BR0102576A - Processo e equipamento de fabricação para a preparação de acetais ou cetais - Google Patents

Processo e equipamento de fabricação para a preparação de acetais ou cetais

Info

Publication number
BR0102576A
BR0102576A BR0102576-7A BR0102576A BR0102576A BR 0102576 A BR0102576 A BR 0102576A BR 0102576 A BR0102576 A BR 0102576A BR 0102576 A BR0102576 A BR 0102576A
Authority
BR
Brazil
Prior art keywords
acetals
ketals
preparation
ketone
alcohol
Prior art date
Application number
BR0102576-7A
Other languages
English (en)
Inventor
Volkmar Boesch
Juan Ramon Herguijuela
Original Assignee
Hoffmann La Roche
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoffmann La Roche filed Critical Hoffmann La Roche
Publication of BR0102576A publication Critical patent/BR0102576A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
    • B01D61/362—Pervaporation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/48—Preparation of compounds having groups
    • C07C41/50—Preparation of compounds having groups by reactions producing groups
    • C07C41/56—Preparation of compounds having groups by reactions producing groups by condensation of aldehydes, paraformaldehyde, or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/48—Preparation of compounds having groups
    • C07C41/58—Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Patente de Invenção: "PROCESSO E EQUIPAMENTO DE FABRICAçãO PARA A PREPARAçãO DE ACETAIS OU CETAIS". A presente invenção refere-se a um novo processo para a preparação de acetais e cetais. Como se sabe, os acetais e os cetais podem ser preparados por reação de um aldeido ou uma cetona com um álcool na presença de um catalisador catiónico. No entanto, a reação é reversível e, em temperatura ambiente ou acima, o equilibrio da reação é desviado para o lado dos materiais de partida, acetal ou cetona, e álcool. A invenção fornece um novo processo para a preparação contínua de acetais e cetais na forma concentrada e evita procedimentos de destilação de energia concentrada dos processos de fabricação convencionais, que freq³entemente tornam-se difíceis pela formação de azeótropos. A presente invenção refere-se ainda a um equipamento de fabricação para a realização do processo da invenção substancialmente como mostrado na figura 1 que compreende um reator (1) contendo um ácido sólido; um recipiente (2) que contém uma base sólida; e uma unidade de pervaporação (3) que tem uma membrana que é permeável para água.
BR0102576-7A 2000-06-26 2001-06-26 Processo e equipamento de fabricação para a preparação de acetais ou cetais BR0102576A (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP00113463 2000-06-26

Publications (1)

Publication Number Publication Date
BR0102576A true BR0102576A (pt) 2002-03-19

Family

ID=8169065

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0102576-7A BR0102576A (pt) 2000-06-26 2001-06-26 Processo e equipamento de fabricação para a preparação de acetais ou cetais

Country Status (7)

Country Link
US (2) US6528025B1 (pt)
JP (1) JP2002020339A (pt)
KR (1) KR20020001588A (pt)
CN (1) CN1217884C (pt)
BR (1) BR0102576A (pt)
CA (1) CA2351124A1 (pt)
TW (1) TWI225047B (pt)

Families Citing this family (42)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001038811A1 (en) 1999-11-26 2001-05-31 Nkk Corporation Thermal storage material using hydrate and thermal storage device therefor, and production method of the thermal storage material
EP1510763B1 (en) * 2002-05-31 2012-02-01 JFE Engineering Corporation Apparatus for producing hydrate slurry
DE102004049056A1 (de) * 2004-10-08 2006-04-13 Ticona Gmbh Verfahren zur Herstellung und Reinigung von zyklischen Formalen
JP2006289158A (ja) * 2005-04-05 2006-10-26 Mitsubishi Heavy Ind Ltd アセタール合成触媒及びアセタール製造方法
JP4949643B2 (ja) * 2005-06-06 2012-06-13 三菱重工業株式会社 ケタール合成装置及びケタール合成方法
JP4690780B2 (ja) * 2005-06-06 2011-06-01 三菱重工業株式会社 ケタール合成装置及びケタール合成方法
EP1954140B1 (en) 2005-11-22 2013-05-29 Segetis, Inc. Glycerol levulinate ketals and their use
WO2009032905A1 (en) 2007-09-04 2009-03-12 Segetis, Inc. Ketal compounds from polyols and oxocarboxylates
BRPI0818370A2 (pt) * 2007-10-09 2017-05-16 Segetis Inc métodos de fabricar cetais e acetais
WO2009146202A2 (en) * 2008-04-16 2009-12-03 Segetis, Inc. Transketalized compositions, synthesis, and applications
WO2010036884A1 (en) 2008-09-25 2010-04-01 Segetis, Inc. Ketal ester derivatives
US20100240915A1 (en) * 2009-02-02 2010-09-23 Robert Jansen Pre-Treatment of Crude Alcohol or Furan Feed to a Vapor Permeation Apparatus
PT104496B (pt) * 2009-04-08 2011-03-14 Univ Do Porto Reactor de membranas adsorptivo de leito móvel simulado, novo processo híbrido de saparação e respectivas utilizações
US9012570B2 (en) * 2009-04-18 2015-04-21 Eastman Chemical Company Continuous production of poly(vinyl butyral)
US7960503B2 (en) * 2009-05-26 2011-06-14 Solutia, Inc. Continuous washing of poly(vinyl butyral)
BRPI1013943B1 (pt) 2009-06-22 2020-03-17 Segetis, Inc. Composto, método para sintetizar o mesmo, composição e composição lubrificante
AU2011250962B2 (en) 2010-05-10 2015-09-03 Gfbiochemicals Limited Personal care formulations containing alkyl ketal esters and methods of manufacture
BR112013000575A2 (pt) 2010-08-03 2016-07-05 Segetis Inc métodos para a fabricação de acetais e cetais, e acetais e cetais produzidos por este meio
US9074065B2 (en) 2010-08-12 2015-07-07 Segetis, Inc. Latex coating compositions including carboxy ester ketal coalescents, methods of manufacture, and uses thereof
WO2012021824A2 (en) 2010-08-12 2012-02-16 Segetis, Inc. Carboxy ester ketal removal compositions, methods of manufacture, and uses thereof
EP2613760A2 (en) 2010-09-07 2013-07-17 Segetis, Inc. Compositions for dyeing keratin fibers
WO2012054505A2 (en) 2010-10-18 2012-04-26 Segetis, Inc. Water reducible coating compositions including carboxy ester ketals, methods of manufacture, and uses thereof
KR20140009179A (ko) 2010-11-11 2014-01-22 세게티스, 인코포레이티드. 폴리케탈 부가물, 그의 제조방법 및 용도
US8507718B2 (en) 2010-11-11 2013-08-13 Segetis, Inc. Ketocarboxylic acids, methods of manufacture and uses thereof
US9187598B2 (en) 2010-11-11 2015-11-17 Segetis, Inc. Polyhydroxy ketal ester adducts, methods of manufacture and uses thereof
CN102079740A (zh) * 2010-12-07 2011-06-01 尹华芳 一种丁醛乙二醇缩醛的制备方法
WO2013004626A1 (en) 2011-07-06 2013-01-10 Dsm Ip Assets B.V. Process for preparing acetals and ketals
