1)	MY143223A (de)
PL (1)	PL1901994T3 (de)
TW (1)	TWI402211B (de)
UA (1)	UA91708C2 (de)
WO (1)	WO2007006458A1 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2012505138A (ja) *	2008-10-10	2012-03-01	ディーエスエムアイピーアセッツビー．ブイ．	アンモニウムイオンの分解
CN103492312B (zh) *	2011-04-22	2016-11-02	Capiii有限公司	制备羟胺的方法
CN103492313B (zh) *	2011-04-22	2016-03-09	Capiii有限公司	催化的羟胺制备
CN103987658A (zh) *	2011-12-29	2014-08-13	帝斯曼知识产权资产管理有限公司	一种连续生产羟铵的方法
RU2644889C2 (ru)	2012-11-27	2018-02-14	Хэмптон Роудз Сэнитейшн Дистрикт	Способ и устройство для очистки сточной воды с использованием гравитационного разделения
CN103318858B (zh) *	2013-06-07	2016-01-27	常州大学	一种利用反应-萃取蒸馏耦合技术制备羟胺盐的方法
AU2015284175B2 (en)	2014-06-30	2018-03-01	D.C. Water & Sewer Authority	Method and apparatus for wastewater treatment using external selection
WO2016014723A1 (en)	2014-07-23	2016-01-28	Hampton Roads Sanitation Distric	A method for deammonification process control using ph, specific conductivity, or ammonia
AU2022232524A1 (en)	2021-03-12	2023-09-28	D.C. Water and Sewer Authority	Method and apparatus for nutrient removal using anoxic biofilms
JP7611432B2 (ja)	2021-03-12	2025-01-09	ハンプトンローズサニテーションディストリクト	水または廃水処理における多重選択解除のための方法および装置

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE759915A (fr) *	1969-12-06	1971-06-04	Stamicarbon	Procede de recyclage pour la preparation et le traitement d'unesolutionde sel d'hydroxylammonium
US3940442A (en) *	1969-12-06	1976-02-24	Stamicarbon B.V.	Recycle process for the preparation and processing of a hydroxylammonium salt solution
NL7507911A (nl) *	1975-07-03	1977-01-05	Stamicarbon	Werkwijze voor de bereiding van een hydroxylamine- zout.
DE3107702A1 (de) *	1981-02-28	1982-09-16	Basf Ag, 6700 Ludwigshafen	Verfahren zur kontinuierlichen herstellung von hydroxylammoniumsalzen
KR830007476A (ko) *	1981-12-18	1983-10-21	전민제	에탄올의 탈수공정에 의한 에틸렌의 제조방법
FR2678944B1 (fr) *	1991-07-10	1993-11-19	Total Raffinage Distribution Sa	Procede et dispositif pour le remplacement en continu du catalyseur dans une unite a lit mobile.
JP2604358Y2 (ja) *	1993-04-09	2000-05-08	ザ・ビーオーシー・グループ・インコーポレーテッド	窒素発生装置
BE1009767A3 (nl) *	1995-11-10	1997-08-05	Dsm Nv	Werkwijze voor de bereiding van hydroxylammoniumzouten.
NL1013899C2 (nl) *	1999-12-21	2001-06-25	Dsm Nv	Werkwijze voor het bereiden en zuiveren van een hydroxylammoniumzoutoplossing.
DE60118745T2 (de) *	2000-06-05	2006-11-16	Dsm Ip Assets B.V.	Verfahren zur herstellung von cyclohexanonoxim
CN1391981A (zh) *	2001-06-15	2003-01-22	中国石油化工股份有限公司巴陵分公司	一种延长羟胺催化剂使用寿命的方法
EP1275616A1 (de) *	2001-07-11	2003-01-15	Dsm N.V.	Verfahren zur Herstellung von Hydroxylamin
JP4318547B2 (ja) *	2001-12-04	2009-08-26	ディーエスエムアイピーアセッツビー．ブイ．	リン酸塩および有機化合物を含む水性媒体を処理する方法

2006
- 2006-07-04 EP EP06754663A patent/EP1901994B1/de not_active Not-in-force
- 2006-07-04 US US11/988,167 patent/US20090221854A1/en not_active Abandoned
- 2006-07-04 PL PL06754663T patent/PL1901994T3/pl unknown
- 2006-07-04 BR BRPI0613171-9A patent/BRPI0613171A2/pt not_active IP Right Cessation
- 2006-07-04 AT AT06754663T patent/ATE456541T1/de not_active IP Right Cessation
- 2006-07-04 WO PCT/EP2006/006507 patent/WO2007006458A1/en not_active Ceased
- 2006-07-04 EA EA200800275A patent/EA014243B1/ru not_active IP Right Cessation
- 2006-07-04 KR KR1020087000390A patent/KR101311626B1/ko active Active
- 2006-07-04 MX MX2008000324A patent/MX2008000324A/es unknown
- 2006-07-04 UA UAA200801248A patent/UA91708C2/ru unknown
- 2006-07-04 DE DE602006012048T patent/DE602006012048D1/de active Active
- 2006-07-04 CN CN2006800249446A patent/CN101218171B/zh not_active Expired - Fee Related
- 2006-07-04 JP JP2008519851A patent/JP5256031B2/ja not_active Expired - Fee Related
- 2006-07-06 MY MYPI20063225A patent/MY143223A/en unknown
- 2006-07-07 TW TW095124830A patent/TWI402211B/zh not_active IP Right Cessation

Also Published As

Publication number	Publication date
TW200710023A (en)	2007-03-16
MY143223A (en)	2011-03-31
CN101218171A (zh)	2008-07-09
EP1901994B1 (de)	2010-01-27
PL1901994T3 (pl)	2010-06-30
UA91708C2 (ru)	2010-08-25
TWI402211B (zh)	2013-07-21
KR20080023725A (ko)	2008-03-14
EA200800275A1 (ru)	2008-06-30
DE602006012048D1 (de)	2010-03-18
JP5256031B2 (ja)	2013-08-07
CN101218171B (zh)	2012-09-26
WO2007006458A1 (en)	2007-01-18
MX2008000324A (es)	2008-03-11
EA014243B1 (ru)	2010-10-29
JP2009500280A (ja)	2009-01-08
BRPI0613171A2 (pt)	2010-12-21
EP1901994A1 (de)	2008-03-26
KR101311626B1 (ko)	2013-09-26
US20090221854A1 (en)	2009-09-03

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Legal Events

Date	Code	Title	Description
2010-07-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties