BE367351A - - Google Patents

Info

Publication number
BE367351A
BE367351A BE367351DA BE367351A BE 367351 A BE367351 A BE 367351A BE 367351D A BE367351D A BE 367351DA BE 367351 A BE367351 A BE 367351A
Authority
BE
Belgium
Prior art keywords
hydrocarbons
treatment
subjected
desc
distillation
Prior art date
Application number
Other languages
French (fr)
Publication of BE367351A publication Critical patent/BE367351A/fr

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/04Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/04Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen
    • C10G27/14Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen with ozone-containing gases

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treating Waste Gases (AREA)

Description

       

   <Desc/Clms Page number 1> 
 



  "Procédé d'épuration des hydro-carbures   " .   



   On sait que les hydrocarbures, même lorsqu'ils sont épurés, contiennent souvent des substances telles que le soufre qui leur donne une odeur désagréable et qui sont une source de difficultés lorsque ces hydrocarbures doivent être utilisés corame combustible dans des moteurs, D'autre part, les hydrocarbures contiennent souvent du carbone en excès, ce qui nuit également à leur emploi comme combustible, 
Ces impuretés qui existent dans les hydrocarbures bruts se retrouvent également dans les hydrocarbures ayant      

 <Desc/Clms Page number 2> 

 subi la distillation.Cette distillation est donc   insuffi-   sante pour débarrasser les hydrocarbures des impuretés   précitées,,'   
Suivant l'invention, on obtient l'élimination dee, produits sulfurés et du carbone en excès,

   en traitant lee   hydrocarbures   bruts, soit après une première distilla- tion, soit avant toute distillation, par un oxydant éner- gique tel que l'oxygène, l'ozone, l'air ozonisa ou   l'oxy-   gène ozonisé 
Dans un premier mode de réalisation, on commence par éliminer les produits lourds par une distillation au contact' de métaux neutres, de cailloux ou de corps analo- gues   offrant-une   grande surface de contact avec l'hydrocar- bure à   traiter,Ce   procédé est connu en lui-même, aussi n'en sera   t-il pas     parle.. plus   complètement.Le distillat résul-   tant     de:   cette opération   est   un hydrocarbure plus léger, que l'on soumet à l'action des oxydants précités. 



   Dans un deuxième mode de réalisation, on soumet les hydrocarbures   bruts a.   l'action oxydante.Ce traitement s'effectue, en gênerai, à la   température   ordinaire mais, dans certains cas, il peut y avoir avantage à chauffer lé   gèrement.   Grâce à ce traitement on obtient, après un simple lavage alcalin, des   hydrocarbures   désulfurés et dé-   sodorisés   et-la teneur en carbone est   également   abaissée. 



  Cesavantages sont précieux, soit que l'on utilise les hydrocarbures bruts tels quels après los avoir soumis au traitement oxydant précité, soit qu'on les distille après ce traitement pour en extraire des hydrocarbures plus légers 

 <Desc/Clms Page number 3> 

 
A titre d'exemple on sourra, pour réaliser   l'opé-     ration   qui   fuit   l'objet de l'invention, faire barboter 
 EMI3.1 
 un courant <i 'ox;,,<1#iie ou d'air ozonisa ou encore d'ozone dans un r,cii:i,v dans lequel on aura placée au préalable l'r.yd:rocc,:I'1: u."e ù traitpr.I.a proeiesiion de l'action du gaz oxydant se reconnaîtra par des analyses effectuées sur des 
 EMI3.2 
 prince; d' eSl"),;' 180 Il Pst entpndu que 1'invention est applicable non sr-1..,1(."0:

   -'ct eux hydrocarbures destinas à donner des essen- ces eu des ]ni1'-=:3 CO!11;ustU<;'.r's, J!I,ais encore a ceux qui òui'i<is<#<.?i=t les 1.iailes de X'Fil:i:'EtG' REVENDI  CATIONS   
1 .-   Procédé   pour débarrasser les hydrocarbures des   impuretés   telles que le soufre ou carbone qu'ils con- 
 EMI3.3 
 tien0nt, ce procède "tant cnractorise par le fait que l'on soumet 1':;?rocr:rla re a l'action d'un oxydant énergique tel que   l'oxygène,   l'ozone, l'air ozonisé ou l'oxygène   ozonise.   



