ATE496928T1 - Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanen - Google Patents

Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanen

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Publication number
ATE496928T1
ATE496928T1 AT05817544T AT05817544T ATE496928T1 AT E496928 T1 ATE496928 T1 AT E496928T1 AT 05817544 T AT05817544 T AT 05817544T AT 05817544 T AT05817544 T AT 05817544T AT E496928 T1 ATE496928 T1 AT E496928T1
Authority
AT
Austria
Prior art keywords
formula
metal
optionally
c18alkenyl
c18alkyl
Prior art date
Application number
AT05817544T
Other languages
English (en)
Inventor
Peter Murer
Jean-Pierre Wolf
Stephan Burkhardt
Hansjoerg Gruetzmacher
Daniel Stein
Kurt Dietliker
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Application granted granted Critical
Publication of ATE496928T1 publication Critical patent/ATE496928T1/de

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • GPHYSICS
    • G03PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03FPHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/004Photosensitive materials
    • G03F7/027Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds
    • G03F7/028Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds with photosensitivity-increasing substances, e.g. photoinitiators
    • G03F7/029Inorganic compounds; Onium compounds; Organic compounds having hetero atoms other than oxygen, nitrogen or sulfur
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/5036Phosphines containing the structure -C(=X)-P or NC-P
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/53Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5337Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/5537Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom the heteroring containing the structure -C(=O)-N-C(=O)- (both carbon atoms belong to the heteroring)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/655Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
    • C07F9/65515Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a five-membered ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/655Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
    • C07F9/6552Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a six-membered ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polymerisation Methods In General (AREA)
AT05817544T 2004-11-23 2005-11-14 Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanen ATE496928T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP04105987 2004-11-23
PCT/EP2005/055935 WO2006056541A1 (en) 2004-11-23 2005-11-14 Process for preparing acylphosphanes and derivatives thereof

Publications (1)

Publication Number Publication Date
ATE496928T1 true ATE496928T1 (de) 2011-02-15

Family

ID=34929912

Family Applications (1)

Application Number Title Priority Date Filing Date
AT05817544T ATE496928T1 (de) 2004-11-23 2005-11-14 Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanen

Country Status (9)

Country Link
US (1) US7687657B2 (de)
EP (1) EP1814891B1 (de)
JP (1) JP5148283B2 (de)
KR (1) KR101230940B1 (de)
CN (1) CN101065388B (de)
AT (1) ATE496928T1 (de)
DE (1) DE602005026156D1 (de)
TW (1) TW200630376A (de)
WO (1) WO2006056541A1 (de)

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EP1838721B1 (de) 2005-01-17 2011-12-21 Basf Se Verfahren zur herstellung von acylphosphan und deren oxide und sulfide
EP2199273B1 (de) 2008-12-18 2018-02-21 Agfa Nv Polymerisierbare Fotoinitiatoren und strahlungshärtbare Zusammensetzungen
EP2421903B1 (de) * 2009-04-20 2014-11-19 ETH Zurich Polymernanopartikel
WO2010133381A1 (en) 2009-05-18 2010-11-25 Agfa Graphics Nv Polymerizable polymeric photoinitiators and radiation curable compositions
US8883872B2 (en) 2009-07-06 2014-11-11 Basf Se Polymer-bound bisacylphosphine oxides
US9062082B2 (en) 2010-06-30 2015-06-23 Dsm Ip Assets B.V. D1479 stable liquid BAP photoinitiator and its use in radiation curable compositions
US8633258B2 (en) 2010-06-30 2014-01-21 Dsm Ip Assets B.V. D1492 liquid BAPO photoinitiator and its use in radiation curable compositions
EP2630164A1 (de) 2010-10-19 2013-08-28 Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. Verfahren zur modifizierung von polymeren, insbesondere polymernanopartikeln
US8921442B2 (en) 2010-10-19 2014-12-30 Max-Planck-Gesellschaft Zur Foerderung Der Wissenschaften E. V. Ultra fast process for the preparation of polymer nanoparticles
CN102924509A (zh) * 2011-08-09 2013-02-13 陈婷 双膦酰膦酸酯化合物
CN103073658A (zh) * 2011-10-26 2013-05-01 深圳市有为化学技术有限公司 新型芳香羟基酮和膦酰氧化物的光引发剂混合物及其与光吸收剂的复合体系
CN103130831A (zh) * 2011-12-01 2013-06-05 深圳市有为化学技术有限公司 巯基取代的酰基膦氧化合物及含有该化合物的光引发剂
WO2014051026A1 (ja) * 2012-09-27 2014-04-03 富士フイルム株式会社 インク組成物、インクジェット記録方法、印刷物、ビスアシルホスフィンオキシド化合物、及び、モノアシルホスフィンオキシド化合物
ES2720760T3 (es) * 2012-10-01 2019-07-24 Eth Zuerich Un procedimiento para la preparación de acilofosfanos
EP2935393A4 (de) 2012-12-18 2016-06-01 Basf Se Halbleitermaterialien auf der basis von naphthalendiimid-vinylen-oligothiophen-vinylenpolymeren
CN110845530A (zh) 2012-12-19 2020-02-28 Igm集团公司 双酰基次膦酸的衍生物、其制备及其作为光敏引发剂的用途
AU2014288876B2 (en) * 2013-07-08 2018-11-22 IGM Group B.V Liquid bisacylphosphine oxide photoinitiator
JP6599446B2 (ja) * 2014-05-30 2019-10-30 アイジーエム レシンス イタリア ソチエタ レスポンサビリタ リミタータ 多官能性アシルホスフィンオキシド光重合開始剤
CN105884824A (zh) * 2014-10-16 2016-08-24 郑成 酰基膦(氧)或磺酰膦(氧)类化合物的制备方法
EP3031798B1 (de) * 2014-12-10 2017-09-27 Belenos Clean Power Holding AG Neuartiger Vernetzer zur Herstellung einer neuen Familie einzelner Ionenleitungspolymere für elektrochemische Vorrichtungen und diese Polymere
CN104592298B (zh) * 2014-12-31 2016-07-06 湖北固润科技股份有限公司 一种酰基膦高效光引发剂及其制备方法
CN104910207B (zh) * 2015-02-12 2019-03-05 天津墨森科技有限公司 双苯甲酰基苯基氧化膦和苯甲酰基二苯基氧化膦的制备方法
EP3296301A1 (de) 2016-09-19 2018-03-21 ETH Zürich Vielseitiges verfahren zur herstellung von acylphosphinen
EP3541440A1 (de) 2016-11-16 2019-09-25 Ecole Polytechnique Federale de Lausanne (EPFL) Fotopolymerisierbares knochenfüllmaterial
WO2018186822A1 (en) 2017-04-03 2018-10-11 Hewlett-Packard Development Company, L.P. Photo active agents
EP3409680B1 (de) * 2017-05-30 2021-01-06 IGM Group B.V. Synthese von bis(acyl)phosphinen durch aktivierung von nicht-reaktiven metallphosphiden
CN107400144B (zh) * 2017-08-03 2020-04-14 深圳有为技术控股集团有限公司 酰基膦(氧)化合物及其制备方法和应用
EP3665232A4 (de) 2017-08-10 2021-04-07 Sun Chemical Corporation Uv-härtbare zusammensetzungen mit acylphosphinoxid-photoinitiatoren
EP3539924A1 (de) 2018-03-14 2019-09-18 ETH Zurich Neuartige vinylphosphine und daraus erhältliche photoinitiatoren
CN112469739A (zh) 2018-04-30 2021-03-09 巴斯夫欧洲公司 来自连续法的高分子量聚合物
US12325723B2 (en) 2018-06-19 2025-06-10 Agfa Nv Acylphosphineoxide initiators
EP3847179A1 (de) 2018-09-07 2021-07-14 IGM Resins Italia S.r.l. Multifunktionelle bisacylphosphinoxid-fotoinitiatoren
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US20220380549A1 (en) 2021-05-12 2022-12-01 Elkem Silicones USA Corp. Method for producing a three-dimensional printed article
US11964425B2 (en) 2021-05-12 2024-04-23 Elkem Silicones USA Corp. Method for producing a three-dimensional printed article
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CN115611943B (zh) * 2021-07-16 2024-12-20 常州强力先端电子材料有限公司 有机磷类引发剂及其制备方法、光固化组合物

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Also Published As

Publication number Publication date
JP5148283B2 (ja) 2013-02-20
TW200630376A (en) 2006-09-01
EP1814891A1 (de) 2007-08-08
CN101065388B (zh) 2011-12-21
US7687657B2 (en) 2010-03-30
KR101230940B1 (ko) 2013-02-08
EP1814891B1 (de) 2011-01-26
WO2006056541A1 (en) 2006-06-01
JP2008520623A (ja) 2008-06-19
KR20070086609A (ko) 2007-08-27
US20080004464A1 (en) 2008-01-03
CN101065388A (zh) 2007-10-31
DE602005026156D1 (de) 2011-03-10

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