BRPI0015808F1 - dispositivo de destilação à vácuo - Google Patents
dispositivo de destilação à vácuo Download PDFInfo
- Publication number
- BRPI0015808F1 BRPI0015808F1 BRC10015808A BRPI0015808A BRPI0015808F1 BR PI0015808 F1 BRPI0015808 F1 BR PI0015808F1 BR C10015808 A BRC10015808 A BR C10015808A BR PI0015808 A BRPI0015808 A BR PI0015808A BR PI0015808 F1 BRPI0015808 F1 BR PI0015808F1
- Authority
- BR
- Brazil
- Prior art keywords
- less
- pressure
- mbar
- solution
- boiling point
- Prior art date
Links
- 238000005292 vacuum distillation Methods 0.000 title 1
- 238000004821 distillation Methods 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 3
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 2
- -1 carboxylate ions Chemical class 0.000 abstract 2
- 150000007524 organic acids Chemical class 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/16—Vacuum
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
Abstract
dispositivo de destilação a vácuo é descrito um dispositivo de destilação a vácuo que compreende: um vaso (50, 60) dotado com uma camisa de aquecimento (51, 61), uma linha de alimentação na entrada (56, 66), uma linha de saída do resíduo (57, 67), e um sistema limpador; e, uma coluna de destilação (52, 62) provida com um recheio (53, 63), um dispositivo de resfriamento (54, 64), e uma linha de vácuo (55, 65), onde o vaso (50, 60) e a coluna de destilação (52, 62) são conectados e integrados num único dispositivo. tal dispositivo é usado principalmente na purificação de uma solução aquosa de um ácido orgânico tendo um ponto de ebulição na pressão atmosférica menor do que 450°c.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL1013682A NL1013682C2 (nl) | 1999-11-26 | 1999-11-26 | Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BRPI0015808E2 BRPI0015808E2 (pt) | 2014-02-25 |
| BRPI0015808F1 true BRPI0015808F1 (pt) | 2020-02-27 |
Family
ID=19770327
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0015808-9A BR0015808B1 (pt) | 1999-11-26 | 2000-11-27 | método para a purificação de uma solução aquosa de um ácido orgánico tendo um ponto de ebulição na pressão atmosférica menor do que 450 c, e, uso do método |
| BRC10015808A BRPI0015808F1 (pt) | 1999-11-26 | 2010-11-30 | dispositivo de destilação à vácuo |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0015808-9A BR0015808B1 (pt) | 1999-11-26 | 2000-11-27 | método para a purificação de uma solução aquosa de um ácido orgánico tendo um ponto de ebulição na pressão atmosférica menor do que 450 c, e, uso do método |
Country Status (11)
| Country | Link |
|---|---|
| US (4) | US7410556B1 (pt) |
| EP (1) | EP1232137B1 (pt) |
| JP (1) | JP5065561B2 (pt) |
| CN (1) | CN1191225C (pt) |
| AT (1) | ATE299487T1 (pt) |
| AU (1) | AU2557301A (pt) |
| BR (2) | BR0015808B1 (pt) |
| DE (1) | DE60021279T2 (pt) |
| ES (1) | ES2244494T3 (pt) |
| NL (1) | NL1013682C2 (pt) |
