BRPI0417052A - processo para a preparação de compostos - Google Patents

processo para a preparação de compostos

Info

Publication number
BRPI0417052A
BRPI0417052A BRPI0417052-0A BRPI0417052A BRPI0417052A BR PI0417052 A BRPI0417052 A BR PI0417052A BR PI0417052 A BRPI0417052 A BR PI0417052A BR PI0417052 A BRPI0417052 A BR PI0417052A
Authority
BR
Brazil
Prior art keywords
formula
thio
phenyl
uracils
compounds
Prior art date
Application number
BRPI0417052-0A
Other languages
English (en)
Inventor
Gerhard Hamprecht
Michael Punl
Bernd Wolf
Michael Keil
Robert Reinhard
Werner Seitz
Guido Mayer
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of BRPI0417052A publication Critical patent/BRPI0417052A/pt
Publication of BRPI0417052B1 publication Critical patent/BRPI0417052B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/52—Two oxygen atoms
    • C07D239/54—Two oxygen atoms as doubly bound oxygen atoms or as unsubstituted hydroxy radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/56—One oxygen atom and one sulfur atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

"PROCESSO PARA A PREPARAçãO DE COMPOSTOS". A invenção diz respeito a um método para a produção de 3-fenil(tio)uracilas ou 3-fenilditiouracilas de fórmula (I), mediante a reação de um feniliso(tio)cianato de fórmula (II) com uma enamina de fórmula (III) e opcionalmente a reação em uma etapa adicional da 3-fenil(tio)uracila ou 3fenilditiouracila de fórmula (I) com R¬ 1¬ = R¬ 1a¬, se R¬ 1¬ for hidrogênio, com um agente de aminação de fórmula (IV) para dar 3-fenil(tio)uracilas ou 3-fenilditiouracilas de fórmula (I) com R¬ 1¬ = amina, em que as variáveis R¬ 1¬, R¬ 1a¬, R¬ 2¬, R¬ 3¬, R¬ 4¬, X¬ 1¬, X¬ 2¬, X¬ 3¬, Ar e A L1 são definidas de acordo com a reivindicação 1.
BRPI0417052-0A 2003-12-03 2004-12-01 Processos para a preparação de 3-fenil(tio)uracilas e 3-fenilditiouracilas BRPI0417052B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10356474.8 2003-12-03
DE10356474 2003-12-03
PCT/EP2004/013615 WO2005054208A1 (de) 2003-12-03 2004-12-01 Verfahren zur herstellung von 3-phenyl(thio)uracilen und 3-phenyldithiouracilen

Publications (2)

Publication Number Publication Date
BRPI0417052A true BRPI0417052A (pt) 2007-02-06
BRPI0417052B1 BRPI0417052B1 (pt) 2014-02-25

Family

ID=34638289

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0417052-0A BRPI0417052B1 (pt) 2003-12-03 2004-12-01 Processos para a preparação de 3-fenil(tio)uracilas e 3-fenilditiouracilas

Country Status (12)

Country Link
US (1) US7737275B2 (pt)
EP (1) EP1692115B1 (pt)
JP (1) JP4528306B2 (pt)
KR (1) KR101135263B1 (pt)
CN (1) CN100558714C (pt)
AT (1) ATE381547T1 (pt)
BR (1) BRPI0417052B1 (pt)
DE (1) DE502004005772D1 (pt)
DK (1) DK1692115T3 (pt)
ES (1) ES2295957T3 (pt)
IL (1) IL175713A (pt)
WO (1) WO2005054208A1 (pt)