   2 .-   Procédé   suivant 1 , caractérise par le fait 
 EMI3.4 
 que l'tlydroc;rb1re est d'abord distille pour le transformer fin hydrocarbure 1-cr, nprèr quoi ce dernier est soumis au traitement   oxydant .   

**ATTENTION** fin du champ DESC peut contenir debut de CLMS **.



   <Desc / Clms Page number 1>
 



  "Hydrocarbon purification process".



   It is known that hydrocarbons, even when they are purified, often contain substances such as sulfur which gives them an unpleasant odor and which are a source of difficulties when these hydrocarbons have to be used as fuel in engines. , hydrocarbons often contain excess carbon, which also affects their use as fuel,
These impurities which exist in crude hydrocarbons are also found in hydrocarbons having

 <Desc / Clms Page number 2>

 undergone distillation. This distillation is therefore insufficient to rid the hydrocarbons of the aforementioned impurities.
According to the invention, the removal of sulfur products and excess carbon is obtained,

   by treating the crude hydrocarbons, either after a first distillation or before any distillation, with an energetic oxidant such as oxygen, ozone, ozonized air or ozonized oxygen
In a first embodiment, the heavy products are first removed by distillation in contact with neutral metals, pebbles or the like offering a large contact surface with the hydrocarbon to be treated. This process is known in itself, so it will not be discussed more fully. The distillate resulting from: this operation is a lighter hydrocarbon, which is subjected to the action of the aforementioned oxidants.



   In a second embodiment, the crude hydrocarbons are subjected to a. oxidizing action. This treatment is generally carried out at room temperature, but in some cases it may be advantageous to heat slightly. By virtue of this treatment, after a simple alkaline washing, desulfurized and deodorized hydrocarbons are obtained and the carbon content is also lowered.



  These advantages are valuable, either that one uses the crude hydrocarbons as they are after having subjected them to the aforementioned oxidizing treatment, or that they are distilled after this treatment to extract therefrom lighter hydrocarbons.

 <Desc / Clms Page number 3>

 
By way of example, to carry out the operation which eludes the object of the invention, we will see
 EMI3.1
 a current <i 'ox; ,, <1 # iie or ozonized air or ozone in a r, cii: i, v in which we have previously placed the rd: rocc,: I' 1: u. "E ù treatpr.Ia preaiesiion of the action of the oxidizing gas will be recognized by analyzes carried out on
 EMI3.2
 prince; d 'eSl ") ,;' 180 It is understood that the invention is applicable not sr-1 .., 1 (. "0:

   -'ct them hydrocarbons destined to give essen- tials had] ni1 '- =: 3 CO! 11; ustU <;'. r's, J! I, but also to those which òui'i <is <# <. ? i = t the 1.iails of X'Fil: i: 'EtG' REVENDI CATIONS
1 .- Process for ridding hydrocarbons of impurities such as sulfur or carbon which they contain
 EMI3.3
 Now, this process is "so cnractorized by the fact that one subjects the:;? rocr: rla re to the action of an energetic oxidant such as oxygen, ozone, ozonized air or oxygen ozonizes.



   2 .- Method according to 1, characterized by the fact
 EMI3.4
 that the ethyldroc; rb1re is first distilled to transform it into a fine 1-cr hydrocarbon, nprèr which the latter is subjected to the oxidative treatment.

** ATTENTION ** end of DESC field can contain start of CLMS **.


    

Claims (1)

3 .- Procède suivant 1 caractérise pcr le fait EMI3.5 qu'après avoir été soumis à l'action oxydante, l'hydrocnr- bure subit un ''¯F.va.e d'alcalin pour éliminer les composes oxycèn03 et acides qui se sont formés au cours du traitement. en cours. **ATTENTION** fin du champ CLMS peut contenir debut de DESC **. 3 .- The following procedure 1 characterizes the fact EMI3.5 that after having been subjected to the oxidizing action, the hydrocnrbide undergoes an alkaline ¯F.va.e to remove the oxycen03 and acid compounds which have formed during the treatment. In progress. ** CAUTION ** end of field CLMS may contain start of DESC **.
BE367351D BE367351A (en)

Publications (1)

Publication Number Publication Date
BE367351A true BE367351A (en)

Family

ID=39333

Family Applications (1)

Application Number Title Priority Date Filing Date
BE367351D BE367351A (en)

Country Status (1)

Country Link
BE (1) BE367351A (en)

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