| WO (1) | WO2001038283A1 (pt) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL1013682C2 (nl) | 1999-11-26 | 2001-05-30 | Purac Biochem Bv | Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur. |
| ES2302753T5 (es) | 2000-09-15 | 2011-12-12 | Purac Biochem B.V. | Método para la purificación de un ácido alfa hidroxi a escala industrial. |
| DE10135716A1 (de) * | 2001-07-21 | 2003-02-06 | Basf Ag | Verbesserter Fallfilmverdampfer zur Auftrennung von Stoffgemischen |
| US6632966B2 (en) | 2001-08-24 | 2003-10-14 | Purac Biochem B.V. | Method for the preparation of lactic acid and calcium sulphate dihydrate |
| AT412951B (de) * | 2003-10-02 | 2005-09-26 | Vtu Engineering Planungs Und B | Dünnschichtverdampfer |
| WO2007063098A1 (en) * | 2005-11-30 | 2007-06-07 | Purac Biochem Bv | Aqueous potassium lactate solution |
| JP5280007B2 (ja) * | 2006-08-02 | 2013-09-04 | 株式会社クレハ | ヒドロキシカルボン酸の精製方法、環状エステルの製造方法およびポリヒドロキシカルボン酸の製造方法 |
| ES2436509T3 (es) | 2009-07-16 | 2014-01-02 | Purac Biochem Bv | Composición líquida de ácido láctico y método para su preparación |
| JP2013505727A (ja) | 2009-09-27 | 2013-02-21 | オーピーエックス バイオテクノロジーズ, インコーポレイテッド | 3−ヒドロキシプロピオン酸および他の生成物を生成するための方法 |
| US20110125118A1 (en) * | 2009-11-20 | 2011-05-26 | Opx Biotechnologies, Inc. | Production of an Organic Acid and/or Related Chemicals |
| WO2011095631A1 (en) | 2010-02-08 | 2011-08-11 | Purac Biochem Bv | Process for manufacturing lactic acid |
| DE102010026835B4 (de) * | 2010-07-11 | 2014-07-10 | Air Liquide Global E&C Solutions Germany Gmbh | Verfahren zur Destillation von temperaturempfindlichen Flüssigkeiten |
| EP2882843A4 (en) | 2012-08-10 | 2016-04-06 | Opx Biotechnologies Inc | MICRO-ORGANISMS AND METHOD FOR THE PRODUCTION OF FATTY ACIDS AND PRODUCTS DERIVED FROM FATTY ACIDS |
| EP2976141A4 (en) | 2013-03-15 | 2016-10-05 | Cargill Inc | FLASHING FOR PRODUCTION CLEANING AND RECOVERY |
| US20150057465A1 (en) | 2013-03-15 | 2015-02-26 | Opx Biotechnologies, Inc. | Control of growth-induction-production phases |
| PL2970086T3 (pl) | 2013-03-15 | 2019-04-30 | Cargill Inc | Odzyskiwanie kwasu 3-hydroksypropionowego |
| US11408013B2 (en) | 2013-07-19 | 2022-08-09 | Cargill, Incorporated | Microorganisms and methods for the production of fatty acids and fatty acid derived products |
| CN106795483A (zh) | 2013-07-19 | 2017-05-31 | 嘉吉公司 | 用于生产脂肪酸和脂肪酸衍生产物的微生物及方法 |
| JP5898733B2 (ja) * | 2013-10-17 | 2016-04-06 | 星野科学株式会社 | 水蒸気蒸留装置 |
| EP2977471A1 (en) | 2014-07-23 | 2016-01-27 | PURAC Biochem BV | Genetic modification of (S)-lactic acid producing thermophilic bacteria |
| PL3174988T3 (pl) | 2014-07-28 | 2023-01-02 | Purac Biochem Bv | Sposób wytwarzania kwasu mlekowego |
| EP2993228B1 (en) | 2014-09-02 | 2019-10-09 | Cargill, Incorporated | Production of fatty acid esters |
| WO2016043264A1 (ja) | 2014-09-17 | 2016-03-24 | 株式会社日本触媒 | 乳酸を含む蒸気組成物の製造方法 |
| BE1024147B1 (fr) | 2016-05-11 | 2017-11-22 | Galactic S.A. | Procede de purification d'une solution aqueuse d'acide lactique |
| WO2018144701A2 (en) | 2017-02-02 | 2018-08-09 | Cargill Incorporated | Genetically modified cells that produce c6-c10 fatty acid derivatives |
