BRPI0416795A - recuperação de fitonutrientes a partir de óleos - Google Patents

recuperação de fitonutrientes a partir de óleos

Info

Publication number
BRPI0416795A
BRPI0416795A BRPI0416795-3A BRPI0416795A BRPI0416795A BR PI0416795 A BRPI0416795 A BR PI0416795A BR PI0416795 A BRPI0416795 A BR PI0416795A BR PI0416795 A BRPI0416795 A BR PI0416795A
Authority
BR
Brazil
Prior art keywords
oils
tocotrienols
tocopherols
carotenoids
sterols
Prior art date
Application number
BRPI0416795-3A
Other languages
English (en)
Inventor
David Ho Sue San
Original Assignee
Carotech Inc
David Ho Sue San
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Carotech Inc, David Ho Sue San filed Critical Carotech Inc
Publication of BRPI0416795A publication Critical patent/BRPI0416795A/pt
Publication of BRPI0416795B1 publication Critical patent/BRPI0416795B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
    • C07C403/24—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by six-membered non-aromatic rings, e.g. beta-carotene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C07D311/70—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with two hydrocarbon radicals attached in position 2 and elements other than carbon and hydrogen in position 6
    • C07D311/72—3,4-Dihydro derivatives having in position 2 at least one methyl radical and in position 6 one oxygen atom, e.g. tocopherols
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Pyrane Compounds (AREA)
  • Fats And Perfumes (AREA)
  • Steroid Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

"RECUPERAçãO DE FITONUTRIENTES A PARTIR DE óLEOS". A presente invenção se refere a um processo aperfeiçoado e integrado para a extração e purificação de tocotrienóis ou tocoferóis, carotenóides e esteróis a partir de óleos vegetais e outros óleos comestíveis. ácidos graxos nos óleos vegetais são submetidos à esterificação alcoólica para formar camada rica em éster que inclui ésteres alquílicos de ácido graxo, carotenóides, tocotrienóis ou tocoferóis, e esteróis. As vantagens desse processo são que os tocotrienóis ou tocoferóis, carotenóides e esteróis são produzidos eficientemente sem qualquer decomposição ou degradação substancial desses fitonutrientes.
BRPI0416795-3B1A 2003-11-19 2004-11-18 Processo integrado para recuperação de fitonutrientes a partir de óleos BRPI0416795B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
MYPI20034440A MY173044A (en) 2003-11-19 2003-11-19 Recovery of phytonutriens from oils
MYPI20034440 2003-11-19
PCT/US2004/038774 WO2005051294A2 (en) 2003-11-19 2004-11-18 Recovery of phytonutrients from oils

Publications (2)

Publication Number Publication Date
BRPI0416795A true BRPI0416795A (pt) 2007-03-06
BRPI0416795B1 BRPI0416795B1 (pt) 2014-09-16

Family

ID=34632192

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0416795-3B1A BRPI0416795B1 (pt) 2003-11-19 2004-11-18 Processo integrado para recuperação de fitonutrientes a partir de óleos

Country Status (8)

