BR0109916A - Purificação de glicol - Google Patents
Purificação de glicolInfo
- Publication number
- BR0109916A BR0109916A BR0109916-7A BR0109916A BR0109916A BR 0109916 A BR0109916 A BR 0109916A BR 0109916 A BR0109916 A BR 0109916A BR 0109916 A BR0109916 A BR 0109916A
- Authority
- BR
- Brazil
- Prior art keywords
- aldehydes
- glycol purification
- acetaldehyde
- formaldehyde
- contacted
- Prior art date
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title abstract 5
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 abstract 2
- 150000001299 aldehydes Chemical class 0.000 abstract 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 abstract 1
- 239000003957 anion exchange resin Substances 0.000 abstract 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Removal Of Specific Substances (AREA)
- Saccharide Compounds (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Furan Compounds (AREA)
- Cleaning Or Drying Semiconductors (AREA)
Abstract
"PURIFICAçãO DE GLICOL". Uma solução aquosa de etilenoglicol contendo aldeídos tais como formaldeído, acetaldeído e semelhantes é contatada com uma resina trocadora de ânion de base forte tratada com bissulfito sólido, e uma solução reduzida em teor de aldeído é separada.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/544,029 | 2000-04-06 | ||
| US09/544,029 US6187973B1 (en) | 2000-04-06 | 2000-04-06 | Glycol purification |
| PCT/US2001/010406 WO2001077049A1 (en) | 2000-04-06 | 2001-03-30 | Glycol purification |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR0109916A true BR0109916A (pt) | 2005-10-18 |
| BR0109916B1 BR0109916B1 (pt) | 2012-10-30 |
Family
ID=24170488
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0109916-7A BR0109916B1 (pt) | 2000-04-06 | 2001-03-30 | método para reduzir o teor de aldeìdos de uma solução aquosa de etilenoglicol contendo aldeìdos. |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US6187973B1 (pt) |
| EP (1) | EP1268377B1 (pt) |
| AT (1) | ATE367370T1 (pt) |
| AU (2) | AU4791201A (pt) |
| BG (1) | BG65962B1 (pt) |
| BR (1) | BR0109916B1 (pt) |
| DE (1) | DE60129421T2 (pt) |
| DK (1) | DK1268377T3 (pt) |
| ES (1) | ES2290122T3 (pt) |
| PT (1) | PT1268377E (pt) |
| RO (1) | RO121025B1 (pt) |
| RU (1) | RU2265584C2 (pt) |
| WO (1) | WO2001077049A1 (pt) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2221766C1 (ru) * | 2002-07-30 | 2004-01-20 | Белокурова Ирина Николаевна | Способ очистки отработанного антифриза на основе водно-этиленгликолевого раствора от продуктов окисления этиленгликоля, продуктов коррозии и механических примесей |
| US7182841B2 (en) * | 2003-04-23 | 2007-02-27 | Huntsman International Llc | Purification of solvents used for the purification of alkylene oxide |
| TW200838838A (en) * | 2006-12-22 | 2008-10-01 | Dow Technology Investments Llc | Process for reducing side-reactions during alkylene glycol and poly-alkylene glycol manufacturing |
| WO2009094103A1 (en) | 2008-01-25 | 2009-07-30 | Dow Technology Investments Llc | Reflux condenser |
| CN106242945A (zh) * | 2008-11-10 | 2016-12-21 | 陶氏技术投资有限公司 | 用于生产低色素二醇的方法 |
| BR112015026194A2 (pt) | 2013-04-15 | 2017-07-25 | Scient Design Co | processo de epoxidação |
| CN106866366B (zh) * | 2015-12-12 | 2020-05-05 | 中国科学院大连化学物理研究所 | 一种去除乙二醇中二元醇或多元醇杂质并增产乙二醇的方法 |
| EP3497088B1 (en) | 2016-08-09 | 2021-12-29 | Scientific Design Company, Inc. | Epoxidation process |
| RU2622395C1 (ru) * | 2016-08-15 | 2017-06-15 | Публичное акционерное общество "СИБУР Холдинг" | Способ очистки гликолей от примесей |
| WO2019097407A1 (en) | 2017-11-16 | 2019-05-23 | Sabic Global Technologies B.V. | Reactive polymeric resin for removal of aldehydes |
| CN109293475A (zh) * | 2018-11-15 | 2019-02-01 | 北京兴高化学技术有限公司 | 煤制乙二醇精制方法及系统 |