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US8357695B2 (en) * 2006-10-13 2013-01-22 Basf Se Hydrates of 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1-(2H)-pyrimidinyl]-4-fluoro-N-[[methyl(1-methylethyl)amino]sulfonyl]benzamide
US8653002B2 (en) 2009-08-27 2014-02-18 Basf Se Aqueous suspension concentrate formulations containing saflufenacil
CN102480963B (zh) 2009-08-27 2014-02-26 巴斯夫欧洲公司 包含苯嘧磺草胺和草甘膦的含水浓缩配制剂
US8481723B2 (en) 2009-11-13 2013-07-09 Basf Se 3-(3,4-dihydro-2H-benzo [1,4]oxazin-6-yl)-1H-Pyrimidin-2,4-dione compounds as herbicides
BR112012013151B1 (pt) 2009-12-09 2017-07-25 Basf Se Formulation of liquid suspension concentrate for plant protection, use of concentration of liquid suspension for plant protection and undesired vegetation control method
CN102651971B (zh) 2009-12-09 2015-05-13 巴斯夫欧洲公司 含有苯嘧磺草胺和草甘膦的液体悬浮浓缩物配制剂
EP2538786A2 (de) 2010-02-26 2013-01-02 Bayer Intellectual Property GmbH Herbizide zusammensetzung enthaltend die hydrate von saflufenacil und glyphosate oder glufosinate
CN103130727B (zh) * 2013-02-27 2015-07-08 江苏省农用激素工程技术研究中心有限公司 苯嘧磺草胺中间体的制备方法
WO2015091642A1 (en) 2013-12-19 2015-06-25 BASF Agro B.V. Dilute aqueous compositions of saflufenacil
WO2016053107A1 (en) * 2014-10-03 2016-04-07 Synaffix B.V. Sulfamide linker, conjugates thereof, and methods of preparation
AU2016208065B2 (en) 2015-01-15 2019-08-22 Basf Se Herbicidal combination comprising saflufenacil and glufosinate
CA2973915C (en) 2015-01-22 2024-01-16 BASF Agro B.V. Ternary herbicidal combination comprising saflufenacil
HUE044213T2 (hu) 2015-07-10 2019-10-28 Basf Agro Bv Cinmetilint és petoxamidot tartalmazó herbicid készítmény
JP6875368B2 (ja) 2015-07-10 2021-05-26 ビーエーエスエフ アグロ ベー．ブイ． シンメチリン及びアセトクロール又はプレチラクロールを含む除草剤組成物
US11219212B2 (en) 2015-07-10 2022-01-11 BASF Agro B.V. Herbicidal composition comprising cinmethylin and imazamox
EA201890268A1 (ru) 2015-07-10 2018-07-31 Басф Агро Б.В. Гербицидная композиция, которая содержит цинметилин и диметенамид
CN107846891B (zh) 2015-07-10 2024-02-20 巴斯夫农业公司 包含环庚草醚和特异性色素合成抑制剂的除草组合物
JP2018524359A (ja) 2015-07-10 2018-08-30 ビーエーエスエフ アグロ ベー．ブイ． シンメチリン及び特定のキノリンカルボン酸を含む除草剤組成物
US11219215B2 (en) 2015-07-10 2022-01-11 BASF Agro B.V. Herbicidal composition comprising cinmethylin and specific inhibitors of protoporphyrinogen oxidase
EA201890259A1 (ru) 2015-07-10 2018-07-31 Басф Агро Б.В. Способ борьбы с устойчивыми или толерантными к гербицидам сорняками
US20180184658A1 (en) 2015-07-10 2018-07-05 BASF Agro B.V. Herbicidal composition comprising cinmethylin and saflufenacil
PL3319437T3 (pl) 2015-07-10 2020-03-31 BASF Agro B.V. Kompozycja chwastobójcza zawierająca cynmetylinę i piroksasulfon
CR20180120A (es) 2015-07-24 2018-08-13 Basf Se Compuestos de piridina útiles para combatir hongos fitopatógenos
US11317628B2 (en) 2015-09-03 2022-05-03 BASF Agro B.V. Microparticle compositions comprising saflufenacil
EP3464261B1 (en) 2016-05-24 2021-07-07 Basf Se Herbicidal uracilpyrid
WO2018019845A1 (en) 2016-07-29 2018-02-01 Basf Se Method for controlling ppo resistant weeds
KR20180081275A (ko) * 2017-01-06 2018-07-16 주식회사 팜한농 3-아릴우라실 화합물의 제조 방법
AU2019391253A1 (en) * 2018-12-04 2021-06-03 Basf Se Process for preparation of 5-bromo-1,3-dichloro-2-fluoro-benzene
PY2047858A (es) 2019-08-26 2021-06-17 Adama Agan Ltd Novedosas composiciones líquidas solubles de saflufenacil, metodo de preparación y uso de estas
AU2021230070A1 (en) 2020-03-06 2022-09-22 Basf Se Herbicidal phenyluracils
AR124927A1 (es) 2021-02-24 2023-05-17 Adama Agan Ltd Composiciones herbicidas que comprenden inhibidores de acetolactato sintasa a base de imidazolinona y usos de los mismos
AU2022230103A1 (en) 2021-03-04 2023-10-05 Adama Agan Ltd. Solid forms of saflufenacil-sodium and saflufenacil-potassium, process of preparation and use thereof
WO2022201155A1 (en) 2021-03-26 2022-09-29 Adama Agan Ltd. Preparation of 2-chloro-4-fluoro-5-nitrobenzoic acid
US20250115560A1 (en) 2021-08-09 2025-04-10 Adama Agan Ltd A new process of saflufenacil production using novel intermediates
CA3227501A1 (en) 2021-08-30 2023-03-09 Rahul Kaduskar Crystalline forms of methyl 2-[2-[2-bromo-4-fluoro-5-[3-methyl-2,6-dioxo-4-(trifluoromethyl)pyrimidin-1-yl]phenoxy]phenoxy]-2-methoxy-acetate
WO2023030935A1 (en) 2021-08-31 2023-03-09 Basf Se Method for controlling ppo-i resistant weeds
WO2023030934A1 (en) 2021-08-31 2023-03-09 Basf Se Herbicidal composition comprising phenyluracils
US20250313536A1 (en) 2022-05-30 2025-10-09 BASF Agro B.V. Process for recovering saflufenacil from process streams
US20250248394A1 (en) 2022-07-13 2025-08-07 BASF Agro B.V. Herbicidal eode formulation comprising several active ingredients
WO2024042134A1 (en) 2022-08-26 2024-02-29 BASF Agro B.V. Aqueous herbicide formulations
IL319021A (en) 2022-08-31 2025-04-01 Adama Agan Ltd Preparation of 2-chloro-4-fluoro-5-nitrobenzoic acid
AR131474A1 (es) 2022-12-22 2025-03-26 Basf Agro Bv Métodos de control de plantas indeseables con herbicidas ppo y combinaciones en plantas de cultivo tolerantes a herbicidas
EP4687448A1 (en) 2023-03-29 2026-02-11 BASF Agro B.V. Method for controlling parasitic weeds (orobanche) in protoporphyrinogen oxidase (ppo)-inhibitor tolerant sunflower crop
CN121039108A (zh) 2023-03-30 2025-11-28 安道麦阿甘有限公司 用于制备磺酰胺衍生物的方法
WO2025120633A1 (en) 2023-12-06 2025-06-12 Adama Agan Ltd. Herbicidal mixtures comprising saflufenacil and fluroxypyr
WO2025124942A1 (en) 2023-12-12 2025-06-19 BASF Agro B.V. Process for preparing a saflufenacil intermediate
WO2025181801A1 (en) 2024-02-26 2025-09-04 Adama Agan Ltd. An herbicidal formulation comprising saflufenacil and fluroxypyr

