BE509498A - - Google Patents
Info
- Publication number
- BE509498A BE509498A BE509498DA BE509498A BE 509498 A BE509498 A BE 509498A BE 509498D A BE509498D A BE 509498DA BE 509498 A BE509498 A BE 509498A
- Authority
- BE
- Belgium
- Prior art keywords
- zone
- reaction zone
- porous inorganic
- reaction
- solid
- Prior art date
Links
- 238000006243 chemical reaction Methods 0.000 claims description 49
- 238000000034 method Methods 0.000 claims description 30
- 239000007787 solid Substances 0.000 claims description 26
- VUNCWTMEJYMOOR-UHFFFAOYSA-N hexachlorocyclopentadiene Chemical compound ClC1=C(Cl)C(Cl)(Cl)C(Cl)=C1Cl VUNCWTMEJYMOOR-UHFFFAOYSA-N 0.000 claims description 19
- 238000011144 upstream manufacturing Methods 0.000 claims description 17
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 13
- 239000000460 chlorine Substances 0.000 claims description 13
- 229910052801 chlorine Inorganic materials 0.000 claims description 13
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 10
- 229910003480 inorganic solid Inorganic materials 0.000 claims description 10
- 239000000126 substance Substances 0.000 claims description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 8
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 8
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- CZTQZXZIADLWOZ-UHFFFAOYSA-O 8-oxo-3-(pyridin-1-ium-1-ylmethyl)-7-[(2-thiophen-2-ylacetyl)amino]-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid Chemical compound C1SC2C(NC(=O)CC=3SC=CC=3)C(=O)N2C(C(=O)O)=C1C[N+]1=CC=CC=C1 CZTQZXZIADLWOZ-UHFFFAOYSA-O 0.000 claims description 7
- 239000007789 gas Substances 0.000 claims description 7
- 229910052759 nickel Inorganic materials 0.000 claims description 5
- 229910017052 cobalt Inorganic materials 0.000 claims description 4
- 239000010941 cobalt Substances 0.000 claims description 4
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- 229910052742 iron Inorganic materials 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 3
- 125000001309 chloro group Chemical group Cl* 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000012808 vapor phase Substances 0.000 claims description 3
- 229910001570 bauxite Inorganic materials 0.000 claims description 2
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical group [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims description 2
- 229910001510 metal chloride Inorganic materials 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 claims 1
- 230000035515 penetration Effects 0.000 claims 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 22
- 238000005660 chlorination reaction Methods 0.000 description 9
- 239000003085 diluting agent Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000005755 formation reaction Methods 0.000 description 4
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000007363 ring formation reaction Methods 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- 239000011449 brick Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000013021 overheating Methods 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- DBTFFTPJMFQGMK-UHFFFAOYSA-N 1,2,3,3,4,4-hexachlorocyclopentene Chemical compound ClC1=C(Cl)C(Cl)(Cl)C(Cl)(Cl)C1 DBTFFTPJMFQGMK-UHFFFAOYSA-N 0.000 description 1
- SQCZQTSHSZLZIQ-UHFFFAOYSA-N 1-chloropentane Chemical class CCCCCCl SQCZQTSHSZLZIQ-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- 229960000892 attapulgite Drugs 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 230000001447 compensatory effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000006298 dechlorination reaction Methods 0.000 description 1
- 238000007033 dehydrochlorination reaction Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- -1 for example Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052625 palygorskite Inorganic materials 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000008262 pumice Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE509498A true BE509498A (de) |
Family
ID=148908
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE509498D BE509498A (de) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE509498A (de) |
-
0
- BE BE509498D patent/BE509498A/fr unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP1281699B1 (de) | Verfahren zur Herstellung von 1,1,1-Trifluoro-2,2-dichloroethan | |
| EP0639549B1 (de) | Verfahren zur Metathese von Olefinen in dem ein verbesserter Rheniumkatalysator verwendet wird | |
| EP0056548B1 (de) | Kontinuierliches Verfahren zur Gasphasenherstellung in kontrollierten Verhältnissen von Trichlortrifluoräthan, Dichlortetrafluoräthan und Monochlorpentafluoräthan | |
| EP1140747A1 (de) | Verfahren zur trennung einer mischung die mindestens einen hydrofluoralkan und fluorwasserstoff enthält, verfahren zur herstellung eines hydrofluoralkans | |
| CA2245155C (fr) | Procede de separation de fluorure d'hydrogene de ses melanges avec un hydrofluoroalcane contenant de 3 a 6 atomes de carbone | |
| FR3078700A1 (fr) | Procede de production du 2,3,3,3-tetrafluoropropene | |
| EP0739875B1 (de) | Verfahren zur Herstellung von 1,1-Difluorethan | |
| EP0582494B1 (de) | Verfahren zur Reinigung von 1,1,1,2-Tetrafluorethan | |
| BE509498A (de) | ||
| FR2631959A1 (fr) | Procede de preparation de 1,1,1,2-tetrafluoroethane a partir de 1,1-dichloro-1,2,2,2-tetrafluoroethane | |
| FR2463745A1 (fr) | Procede pour preparer le sulfure de carbonyle | |
| EP0798043A1 (de) | Regenerierung von Katalysatoren zur Fluorierung in der Gasphase | |
| FR2510101A1 (fr) | Procede d'hydrolyse catalytique en phase vapeur de chlorure de benzal ou son substitut avec un halogene ou un trifluoromethyle, pour former du benzaldehyde ou son substitut | |
| FR2805534A1 (fr) | Procede de preparation du 1,1,1-trifluoro-2,2-dichloroethane | |
| EP0882012B1 (de) | Verfahren zur herstellung von aromatischen derivaten die ortho-disubstituiert sind durch ein halogenatom anders als fluor, und durch eine cyanogruppe | |
| FR3068969A1 (fr) | Procede de production du 2,3,3,3-tetrafluoropropene. | |
| EP0732314B1 (de) | Verfahren zur Herstellung von Difluormethan | |
| EP1165475A1 (de) | Verfahren zur abtrennung von fluorwasserstoff aus seinen mischungen mit 1,1,1,3,3-pentafluorbutan und verfahren zur herstellung von pentafluorbutan | |
| BE897411A (fr) | Procede de formation de nitromethane | |
| EP0235110B1 (de) | Verfahren zur Stabilisierung von Silikalit-Katalysatoren | |
| EP0732315A1 (de) | Verfahren zur Hydrogenolyse von Chlorfluorkohlenwasserstoffen und Hydrochlorfluorkohlenwasserstoffen | |
| BE845572A (fr) | Procede catalytique de decomposition de composes organiques halogenes | |
| FR2648812A1 (fr) | Procede d'oxydation de l'ethylene glycol pour la production de glyoxal | |
| CA2094201A1 (fr) | Procede pour l'epuration de 1,1,-dichloro-1-fluoroethane | |
| BE483331A (de) |