Country Link
US (1) US7544822B2 (pt)
EP (1) EP1689353B1 (pt)
JP (1) JP5327730B2 (pt)
CN (1) CN1964960B (pt)
BR (1) BRPI0416795B1 (pt)
EC (1) ECSP066650A (pt)
MY (1) MY173044A (pt)
WO (1) WO2005051294A2 (pt)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070124992A1 (en) * 2005-12-01 2007-06-07 Her Majesty In Right Of Canada Methods for concentration and extraction of lubricity compounds and biologically active fractions from naturally derived fats, oils and greases
US7850745B2 (en) 2005-12-01 2010-12-14 Her Majesty In Right Of Canada As Represented By The Minister Of Agriculture And Agri-Food Canada Method for concentration and extraction of lubricity compounds from vegetable and animal oils
US20070151146A1 (en) * 2005-12-29 2007-07-05 Inmok Lee Processes of Producing Biodiesel and Biodiesel Produced Therefrom
KR101481197B1 (ko) 2007-05-24 2015-01-09 로더스 크로클란 비.브이. 토코페롤 및 토코트리에놀을 함유하는 조성물의 제조방법
JP4969370B2 (ja) * 2007-08-29 2012-07-04 Ｊｘ日鉱日石エネルギー株式会社 カロテノイドの製造方法
US8158185B2 (en) 2007-10-04 2012-04-17 Bunge Oils, Inc. Controlled viscosity oil composition and method of making
CA2739311A1 (en) * 2008-10-03 2010-04-08 Dag Arntsen Process for removal of contaminations from organic oils
WO2010051277A1 (en) * 2008-10-28 2010-05-06 Edison Pharmaceuticals, Inc. Process for the production of alpha-tocotrienol and derivatives
DE102011117510A1 (de) 2010-11-03 2012-05-03 Verbio Vereinigte Bioenergie Ag Verfahren zur Gewinnung von Phytosterolen und/oder Tocopherolen aus Rückständen einer Destillation von Estern pflanzlicher Öle, vorzugsweise aus Destillationsrückständen aus einer Umesterung von pflanzlichen Ölen
WO2013070058A1 (en) * 2011-11-11 2013-05-16 Malaysian Palm Oil Board A process for extracting phytonutrients in palm oil
US9039898B2 (en) * 2011-11-15 2015-05-26 Engineering Research Associates, Inc. Method for separating components in natural oil
US8937191B2 (en) * 2012-12-20 2015-01-20 Orochem Technologies, Inc. Recovery of highly pure alpha-tocotrienol from crude palm oil extract
US9163198B2 (en) 2014-01-17 2015-10-20 Orochem Technologies, Inc. Process for purification of EPA (eicosapentanoic acid) ethyl ester from fish oil
SG11201606162XA (en) 2014-02-11 2016-08-30 Evonik Membrane Extraction Technology Ltd Method for producing vitamine e-enriched, especially tocotrienol-enriched, compositions from natural oils
WO2015179131A1 (en) * 2014-05-21 2015-11-26 Elevance Renewable Sciences, Inc. Low-color ester compositions and methods of making and using the same
SG11201609983VA (en) * 2014-05-29 2016-12-29 Malaysian Palm Oil Board Mpob A process to enhance the concentration of tocols from palm oil
MY193786A (en) * 2015-01-12 2022-10-27 Ho Sue San David Recovery of tocopherols/tocotrienols, carotenoids, glycerols, sterols and fatty acid esters from crude vegetable oil and the process thereof
MY176376A (en) * 2015-02-06 2020-08-04 Ho Sue San David Recovery of tocopherols/tocotrienols, glycerine, sterols and fatty acid esters from vegetable oil distillate and the process thereof
JP6548087B2 (ja) 2015-05-18 2019-07-24 国立大学法人東北大学 ビタミンｅ類の選択的な分離方法
CN106632209A (zh) * 2015-11-03 2017-05-10 浙江医药股份有限公司新昌制药厂 一种高纯度生育酚和生育三烯酚浓缩混合物的制备方法
JP7117241B2 (ja) 2015-12-16 2022-08-12 ピーティーシー セラピューティクス， インコーポレイテッド 混合されたトコール組成物からアルファ－トコトリエノールを富化するための改良された方法
ES2959817T3 (es) * 2016-12-16 2024-02-28 Praj Industries Ltd Procedimiento para la preparación de tocoles y escualeno
JP7106075B2 (ja) 2017-02-17 2022-07-26 ファイトケミカルプロダクツ株式会社 ビタミンｅ類の製造方法およびビタミンｅ類製造装置
CN114450386A (zh) * 2019-09-27 2022-05-06 巴斯夫欧洲公司 用于生产甾醇和/或生育酚并回收副产物的方法
EP4034619A1 (en) 2019-09-27 2022-08-03 Basf Se Process for the production and purification of sterols
US20240209280A1 (en) * 2021-04-22 2024-06-27 Desmet Belgium Novel process and equipment for solvent fractionation
WO2025172861A2 (en) 2024-02-14 2025-08-21 Biosergen As Compositions of a therapeutic polyene macrolide and methods of their use

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8729232D0 (en) 1987-12-15 1988-01-27 Palm Oil Research Inst Of Mala Recovery of carotenoids tocopherols tocotrienols & sterols from esterified palm oil
US5157132A (en) 1990-05-18 1992-10-20 Carotech Associates Integrated process for recovery of carotenoids and tocotrienols from oil
US5660691A (en) * 1995-11-13 1997-08-26 Eastman Chemical Company Process for the production of tocotrienol/tocopherol blend concentrates
EP1051412B1 (en) * 1998-01-29 2003-09-24 Eastman Chemical Company Methods for separating a tocotrienol from a tocol-containing mixture and compositions thereof
ES2152856B1 (es) * 1998-10-08 2001-11-16 Biocaps S A Procedimiento para el aislamiento y extraccion de tocoferoles y otros compuestos a partir de subproductos obtenidos en la refinacion de aceites vegetales.
MY138186A (en) * 2000-12-14 2009-05-29 Supervitamins Sdn Bhd Recovery of minor components and refining of vegetable oils and fats

Also Published As

Publication number Publication date
JP2007521382A (ja) 2007-08-02
WO2005051294A2 (en) 2005-06-09
EP1689353B1 (en) 2013-01-09
JP5327730B2 (ja) 2013-10-30
US7544822B2 (en) 2009-06-09
US20070238886A1 (en) 2007-10-11
CN1964960B (zh) 2013-05-29
CN1964960A (zh) 2007-05-16
EP1689353A4 (en) 2009-04-15
WO2005051294A3 (en) 2006-10-26
MY173044A (en) 2019-12-20
HK1103739A1 (en) 2007-12-28
EP1689353A2 (en) 2006-08-16
ECSP066650A (pt) 2006-10-25
BRPI0416795B1 (pt) 2014-09-16

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Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B15K Others concerning applications: alteration of classification

Free format text: ALTERACAO DA CLASSIFICACAO DE: C07D 311/72 PARA: C07D 311/72; B01D3/12; C07J9/00; C07C403/2

Ipc: C07D 311/72 (2006.01), B01D 3/12 (2006.01), C07J 9

B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 18/11/2004, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 12A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2386 DE 27-09-2016 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.