BR9909355A - Processos para a preparação de ácido acrìlico e de acrilato - Google Patents

Processos para a preparação de ácido acrìlico e de acrilato

Info

Publication number
BR9909355A
BR9909355A BR9909355-3A BR9909355A BR9909355A BR 9909355 A BR9909355 A BR 9909355A BR 9909355 A BR9909355 A BR 9909355A BR 9909355 A BR9909355 A BR 9909355A
Authority
BR
Brazil
Prior art keywords
acrylic acid
esters
acrylate
processes
preparation
Prior art date
Application number
BR9909355-3A
Other languages
English (en)
Inventor
Gerhard Nestler
J Rgen Sch Rder
Gerhard Bolz
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of BR9909355A publication Critical patent/BR9909355A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

"PROCESSOS PARA A PREPARAçãO DE áCIDO ACRìLICO E DE ACRILATO". A invenção está relacionada a processo para a produção de ácido acrílico ou ésteres de ácido acrílico, a qual compreende a etapa A e opcionalmente as etapas B e C, como se segue: A: resfriar uma mistura gasosa de reação formada durante o processo de oxidação em fase gasosa para a produção de ácido acrílico e que contém ácido acrílico, usando um solvente inerte com alto ponto de ebulição, para produzir uma mistura gasosa contendo ácido acrílico; B: separar a mistura gasosa contendo ácido acrílico para produzir uma fração com baixo ponto de ebulição, um ácido acrílico bruto e um produto de fundo, e C: esterificar o ácido acrílico bruto obtido na etapa B usando um ou mais alcanóis para obter uma mistura da esterificação contendo um ou mais ésteres do ácido acrílico e um ou mais ésteres do ácido acético.
BR9909355-3A 1998-03-31 1999-03-24 Processos para a preparação de ácido acrìlico e de acrilato BR9909355A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19814375A DE19814375A1 (de) 1998-03-31 1998-03-31 Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern
PCT/EP1999/001998 WO1999050220A1 (de) 1998-03-31 1999-03-24 Verfahren zur herstellung von acrylsäure und acrylsäureestern

Publications (1)

Publication Number Publication Date
BR9909355A true BR9909355A (pt) 2000-12-12

Family

ID=7863098

Family Applications (1)

Application Number Title Priority Date Filing Date
BR9909355-3A BR9909355A (pt) 1998-03-31 1999-03-24 Processos para a preparação de ácido acrìlico e de acrilato

Country Status (8)

Country Link
US (1) US6555707B1 (pt)
EP (1) EP1066240B1 (pt)
JP (1) JP4410935B2 (pt)
CN (1) CN1133614C (pt)
BR (1) BR9909355A (pt)
DE (2) DE19814375A1 (pt)
MY (1) MY120799A (pt)
WO (1) WO1999050220A1 (pt)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MY122671A (en) 1999-03-06 2006-04-29 Basf Ag Fractional condensation of a product gas mixture containing acrylic acid
ES2206197T3 (es) 1999-03-06 2004-05-16 Basf Aktiengesellschaft Procedimiento para la obtencion de acido acrilico.
JP2001226320A (ja) * 2000-02-14 2001-08-21 Nippon Shokubai Co Ltd アクリル酸の捕集方法およびアクリル酸の精製方法
US6888025B2 (en) 2000-02-14 2005-05-03 Nippon Shokubai, Co. Ltd. Method for absorbing acrylic acid and method for purifying acrylic acid
DE10063161A1 (de) * 2000-12-18 2002-06-20 Basf Ag Verfahren zum Abschrecken eines heißen (Meth)acrylsäure enthaltenden Gasgemisches
WO2003095411A1 (de) * 2002-05-08 2003-11-20 Basf Aktiengesellschaft Verfahren zur herstellung von acrylsäure und/ oder deren ester sowie von propionsäure und/ oder deren ester im verbund
US8431743B2 (en) 2004-07-01 2013-04-30 Basf Aktiengesellschaft Preparation of acrylic acid by heterogeneously catalyzed partial gas phase oxidation of propylene
US7601866B2 (en) 2005-03-01 2009-10-13 Basf Aktiengesellschaft Process for removing methacrolein from liquid phase comprising acrylic acid as a main constituent and target product, and methacrolein as a secondary component
US7705181B2 (en) 2005-03-01 2010-04-27 Basf Akiengesellschaft Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component
KR100999428B1 (ko) * 2006-01-20 2010-12-09 니폰 쇼쿠바이 컴파니 리미티드 (메타)아크릴산의 제조 방법
JP5368673B2 (ja) * 2006-01-20 2013-12-18 株式会社日本触媒 （メタ）アクリル酸の製造方法
US8242308B2 (en) 2006-09-15 2012-08-14 Arkema Inc. Process for producing acrylic acid
CN101589015B (zh) * 2007-01-26 2013-11-13 巴斯夫欧洲公司 生产丙烯酸的方法
DE102008040799A1 (de) 2008-07-28 2008-12-11 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
DE102008041573A1 (de) 2008-08-26 2010-03-04 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
BRPI0916635B1 (pt) 2008-07-28 2020-04-14 Basf Se processo para separar ácido acrílico, presente como um produto principal, e glioxal, presente como um subproduto em uma mistura gasosa
US8828231B2 (en) * 2008-09-03 2014-09-09 Arkema Inc. Method for recovering carboxylic acids from dilute aqueous streams
DE102010042216A1 (de) 2010-10-08 2011-06-09 Basf Se Verfahren zur Hemmung der unerwünschten radikalischen Polymerisation von in einer flüssigen Phase P befindlicher Acrylsäure
KR102893876B1 (ko) 2018-07-26 2025-12-03 바스프 에스이 액상 p 중 존재하는 아크릴산의 원치않는 라디칼 중합의 억제 방법
WO2021191042A1 (de) 2020-03-26 2021-09-30 Basf Se Verfahren zur hemmung der unerwünschten radikalischen polymerisation von in einer flüssigen phase p befindlicher acrylsäure
DE102023212959A1 (de) 2023-12-19 2025-06-26 Powerco Se Beschichtungsverfahren und Beschichtungsanlage zum Beschichten eines Objekts

