BRPI0820774A2 - Método para produzir lactídeos. - Google Patents
Método para produzir lactídeos.Info
- Publication number
- BRPI0820774A2 BRPI0820774A2 BRPI0820774-7A BRPI0820774A BRPI0820774A2 BR PI0820774 A2 BRPI0820774 A2 BR PI0820774A2 BR PI0820774 A BRPI0820774 A BR PI0820774A BR PI0820774 A2 BRPI0820774 A2 BR PI0820774A2
- Authority
- BR
- Brazil
- Prior art keywords
- lactide
- catalyst
- lactic acid
- metal
- lactides
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 abstract 4
- JJTUDXZGHPGLLC-UHFFFAOYSA-N lactide Chemical compound CC1OC(=O)C(C)OC1=O JJTUDXZGHPGLLC-UHFFFAOYSA-N 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 235000014655 lactic acid Nutrition 0.000 abstract 2
- 239000004310 lactic acid Substances 0.000 abstract 2
- 229910052751 metal Inorganic materials 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052718 tin Inorganic materials 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
- C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Catalysts (AREA)
- Polyesters Or Polycarbonates (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07024679A EP2072508A1 (fr) | 2007-12-19 | 2007-12-19 | Procédé d'obtention de lactide |
| PCT/EP2008/067994 WO2009077615A1 (fr) | 2007-12-19 | 2008-12-19 | Procédé d'obtention de lactide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BRPI0820774A2 true BRPI0820774A2 (pt) | 2015-06-16 |
| BRPI0820774B1 BRPI0820774B1 (pt) | 2016-12-13 |
Family
ID=39386345
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0820774A BRPI0820774B1 (pt) | 2007-12-19 | 2008-12-19 | método para produzir lactídeos. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US8592609B2 (pt) |
| EP (2) | EP2072508A1 (pt) |
| JP (1) | JP5179595B2 (pt) |
| CN (1) | CN101903370B (pt) |
| AT (1) | ATE512956T1 (pt) |
| AU (1) | AU2008337402B2 (pt) |
| BR (1) | BRPI0820774B1 (pt) |
| ES (1) | ES2365589T3 (pt) |
| WO (1) | WO2009077615A1 (pt) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8900834B2 (en) | 2010-10-28 | 2014-12-02 | Total Research & Technology Feluy S.A. | Process for polylactic acid production using monascus |
| WO2013039038A1 (ja) * | 2011-09-12 | 2013-03-21 | 株式会社クレハ | グリコリドの製造方法 |
| EP2725019B1 (de) | 2012-10-26 | 2015-04-08 | Uhde Inventa-Fischer GmbH | Verfahren zur Herstellung cyclischer Diester, insbesondere Dilactid |
| CN103193759B (zh) * | 2013-04-24 | 2014-11-26 | 南京大学 | 生物质有机胍催化法合成光学纯l-/d-丙交酯的工艺方法 |
| EP3056490A1 (en) * | 2015-02-13 | 2016-08-17 | PURAC Biochem BV | Method for manufacturing lactide |
| US10286729B2 (en) | 2015-04-07 | 2019-05-14 | Lehigh Technologies, Inc. | Tire having crack resistant sidewalls |
| CN104892564B (zh) * | 2015-06-04 | 2017-07-07 | 中国科学院长春应用化学研究所 | 一种高分子量聚乳酸制备丙交酯的方法 |
| CN107118200B (zh) | 2016-02-24 | 2020-02-28 | 香港纺织及成衣研发中心有限公司 | 一种利用乳酸催化合成丙交酯的方法 |
| BE1024147B1 (fr) | 2016-05-11 | 2017-11-22 | Galactic S.A. | Procede de purification d'une solution aqueuse d'acide lactique |
| JP6751164B2 (ja) * | 2017-01-24 | 2020-09-02 | 株式会社クレハ | α−ヒドロキシカルボン酸2量体環状エステルの製造方法 |
| CN106892893B (zh) * | 2017-03-01 | 2020-09-25 | 中国科学院长春应用化学研究所 | 一种乳酸低聚物制备丙交酯的方法 |
| CN108424408B (zh) * | 2018-03-08 | 2020-04-03 | 深圳市立心科学有限公司 | 医用丙交酯的制备方法 |
| CN112427048A (zh) * | 2020-12-15 | 2021-03-02 | 江苏景宏新材料科技有限公司 | 一种亚锡盐配合物催化剂及其生产l-丙交酯的方法 |
| BE1028899B1 (nl) | 2020-12-15 | 2022-07-19 | Despriet Gebroeders Nv | Systeem voor de recyclage van polymelkzuur in afvalstromen om lactide te verkrijgen |
| BE1028893B1 (nl) | 2020-12-15 | 2022-07-19 | Despriet Gebroeders Nv | Recyclageproces voor polymelkzuur in afvalstromen om lactide te verkrijgen |
| KR102939245B1 (ko) * | 2021-07-05 | 2026-03-12 | 주식회사 엘지화학 | 폴리락트산 중합체의 제조 방법 |
| CN114634526B (zh) * | 2022-03-10 | 2024-04-02 | 江苏景宏新材料科技有限公司 | 一种Ti-P配合物的制备方法及其应用 |