| WO2021139894A1 (en) | 2020-01-10 | 2021-07-15 | BluCon Biotech GmbH | Extreme thermophilic bacteria of the genus caldicellulosiruptor suitable for the conversion of cellulosic and starchy biomass |
| CA3136780A1 (en) | 2019-04-18 | 2020-10-22 | BluCon Biotech GmbH | Extreme thermophilic bacteria of the genus caldicellulosiruptor suitable for the conversion of cellulosic and starchy biomass |
| WO2021139895A1 (en) | 2020-01-10 | 2021-07-15 | BluCon Biotech GmbH | Methods of producing lactic acid from unmodified starch |
| KR102721328B1 (ko) * | 2020-11-24 | 2024-10-24 | 주식회사 엘지화학 | 아크릴산의 제조 공정 |
| KR102690123B1 (ko) * | 2020-11-24 | 2024-07-30 | 주식회사 엘지화학 | 아크릴산의 제조 공정 |
| AU2021428925B2 (en) * | 2021-02-22 | 2024-06-13 | Polywin Pte. Ltd. | Method and device for the production of lactide |
| CN115501829B (zh) * | 2021-06-22 | 2025-07-25 | 上海浦景化工技术股份有限公司 | 适用于制备窄分子量分布聚乙醇酸的装置及其制备方法 |
| JP7720470B2 (ja) | 2021-07-13 | 2025-08-07 | プリシジョン アナライザー カンパニー エル.ピー. | 部分蒸留による石油試料の蒸留特性を決定するためのシステムおよび方法 |
| MX2024001234A (es) | 2021-07-30 | 2024-02-13 | Purac Biochem Bv | Procedimiento para fabricar acido lactico. |
| CN114573448B (zh) * | 2022-01-29 | 2023-12-15 | 安徽丰原发酵技术工程研究有限公司 | 一种提取乳酸的方法 |
| US11793785B2 (en) * | 2022-10-05 | 2023-10-24 | Vapor Oil Technology LLC | Thin film oxidation of crystallized cannabis products |
| US12246050B2 (en) | 2022-10-05 | 2025-03-11 | Vapor Oil Technology LLC | Post extraction purification of terpenes |
Family Cites Families (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1594843A (en) * | 1921-08-19 | 1926-08-03 | Du Pont | Purification of lactic acid |
| US2088624A (en) * | 1930-07-18 | 1937-08-03 | Tschudy Frederick | Process of and apparatus for treating materials |
| US2013096A (en) * | 1933-04-13 | 1935-09-03 | Du Pont | Purification of lactic acid |
| BE518997A (pt) * | 1952-04-24 | |||
| US2885436A (en) * | 1957-02-26 | 1959-05-05 | Danske Sukkerfab | Process for the purification of lactic acid |
| DE1159901B (de) * | 1959-09-16 | 1963-12-27 | Leybold Hochvakuum Anlagen | Vorrichtung zur fraktionierenden Destillation unter Vakuum |
| FR1290212A (fr) | 1961-02-27 | 1962-04-13 | Melle Usines Sa | Procédé de décoloration et de purification de solutions impures d'acides organiques |
| AT274743B (de) * | 1967-09-28 | 1969-09-25 | Krems Chemie Gmbh | Verfahren und Vorrichtung zur kontinuierlichen Fraktionierung von Tallöl oder andern organischen Mehrstoffgemischen |
| BE759328A (fr) * | 1969-11-24 | 1971-05-24 | Rhone Poulenc Sa | Procede de separation de melanges d'acides |
| CS181054B1 (en) * | 1974-04-10 | 1978-02-28 | Alexander Tkac | Equipment adapted for multistage vacuum and molecular distillation with wiped off film with single evaporating body |
| FR2394512A1 (fr) * | 1977-06-14 | 1979-01-12 | Rhone Poulenc Ind | Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle |
| CS229404B1 (en) * | 1981-06-22 | 1984-06-18 | Alexander Prof Drsc Tkac | Bloc short travel evaporator with a wiped film |
| US4601790A (en) * | 1982-07-23 | 1986-07-22 | Hermann Stage | Process for deodorizing and/or physical refining of cocoa butter and cocoa butter substitutes |
| DE3339051A1 (de) * | 1983-10-28 | 1985-05-09 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur verbesserten destillativen aufarbeitung von glycerin |
| JPH0789942B2 (ja) * | 1987-09-30 | 1995-10-04 | 株式会社島津製作所 | 乳酸の精製法 |
| US4867849A (en) * | 1988-07-25 | 1989-09-19 | Cova Dario R | Purification of alkyl glyoxylate |
| US5171407A (en) * | 1989-09-22 | 1992-12-15 | Sulzer Brothers Limited | Distillation plant for producing hydrogen peroxide |
| US5051152A (en) * | 1989-09-26 | 1991-09-24 | Air Products And Chemicals, Inc. | Preparation of urethane prepolymers having low levels of residual toluene diisocyanate |
| US5202001A (en) * | 1989-09-26 | 1993-04-13 | Air Products And Chemicals, Inc. | Preparation of urethane prepolymers having low levels of residual toluene diisocyanate |
| US6326458B1 (en) * | 1992-01-24 | 2001-12-04 | Cargill, Inc. | Continuous process for the manufacture of lactide and lactide polymers |
| US5420304A (en) * | 1992-03-19 | 1995-05-30 | Biopak Technology, Ltd. | Method to produce cyclic esters |
| US5208342A (en) | 1992-03-30 | 1993-05-04 | Hoechst Celanese Corporation | Conversion of pyridine-2,3-dicarboxylic acid esters to cyclic anhydrides |
| US5334130A (en) * | 1992-05-13 | 1994-08-02 | Savant Instruments, Inc. | Centrifugal vacuum concentration with holder assembly |
| US5303769A (en) * | 1992-09-25 | 1994-04-19 | The M. W. Kellogg Company | Integrated thermosiphon heat exchanger apparatus |
| DE4239117A1 (de) * | 1992-11-20 | 1994-05-26 | Wacker Chemie Gmbh | Verfahren zur Isolierung von reinem Diketen unter Rückgewinnung von Wertstoffen |
| GB9306409D0 (en) * | 1993-03-26 | 1993-05-19 | Bp Chem Int Ltd | Process |
| FR2713878B1 (fr) * | 1993-12-07 | 1996-03-08 | Garidel Jean Paul | Machine pour assembler des composants sur un support, en phase vapeur, auto-stabilisée thermiquement. |
| BE1008099A3 (fr) * | 1994-03-04 | 1996-01-16 | Brussels Biotech Sa | Production semi-continue de polylactides par ouverture de cycle lactides obtenus a partir de derives d'acide lactique. |
| US5582692A (en) * | 1994-10-07 | 1996-12-10 | Artisan Industries, Inc. | Method for the purification of vitamin E |
| US6254734B1 (en) * | 1995-03-14 | 2001-07-03 | Hugo H Sephton | Barometric evaporation process and evaporator |
| DE19522377A1 (de) * | 1995-06-22 | 1997-01-02 | Basf Ag | Verfahren zur Gewinnung von Hydroxycarbonsäuren aus wäßrigen Lösungen |
| US5660691A (en) * | 1995-11-13 | 1997-08-26 | Eastman Chemical Company | Process for the production of tocotrienol/tocopherol blend concentrates |
| BE1011197A3 (fr) * | 1997-06-06 | 1999-06-01 | Brussels Biotech En Abrege Bb | Procede de purification d'acide lactique. |
| DE19733903A1 (de) * | 1997-08-05 | 1999-02-11 | Basf Ag | Verfahren zur Gewinnung von Hydroxxpivalinsäureneopentylglykolester (HPN) |
| US6706898B2 (en) * | 1998-01-29 | 2004-03-16 | Archer-Daniels-Midland Company | Methods for separating a tocopherol from a tocopherol-containing mixture |
| WO2000056693A1 (en) * | 1999-03-22 | 2000-09-28 | Purac Biochem B.V. | Method of industrial-scale purification of lactic acid |
| NL1013682C2 (nl) | 1999-11-26 | 2001-05-30 | Purac Biochem Bv | Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur. |
| US6509179B1 (en) * | 2000-10-12 | 2003-01-21 | Barbara I. Veldhuis-Stribos | Continuous process for preparing lactic acid |
| US6982026B2 (en) * | 2001-03-15 | 2006-01-03 | Tate & Lyle Ingredients Americas, Inc. | Azeotropic distillation process for producing organic acids or organic acid amides |
| AT412951B (de) * | 2003-10-02 | 2005-09-26 | Vtu Engineering Planungs Und B | Dünnschichtverdampfer |
-
1999
- 1999-11-26 NL NL1013682A patent/NL1013682C2/nl not_active IP Right Cessation
-
2000
- 2000-11-27 US US10/130,990 patent/US7410556B1/en not_active Expired - Lifetime
- 2000-11-27 AU AU25573/01A patent/AU2557301A/en not_active Abandoned
- 2000-11-27 CN CNB008162980A patent/CN1191225C/zh not_active Expired - Lifetime
- 2000-11-27 BR BRPI0015808-9A patent/BR0015808B1/pt not_active IP Right Cessation
- 2000-11-27 EP EP00989029A patent/EP1232137B1/en not_active Expired - Lifetime
- 2000-11-27 AT AT00989029T patent/ATE299487T1/de not_active IP Right Cessation
- 2000-11-27 ES ES00989029T patent/ES2244494T3/es not_active Expired - Lifetime
- 2000-11-27 DE DE60021279T patent/DE60021279T2/de not_active Expired - Lifetime
- 2000-11-27 JP JP2001539840A patent/JP5065561B2/ja not_active Expired - Fee Related
- 2000-11-27 WO PCT/NL2000/000865 patent/WO2001038283A1/en not_active Ceased
-
2007
- 2007-07-19 US US11/780,388 patent/US7875153B2/en not_active Expired - Fee Related
-
2008
- 2008-04-16 US US12/104,302 patent/US7879197B2/en not_active Expired - Fee Related
-
2010
- 2010-11-30 BR BRC10015808A patent/BRPI0015808F1/pt unknown
- 2010-12-20 US US12/973,775 patent/US8192589B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1399623A (zh) | 2003-02-26 |
| JP2003514885A (ja) | 2003-04-22 |
| US7879197B2 (en) | 2011-02-01 |
| WO2001038283A1 (en) | 2001-05-31 |
| BR0015808A (pt) | 2002-08-06 |
| EP1232137B1 (en) | 2005-07-13 |
| US7875153B2 (en) | 2011-01-25 |
| BR0015808B1 (pt) | 2011-05-03 |
| US8192589B2 (en) | 2012-06-05 |
| EP1232137A1 (en) | 2002-08-21 |
| US20110089016A1 (en) | 2011-04-21 |
| NL1013682C2 (nl) | 2001-05-30 |
| US7410556B1 (en) | 2008-08-12 |
| US20080308402A1 (en) | 2008-12-18 |
| ATE299487T1 (de) | 2005-07-15 |
| ES2244494T3 (es) | 2005-12-16 |
| BRPI0015808E2 (pt) | 2014-02-25 |
| DE60021279D1 (de) | 2005-08-18 |
| JP5065561B2 (ja) | 2012-11-07 |
| CN1191225C (zh) | 2005-03-02 |
| AU2557301A (en) | 2001-06-04 |
| DE60021279T2 (de) | 2006-05-18 |
| US20080257710A1 (en) | 2008-10-23 |
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