CN107673955A (zh) 2011-07-06 2018-02-09 帝斯曼知识产权资产管理有限公司 通过渗透蒸发的方式制备或回收缩醛或缩酮的方法
CN102731273B (zh) * 2012-07-09 2014-11-26 北京大学 一种缩醛的制备方法
US9458414B2 (en) 2012-09-21 2016-10-04 Gfbiochemicals Limited Cleaning, surfactant, and personal care compositions
JP2016506383A (ja) 2012-11-29 2016-03-03 サジティス・インコーポレイテッド カルボキシエステルケタール、その製造方法および使用
CN104326888B (zh) * 2014-09-27 2016-06-08 安徽华甬新材料有限公司 一种2,2-二甲氧基丙烷制备方法
CN105817228B (zh) * 2016-04-15 2018-11-23 黄山学院 直接使用粉煤灰催化制备环己酮二醇缩酮类化合物的方法
CN106631720B (zh) * 2016-11-02 2020-06-05 东方红升江苏新能源有限公司 以稀甲醛和甲缩醛为原料直接合成聚甲氧基二甲醚的方法
CN106540550A (zh) * 2016-11-02 2017-03-29 东方红升江苏新能源有限公司 用于制取聚甲氧基二甲醚的原料膜脱水方法
CN110304997B (zh) * 2018-03-20 2022-02-11 中国石油化工股份有限公司 一种2,2-二甲氧基丙烷的生产方法
CN110227558B (zh) * 2019-06-18 2022-03-11 万华化学集团股份有限公司 一种用于制备缩醛/酮的固体酸催化剂及其制备方法和应用
CA3160961A1 (en) 2019-11-22 2021-05-27 Endurance Solar Solutions B.V. Photovoltaic module backsheet comprising polyolefin layers
CN115135630A (zh) * 2020-02-28 2022-09-30 帝斯曼知识产权资产管理有限公司 用于制造1,1,4,4-四甲氧基-2-丁烯的可持续方法
CN112250659B (zh) * 2020-10-21 2021-12-21 江苏阿尔法药业股份有限公司 一种阿托伐他汀钙中间体的合成方法
CN113461498B (zh) * 2021-07-19 2023-04-25 老河口光联科技有限公司 一种缩醛的环保型制备方法
CN117427469A (zh) * 2023-11-30 2024-01-23 福建海德福新材料有限公司 一种去除混合气体中全氟异丁烯的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2929827A1 (de) 1979-07-23 1981-02-26 Basf Ag Verfahren zur kontinuierlichen herstellung von 2,2-dimethoxypropan
US5156740A (en) 1982-06-01 1992-10-20 Gft Ingenieurburo Fur Industrieanlagenbau Multi-layer membrane and the use thereof for the separation of liquid mixtures according to the pervaporation process
DE3220570A1 (de) 1982-06-01 1983-12-01 GFT Ingenieurbüro für Industrieanlagenbau, 6650 Homburg Mehrschichtige membran und ihre verwendung zur trennung von fluessigkeitsgemischen nach dem pervaporationsverfahren
US4775447A (en) * 1984-06-18 1988-10-04 Sun Refining And Marketing Company Process for the production of 2,2-dimethoxypropane
US5717081A (en) 1993-09-17 1998-02-10 Unichema Chemie B.V. Process for producing an alkylglycoside using a pervaporation membrane to remove reaction water
DE4431994A1 (de) 1994-09-08 1996-03-14 Degussa Verfahren zur Herstellung von 1,1,3-Trialkoxypropan
DE19617893C1 (de) * 1996-05-04 1997-10-02 Hoechst Ag Verfahren zur Herstellung von Polyvinylacetalen und -ketalen
DE19811451C1 (de) 1998-03-17 1999-10-14 Henkel Kgaa Verfahren zur Acetalisierung bzw. Ketalisierung

Also Published As

Publication number Publication date
CN1330058A (zh) 2002-01-09
CA2351124A1 (en) 2001-12-26
US6806392B2 (en) 2004-10-19
US6528025B1 (en) 2003-03-04
JP2002020339A (ja) 2002-01-23
KR20020001588A (ko) 2002-01-09
TWI225047B (en) 2004-12-11
CN1217884C (zh) 2005-09-07
US20040106832A1 (en) 2004-06-03

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Legal Events

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B25A Requested transfer of rights approved

Free format text: DSM IP ASSETS B.V. (NL)

B03H Publication of an application: rectification [chapter 3.8 patent gazette]

Free format text: REFERENTE A RPI 1628 DE 19/03/2002, ITEM 72.

B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: REFERENTE A 8A ANUIDADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE AO DESPACHO 8.6 DA RPI 2012 DE 28/07/2009.