| US12303859B2 (en) | 2019-08-27 | 2025-05-20 | Sabic Global Technologies B.V. | Mass transfer swirler including distribution member |
| CN112441880B (zh) * | 2019-09-02 | 2023-04-07 | 中国石油化工股份有限公司 | 用于乙二醇脱醛精制的脱醛剂及乙二醇脱醛精制的方法 |
| US11926540B2 (en) | 2021-03-05 | 2024-03-12 | Scientific Design Company, Inc. | Cycle water treatment process for ethlyene epoxidation |
| EP4724514A1 (de) | 2023-06-06 | 2026-04-15 | Zschimmer & Schwarz Chemie GmbH | Verfahren zur mindestens teilweisen entfernung von aldehyden aus einer zusammensetzung enthaltend mindestens eine verbindung mit mindestens einer alkylenoxideinheit |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3904656A (en) | 1973-02-13 | 1975-09-09 | Ppg Industries Inc | Process for preparing monoethylene glycol and ethylene oxide |
| FR2295938A1 (fr) | 1974-12-24 | 1976-07-23 | Naphtachimie Sa | Separation des glycols contenus dans des solutions residuaires |
| IT1063805B (it) | 1976-11-17 | 1985-02-18 | Snam Progetti | Procedimento per la produzione di glicoli etilenici ad alta purezza |
| DE3001727A1 (de) | 1980-01-18 | 1981-07-23 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von hochreinem monoethylenglykol |
| US4560813A (en) | 1984-03-28 | 1985-12-24 | Union Carbide Corporation | Processes for the production of alkylene glycol in the presence of organometalate |
| CA1330350C (en) * | 1986-10-07 | 1994-06-21 | Thomas Martin Schmitt | Method for purification of ethylene glycol |
| US5440058A (en) | 1994-06-07 | 1995-08-08 | Union Carbide Chemicals & Plastics Technology Corporation | Method for separating compounds in process streams |
| RU2122995C1 (ru) * | 1997-09-09 | 1998-12-10 | Швец Валерий Федорович | Способ получения алкиленгликолей |
| CN1069605C (zh) * | 1998-08-20 | 2001-08-15 | 南亚塑胶工业股份有限公司 | 从乙二醇制程水中去除甲酸、乙酸的方法和装置 |
-
2000
- 2000-04-06 US US09/544,029 patent/US6187973B1/en not_active Expired - Lifetime
-
2001
- 2001-03-30 PT PT01920904T patent/PT1268377E/pt unknown
- 2001-03-30 DE DE60129421T patent/DE60129421T2/de not_active Expired - Lifetime
- 2001-03-30 DK DK01920904T patent/DK1268377T3/da active
- 2001-03-30 ES ES01920904T patent/ES2290122T3/es not_active Expired - Lifetime
- 2001-03-30 BR BRPI0109916-7A patent/BR0109916B1/pt not_active IP Right Cessation
- 2001-03-30 RU RU2002128919/04A patent/RU2265584C2/ru active
- 2001-03-30 RO ROA200201276A patent/RO121025B1/ro unknown
- 2001-03-30 WO PCT/US2001/010406 patent/WO2001077049A1/en not_active Ceased
- 2001-03-30 AU AU4791201A patent/AU4791201A/xx active Pending
- 2001-03-30 AU AU2001247912A patent/AU2001247912B2/en not_active Expired
- 2001-03-30 AT AT01920904T patent/ATE367370T1/de active
- 2001-03-30 EP EP01920904A patent/EP1268377B1/en not_active Expired - Lifetime
-
2002
- 2002-09-27 BG BG107154A patent/BG65962B1/bg unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BG107154A (bg) | 2003-05-30 |
| EP1268377A4 (en) | 2005-09-21 |
| WO2001077049A1 (en) | 2001-10-18 |
| PT1268377E (pt) | 2007-10-24 |
| EP1268377B1 (en) | 2007-07-18 |
| DE60129421D1 (de) | 2007-08-30 |
| ES2290122T3 (es) | 2008-02-16 |
| DE60129421T2 (de) | 2008-04-17 |
| RU2265584C2 (ru) | 2005-12-10 |
| DK1268377T3 (da) | 2007-11-12 |
| US6187973B1 (en) | 2001-02-13 |
| RO121025B1 (ro) | 2006-11-30 |
| EP1268377A1 (en) | 2003-01-02 |
| BR0109916B1 (pt) | 2012-10-30 |
| AU4791201A (en) | 2001-10-23 |
| ATE367370T1 (de) | 2007-08-15 |
| BG65962B1 (bg) | 2010-07-30 |
| AU2001247912B2 (en) | 2005-10-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 30/10/2012, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B21A | Patent or certificate of addition expired [chapter 21.1 patent gazette] |
Free format text: PATENTE EXTINTA EM 30.10.2022 |