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US4309209A (en) 1977-08-15 1982-01-05 Chevron Research Herbicidal method and composition
US6207830B1 (en) 1987-09-23 2001-03-27 Syngenta Crop Protection, Inc. Process for the production of 3-aryl-uracils
US4943309A (en) 1988-09-06 1990-07-24 Uniroyal Chemical Company, Inc. Method of defoleating cotton plants employing 3-carbonylphenyl uracil derivatives
US5169430A (en) * 1991-08-09 1992-12-08 Uniroyal Chemical Company, Inc. Benzenesulfonamide derivatives and methods for their production
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EP0831091A3 (en) * 1996-09-23 1998-04-15 Novartis AG Process for the production of 3-aryl-uracils
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Also Published As

Publication number Publication date
JP4528306B2 (ja) 2010-08-18
WO2005054208A1 (de) 2005-06-16
JP2007513110A (ja) 2007-05-24
EP1692115A1 (de) 2006-08-23
ATE381547T1 (de) 2008-01-15
KR20060120187A (ko) 2006-11-24
ES2295957T3 (es) 2008-04-16
US20060293520A1 (en) 2006-12-28
DK1692115T3 (da) 2008-03-25
BRPI0417052B1 (pt) 2014-02-25
KR101135263B1 (ko) 2012-04-12
US7737275B2 (en) 2010-06-15
IL175713A0 (en) 2006-09-05
EP1692115B1 (de) 2007-12-19
CN1890222A (zh) 2007-01-03
DE502004005772D1 (de) 2008-01-31
IL175713A (en) 2010-12-30
CN100558714C (zh) 2009-11-11

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Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B25D Requested change of name of applicant approved

Owner name: BASF SE (DE)

B15K Others concerning applications: alteration of classification

Free format text: "ALTERADA A CLASSIFICACAO DE: C07D 239/56

Ipc: C07D 239/56 (2006.01), C07D 239/54 (2006.01)

Free format text: ALTERADA A CLASSIFICACAO DE: C07D 239/56; C07D 239/54 PARA: C07D 239/56; C07D 239/54; A01N43/48

Ipc: C07D 239/56 (2006.01), C07D 239/54 (2006.01)

B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 01/12/2004, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 20A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2803 DE 24-09-2024 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.