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1452566A (fr) 1964-11-06 1966-02-25 Mitsubishi Petrochemical Co Procédé perfectionné pour récupérer les esters acryliques et méthacryliques sous forme purifiée à partir de solutions aqueuses diluées d'acide acrylique et méthacrylique
US3555082A (en) 1966-12-15 1971-01-12 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein
DE1668362B2 (de) 1968-02-17 1976-11-11 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung aliphatischer acrylsaeureester
DE1910795A1 (de) * 1969-03-04 1970-09-17 Degussa Verfahren zur Vermeidung von Nachreaktionen bei der katalytischen Oxydation von Propylen oder Acrolein
JPS4924898B1 (pt) 1970-12-26 1974-06-26
DE2121123C3 (de) 1971-04-29 1980-06-12 Basf Ag, 6700 Ludwigshafen Verfahren zum Abtrennen von Wasser aus wäßrigen Lösungen von Acrylsäure durch azeotrope Destillation
BE786398A (fr) * 1971-07-21 1973-01-18 Basf Ag Procede de preparation de l'acide acrylique anhydre
IN151108B (pt) 1978-09-13 1983-02-19 Standard Oil Co
GB2146636B (en) 1983-08-11 1987-02-04 Nippon Catalytic Chem Ind Process for producing acrylic acid
US4999452A (en) 1989-05-15 1991-03-12 Union Carbide Chemicals And Plastics Company Inc. Process for producing acrylic ester
US5154800A (en) 1992-01-31 1992-10-13 Lloyd Berg Dehydration of acrylic acid by extractive distillation
DE4308987C2 (de) 1993-03-20 2003-01-09 Hansgrohe Ag Vorrichtung zum Betätigen eines Sanitär-Elements
DE19600955A1 (de) * 1996-01-12 1997-07-17 Basf Ag Verfahren zur Herstellung von Acrylsäure und deren Ester
DE19740253A1 (de) 1997-09-12 1999-03-18 Basf Ag Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten

Also Published As

Publication number Publication date
US6555707B1 (en) 2003-04-29
CN1295553A (zh) 2001-05-16
MY120799A (en) 2005-11-30
JP4410935B2 (ja) 2010-02-10
JP2002509903A (ja) 2002-04-02
DE59900932D1 (de) 2002-04-11
WO1999050220A1 (de) 1999-10-07
CN1133614C (zh) 2004-01-07
EP1066240A1 (de) 2001-01-10
EP1066240B1 (de) 2002-03-06
DE19814375A1 (de) 1999-10-07

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