| CN115253994A (zh) * | 2022-08-25 | 2022-11-01 | 陕西德信祥能源科技有限公司 | 一种制备丙交酯的装置及方法 |
| EP4613742A1 (en) * | 2024-03-07 | 2025-09-10 | Sulzer Management AG | A method and plant for preparing a crude lactide composition using a lactide synthesis reactor comprising a distillation column and a loop reactor |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4504382A (en) * | 1982-10-14 | 1985-03-12 | Exxon Research And Engineering Co. | Phosphorus-containing catalyst and catalytic cracking process utilizing the same |
| EP0261572A1 (de) * | 1986-09-20 | 1988-03-30 | Boehringer Ingelheim Kg | Verfahren zur Herstellung von Lactid |
| US5274127A (en) | 1990-09-18 | 1993-12-28 | Biopak Technology, Ltd. | Lactide production from dehydration of aqueous lactic acid feed |
| US4977122A (en) * | 1989-06-05 | 1990-12-11 | Exxon Research And Engineering Company | Cracking catalyst |
| JP3075607B2 (ja) * | 1991-10-18 | 2000-08-14 | 三井化学株式会社 | ラクチドの製造法 |
| US5236560A (en) * | 1992-03-13 | 1993-08-17 | E. I. Du Pont De Nemours And Company | Solventless dimeric cyclic ester distillation process |
| JPH0631175A (ja) * | 1992-07-14 | 1994-02-08 | Toyobo Co Ltd | ラクチド化触媒 |
| DE69330046T2 (de) * | 1992-10-02 | 2001-11-15 | Cargill, Inc. | Schmelzstabiles lactidpolymergewebe und verfahren zu seiner herstellung |
| JP3601075B2 (ja) * | 1994-06-08 | 2004-12-15 | 大日本インキ化学工業株式会社 | ラクタイド類の製造方法 |
| DE19546657A1 (de) * | 1995-12-14 | 1997-06-19 | Giulini Chemie | Neue hydrolysenbeständige aliphatische Polyesteramide, ihre Herstellung und Verwendung |
| JP3780567B2 (ja) * | 1996-06-11 | 2006-05-31 | トヨタ自動車株式会社 | ラクチド製造方法 |
| EP0894156A4 (en) * | 1996-11-14 | 2002-06-26 | Atotech Deutschland Gmbh | REMOVAL OF ORTHOPHOSPHITIONS FROM ELECTRICIZED NICKEL PLATING BATHS |
| GB2331986B (en) * | 1997-12-03 | 2002-06-26 | Kobe Steel Europ Ltd | Stabiliser for cyclic lactone production |
| CA2552395A1 (en) * | 2003-12-10 | 2005-06-23 | Tate & Lyle Public Limited Company | Purification process for lactide |
| JP4565278B2 (ja) * | 2004-03-10 | 2010-10-20 | 株式会社日立プラントテクノロジー | ラクチド合成方法及びラクチド合成装置 |
| BE1018247A3 (fr) * | 2008-08-14 | 2010-07-06 | Futerro Sa | Procede d'obtention de lactide. |
-
2007
- 2007-12-19 EP EP07024679A patent/EP2072508A1/fr not_active Withdrawn
-
2008
- 2008-12-19 AU AU2008337402A patent/AU2008337402B2/en not_active Ceased
- 2008-12-19 EP EP08862516A patent/EP2222658B1/fr active Active
- 2008-12-19 ES ES08862516T patent/ES2365589T3/es active Active
- 2008-12-19 BR BRPI0820774A patent/BRPI0820774B1/pt not_active IP Right Cessation
- 2008-12-19 US US12/809,216 patent/US8592609B2/en active Active
- 2008-12-19 WO PCT/EP2008/067994 patent/WO2009077615A1/fr not_active Ceased
- 2008-12-19 CN CN2008801215179A patent/CN101903370B/zh active Active
- 2008-12-19 AT AT08862516T patent/ATE512956T1/de active
- 2008-12-19 JP JP2010538750A patent/JP5179595B2/ja active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US8592609B2 (en) | 2013-11-26 |
| JP2011506573A (ja) | 2011-03-03 |
| ES2365589T3 (es) | 2011-10-07 |
| CN101903370B (zh) | 2013-07-03 |
| BRPI0820774B1 (pt) | 2016-12-13 |
| EP2222658B1 (fr) | 2011-06-15 |
| ATE512956T1 (de) | 2011-07-15 |
| WO2009077615A1 (fr) | 2009-06-25 |
| AU2008337402B2 (en) | 2011-09-01 |
| JP5179595B2 (ja) | 2013-04-10 |
| CN101903370A (zh) | 2010-12-01 |
| AU2008337402A1 (en) | 2009-06-25 |
| EP2222658A1 (fr) | 2010-09-01 |
| EP2072508A1 (fr) | 2009-06-24 |
| US20110155557A1 (en) | 2011-06-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 19/12/2008, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 10A ANUIDADE. |
|
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2494 DE 23-10-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |