BRPI0922311A2 - processos para a purificação de polimetilol bruto, e para a produção de polímeros ou redes. - Google Patents

processos para a purificação de polimetilol bruto, e para a produção de polímeros ou redes.

Info

Publication number
BRPI0922311A2
BRPI0922311A2 BRPI0922311A BRPI0922311A BRPI0922311A2 BR PI0922311 A2 BRPI0922311 A2 BR PI0922311A2 BR PI0922311 A BRPI0922311 A BR PI0922311A BR PI0922311 A BRPI0922311 A BR PI0922311A BR PI0922311 A2 BRPI0922311 A2 BR PI0922311A2
Authority
BR
Brazil
Prior art keywords
networks
purification
polymers
processes
production
Prior art date
Application number
BRPI0922311A
Other languages
English (en)
Portuguese (pt)
Inventor
Michael Steiniger
Stefan Rittinger
Steffen Maas
Tilman Sirch
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BRPI0922311A2 publication Critical patent/BRPI0922311A2/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/82—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C59/01—Saturated compounds having only one carboxyl group and containing hydroxy or O-metal groups
    • C07C59/06—Glycolic acid
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/56—Polyacetals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
    • C08L75/04—Polyurethanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
BRPI0922311A 2008-12-09 2009-12-07 processos para a purificação de polimetilol bruto, e para a produção de polímeros ou redes. BRPI0922311A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP08171044 2008-12-09
PCT/EP2009/066521 WO2010066673A2 (de) 2008-12-09 2009-12-07 Verfahren zur herstellung von polymethylolen

Publications (1)

Publication Number Publication Date
BRPI0922311A2 true BRPI0922311A2 (pt) 2016-01-05

Family

ID=42111051

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0922311A BRPI0922311A2 (pt) 2008-12-09 2009-12-07 processos para a purificação de polimetilol bruto, e para a produção de polímeros ou redes.

Country Status (10)

Country Link
US (1) US8575401B2 (de)
EP (1) EP2376414A2 (de)
JP (1) JP2012511533A (de)
KR (1) KR20110098941A (de)
CN (1) CN101747144A (de)
BR (1) BRPI0922311A2 (de)
MY (1) MY153850A (de)
RU (1) RU2530027C2 (de)
TW (1) TWI450883B (de)
WO (1) WO2010066673A2 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8575401B2 (en) 2008-12-09 2013-11-05 Basf Se Method for purifying crude polymethylols
US8884076B2 (en) 2008-12-09 2014-11-11 Basf Se Method for preparing polymethylols
BRPI1006870A2 (pt) 2009-01-12 2016-03-15 Basf Se processo para recuperar componentes de uma mistura de baixo ponto de ebulição
US8853465B2 (en) 2010-05-12 2014-10-07 Basf Se Process for preparing neopentyl glycol
JP5923265B2 (ja) * 2011-09-22 2016-05-24 株式会社ササクラ 蒸発濃縮装置および蒸発濃縮方法
DE102011118993A1 (de) * 2011-11-19 2013-05-23 Oxea Gmbh Verfahren zur Gewinnung von Di-Trimethylpropan und mit Trimethylpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung
DE102011118956A1 (de) * 2011-11-19 2013-05-23 Oxea Gmbh Verfahren zur Gewinnung von Di-Trimethylolpropan und mit Trimethylolpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung
CN102795964B (zh) * 2012-09-12 2013-05-29 江西高信有机化工有限公司 一种年产2万吨钙法三羟甲基丙烷的生产工艺
US8710278B1 (en) 2013-01-31 2014-04-29 Eastman Chemical Company Process for producing polyols
US9056824B2 (en) 2013-01-31 2015-06-16 Eastman Chemical Company Preparation of hydroxy aldehydes
KR101529828B1 (ko) 2013-07-26 2015-06-17 주식회사 엘지화학 메틸올알칸알의 제조방법
US10913700B2 (en) 2018-02-01 2021-02-09 Lg Chem, Ltd. Method for producing dimethylolbutanal and distillation apparatus for producing same
CN109180428B (zh) * 2018-08-06 2020-06-05 吉林市道特化工科技有限责任公司 一种2,2-二甲基-1,3-丙二醇的生产工艺
CN110372476B (zh) * 2019-08-06 2021-03-23 北京合宜集通科技有限公司 一种2,2-二甲基-1,3-丙二醇精馏工艺

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU125552A1 (ru) * 1959-03-03 1959-11-30 Поблотивернер Винцер Хельмут Способ очистки триметилолпропана
BE754868A (fr) 1969-08-16 1971-02-15 Basf Ag Procede pour la mise en oeuvre de reactions exothermiques entreun gaz et un liquide
BE758910A (fr) 1969-11-15 1971-05-13 Basf Ag Preparation de dimethyl-2, 2-propanediol-1, 3
DE2040501C3 (de) 1970-08-14 1984-01-05 Basf Ag, 6700 Ludwigshafen Verfahren zur Durchführung von exothermen Reaktionen zwischen einem Gas und einer Flüssigkeit
US4021496A (en) 1974-06-26 1977-05-03 Eastman Kodak Company Process for the purification of neopentyl glycol
DE2702582C3 (de) 1977-01-22 1980-12-04 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von Trimethylolalkanen
DE2813201A1 (de) 1978-03-25 1979-10-04 Bayer Ag Verfahren zur herstellung von 2,2-dimethylolalkanalen
DE2827795A1 (de) * 1978-06-24 1980-01-10 Huels Chemische Werke Ag Verfahren zur gewinnung von reinem neopentylglykol
DE3027890A1 (de) 1980-07-23 1982-03-04 Basf Ag, 6700 Ludwigshafen Hydrierkatalysatoren fuer die herstellung von propandiolen und verfahren zur herstellung von propandiolen mit solchen katalysatoren
US4935555A (en) * 1988-11-25 1990-06-19 Elias Carole L Purification of neopentyl glycol
US5532417A (en) * 1991-04-26 1996-07-02 Aristech Chemical Corporation Manufacture of neopentyl glycol (IV)
ATE150439T1 (de) * 1991-06-28 1997-04-15 Aristech Chemical Corp Herstellung von neopentylglykol (iv)
JP3175360B2 (ja) * 1992-12-10 2001-06-11 三菱化学株式会社 1,4−ブタンジオールの精製方法
CN1159275C (zh) 1994-05-19 2004-07-28 巴斯福股份公司 醇的制备方法
JPH0987273A (ja) * 1995-09-22 1997-03-31 Mitsubishi Gas Chem Co Inc ε−カプロラクトンの精製方法
WO1998017614A1 (en) * 1996-10-22 1998-04-30 Lg Chemical Limited Process for the continuous production of neopentyl glycol
DE19653093A1 (de) 1996-12-20 1998-06-25 Basf Ag Verfahren zur Herstellung von Polyalkoholen
DE19809418A1 (de) 1998-03-05 1999-09-09 Basf Ag Verfahren zur Hydrierung von Carbonylverbindungen
DE19963435A1 (de) * 1999-12-28 2001-07-05 Basf Ag Verfahren zur Reinigung von durch Hydrierung hergestelltem Trimethylolpropan durch kontinuierliche Destillation
DE10160180A1 (de) * 2001-12-07 2003-06-18 Basf Ag Verfahren zur Isolierung von Trimethylolpropan aus einem Reaktionsgemisch
US7462747B2 (en) 2007-01-05 2008-12-09 Basf Aktiengesellschaft Process for preparing polyalcohols from formaldehyde having a low formic acid content
EP2118044B1 (de) * 2007-02-15 2013-05-15 Basf Se Verfahren zur herstellung von sehr reinem 1,4-butandiol
US7767865B2 (en) 2007-03-02 2010-08-03 Basf Se Method for producing hydroxypivalaldehyde and neopentyl glycol
CN101675022B (zh) 2007-03-23 2013-01-23 巴斯夫欧洲公司 通过蒸馏获得马来酸酐的方法
KR20100020036A (ko) 2007-06-14 2010-02-19 바스프 에스이 ε-카프로락톤의 제법
CN101848904B (zh) 2007-11-05 2013-05-01 巴斯夫欧洲公司 生产ε-己内酯的方法
KR20100110830A (ko) 2007-12-21 2010-10-13 바스프 에스이 ε-카프로락톤의 제조 방법
ES2393838T5 (es) 2008-02-15 2016-03-02 Basf Se Procedimiento para la obtención de ésteres de ácido 6-hidroxicaprónico
WO2010003934A1 (en) 2008-07-07 2010-01-14 Basf Se Enzyme composition comprising enzyme containing polymer particles
CN102159311B (zh) 2008-09-19 2013-07-10 巴斯夫欧洲公司 使用铝-铜催化剂连续制备胺的方法
US8884076B2 (en) 2008-12-09 2014-11-11 Basf Se Method for preparing polymethylols
US8575401B2 (en) 2008-12-09 2013-11-05 Basf Se Method for purifying crude polymethylols

Also Published As

Publication number Publication date
JP2012511533A (ja) 2012-05-24
TW201029962A (en) 2010-08-16
US8575401B2 (en) 2013-11-05
EP2376414A2 (de) 2011-10-19
RU2530027C2 (ru) 2014-10-10
US20110313203A1 (en) 2011-12-22
RU2011127887A (ru) 2013-01-20
KR20110098941A (ko) 2011-09-02
MY153850A (en) 2015-03-31
TWI450883B (zh) 2014-09-01
WO2010066673A3 (de) 2011-01-06
CN101747144A (zh) 2010-06-23
WO2010066673A2 (de) 2010-06-17

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Legal Events

Date Code Title Description
B08F Application fees: application dismissed [chapter 8.6 patent gazette]

Free format text: REFERENTE A 7A ANUIDADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]