CA1034739A - Procede d'epuration des fumees et des gaz et de productin d'acide sulfurique - Google Patents

Procede d'epuration des fumees et des gaz et de productin d'acide sulfurique

Info

Publication number: CA1034739A
Authority: CA; Canada
Prior art keywords: solution; gases; fumes; fact; sulfur dioxide
Prior art date: 1973-07-26
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA205,374A

Other languages

English (en)

French (fr)

Other versions

CA205374S (en

Inventor

Andre Salaun

Rene Trempu

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Alcatel CIT SA

Original Assignee

Compagnie Industrielle de Telecommunication CIT Alcatel SA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-07-26

Filing date

1974-07-19

Publication date

1978-07-18

1974-07-19 Application filed by Compagnie Industrielle de Telecommunication CIT Alcatel SA filed Critical Compagnie Industrielle de Telecommunication CIT Alcatel SA

1978-07-18 Application granted granted Critical

1978-07-18 Publication of CA1034739A publication Critical patent/CA1034739A/fr

Status Expired legal-status Critical Current

Links

239000007789 gas Substances 0.000 title claims abstract description 126
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims abstract description 123
238000004519 manufacturing process Methods 0.000 title claims abstract description 6
239000003517 fume Substances 0.000 title claims description 63
238000001914 filtration Methods 0.000 title claims description 10
235000011149 sulphuric acid Nutrition 0.000 title 1
239000001117 sulphuric acid Substances 0.000 title 1
239000000243 solution Substances 0.000 claims abstract description 184
RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims abstract description 142
238000005406 washing Methods 0.000 claims abstract description 109
238000000034 method Methods 0.000 claims abstract description 55
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 37
229910052760 oxygen Inorganic materials 0.000 claims abstract description 37
239000001301 oxygen Substances 0.000 claims abstract description 37
230000008569 process Effects 0.000 claims abstract description 28
230000001590 oxidative effect Effects 0.000 claims abstract description 16
239000007864 aqueous solution Substances 0.000 claims abstract description 14
239000000567 combustion gas Substances 0.000 claims abstract description 6
150000001875 compounds Chemical class 0.000 claims abstract description 6
229910001868 water Inorganic materials 0.000 claims description 32
239000000203 mixture Substances 0.000 claims description 31
239000000779 smoke Substances 0.000 claims description 31
238000000746 purification Methods 0.000 claims description 26
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
239000011572 manganese Substances 0.000 claims description 19
238000007254 oxidation reaction Methods 0.000 claims description 16
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 15
229910052748 manganese Inorganic materials 0.000 claims description 14
239000004071 soot Substances 0.000 claims description 14
230000003647 oxidation Effects 0.000 claims description 13
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical group [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 12
239000000446 fuel Substances 0.000 claims description 12
238000012856 packing Methods 0.000 claims description 12
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 8
239000002253 acid Substances 0.000 claims description 8
230000014759 maintenance of location Effects 0.000 claims description 8
230000005587 bubbling Effects 0.000 claims description 7
238000002156 mixing Methods 0.000 claims description 6
150000003463 sulfur Chemical class 0.000 claims description 6
229910017052 cobalt Inorganic materials 0.000 claims description 5
239000010941 cobalt Substances 0.000 claims description 5
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 5
238000002485 combustion reaction Methods 0.000 claims description 4
150000002697 manganese compounds Chemical class 0.000 claims description 4
229910052759 nickel Inorganic materials 0.000 claims description 4
230000008030 elimination Effects 0.000 claims description 3
238000003379 elimination reaction Methods 0.000 claims description 3
WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 3
239000007787 solid Substances 0.000 claims description 3
238000003756 stirring Methods 0.000 claims description 3
LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 2
239000012736 aqueous medium Substances 0.000 claims description 2
238000010790 dilution Methods 0.000 claims description 2
239000012895 dilution Substances 0.000 claims description 2
239000008240 homogeneous mixture Substances 0.000 claims description 2
239000002245 particle Substances 0.000 claims description 2
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims 1
150000008064 anhydrides Chemical class 0.000 abstract description 10
-1 coordination complex sulfite Chemical class 0.000 abstract description 4
235000010269 sulphur dioxide Nutrition 0.000 description 53
NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 14
239000011702 manganese sulphate Substances 0.000 description 13
235000007079 manganese sulphate Nutrition 0.000 description 13
SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 description 13
239000007800 oxidant agent Substances 0.000 description 13
229910052717 sulfur Inorganic materials 0.000 description 13
239000007788 liquid Substances 0.000 description 12
238000012546 transfer Methods 0.000 description 12
239000011593 sulfur Substances 0.000 description 11
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 9
238000006243 chemical reaction Methods 0.000 description 8
238000009434 installation Methods 0.000 description 8
239000012141 concentrate Substances 0.000 description 7
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 7
229910052753 mercury Inorganic materials 0.000 description 7
229940099596 manganese sulfate Drugs 0.000 description 6
230000003287 optical effect Effects 0.000 description 6
229910021653 sulphate ion Inorganic materials 0.000 description 6
238000011049 filling Methods 0.000 description 5
230000009466 transformation Effects 0.000 description 5
230000007423 decrease Effects 0.000 description 4
239000000463 material Substances 0.000 description 4
210000000056 organ Anatomy 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 3
239000006185 dispersion Substances 0.000 description 3
230000000694 effects Effects 0.000 description 3
239000012530 fluid Substances 0.000 description 3
239000010763 heavy fuel oil Substances 0.000 description 3
230000035800 maturation Effects 0.000 description 3
239000003921 oil Substances 0.000 description 3
NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 3
239000002244 precipitate Substances 0.000 description 3
238000000926 separation method Methods 0.000 description 3
CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 2
LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 2
TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 description 2
238000010936 aqueous wash Methods 0.000 description 2
230000003197 catalytic effect Effects 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
239000000706 filtrate Substances 0.000 description 2
239000003546 flue gas Substances 0.000 description 2
UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
235000013980 iron oxide Nutrition 0.000 description 2
159000000014 iron salts Chemical class 0.000 description 2
VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 2
RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 description 2
229910000360 iron(III) sulfate Inorganic materials 0.000 description 2
229920000915 polyvinyl chloride Polymers 0.000 description 2
239000004800 polyvinyl chloride Substances 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
108090000623 proteins and genes Proteins 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
239000000126 substance Substances 0.000 description 2
150000003464 sulfur compounds Chemical class 0.000 description 2
229940116269 uric acid Drugs 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
241000556720 Manga Species 0.000 description 1
DGEZNRSVGBDHLK-UHFFFAOYSA-N [1,10]phenanthroline Chemical compound C1=CN=C2C3=NC=CC=C3C=CC2=C1 DGEZNRSVGBDHLK-UHFFFAOYSA-N 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
238000013019 agitation Methods 0.000 description 1
210000000988 bone and bone Anatomy 0.000 description 1
238000001354 calcination Methods 0.000 description 1
230000008859 change Effects 0.000 description 1
238000003889 chemical engineering Methods 0.000 description 1
150000004696 coordination complex Chemical class 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000001739 density measurement Methods 0.000 description 1
RMGVZKRVHHSUIM-UHFFFAOYSA-N dithionic acid Chemical compound OS(=O)(=O)S(O)(=O)=O RMGVZKRVHHSUIM-UHFFFAOYSA-N 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000009977 dual effect Effects 0.000 description 1
238000005265 energy consumption Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000000605 extraction Methods 0.000 description 1
239000011790 ferrous sulphate Substances 0.000 description 1
235000003891 ferrous sulphate Nutrition 0.000 description 1
239000000295 fuel oil Substances 0.000 description 1
239000013529 heat transfer fluid Substances 0.000 description 1
150000002696 manganese Chemical class 0.000 description 1
CAQPCGTWHYQICV-UHFFFAOYSA-L manganese(2+);sulfite Chemical compound [Mn+2].[O-]S([O-])=O CAQPCGTWHYQICV-UHFFFAOYSA-L 0.000 description 1
ISPYRSDWRDQNSW-UHFFFAOYSA-L manganese(II) sulfate monohydrate Chemical compound O.[Mn+2].[O-]S([O-])(=O)=O ISPYRSDWRDQNSW-UHFFFAOYSA-L 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
FRZJZRVZZNTMAW-UHFFFAOYSA-N n,n-diethyl-3-(hydroxymethyl)benzamide Chemical compound CCN(CC)C(=O)C1=CC=CC(CO)=C1 FRZJZRVZZNTMAW-UHFFFAOYSA-N 0.000 description 1
APVPOHHVBBYQAV-UHFFFAOYSA-N n-(4-aminophenyl)sulfonyloctadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NS(=O)(=O)C1=CC=C(N)C=C1 APVPOHHVBBYQAV-UHFFFAOYSA-N 0.000 description 1
VIKNJXKGJWUCNN-XGXHKTLJSA-N norethisterone Chemical compound O=C1CC[C@@H]2[C@H]3CC[C@](C)([C@](CC4)(O)C#C)[C@@H]4[C@@H]3CCC2=C1 VIKNJXKGJWUCNN-XGXHKTLJSA-N 0.000 description 1
238000005457 optimization Methods 0.000 description 1
ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
235000020004 porter Nutrition 0.000 description 1
239000000047 product Substances 0.000 description 1
230000009467 reduction Effects 0.000 description 1
102000012498 secondary active transmembrane transporter activity proteins Human genes 0.000 description 1
108040003878 secondary active transmembrane transporter activity proteins Proteins 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
239000000725 suspension Substances 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
230000009897 systematic effect Effects 0.000 description 1
238000012360 testing method Methods 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1
238000001429 visible spectrum Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/74—Preparation
- C01B17/76—Preparation by contact processes
- C01B17/775—Liquid phase contacting processes or wet catalysis processes
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/507—Sulfur oxides by treating the gases with other liquids
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
- B01D53/8603—Removing sulfur compounds
- B01D53/8609—Sulfur oxides

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Environmental & Geological Engineering (AREA)
Chemical Kinetics & Catalysis (AREA)
Health & Medical Sciences (AREA)
Biomedical Technology (AREA)
Analytical Chemistry (AREA)
General Chemical & Material Sciences (AREA)
Oil, Petroleum & Natural Gas (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Treating Waste Gases (AREA)

CA205,374A 1973-07-26 1974-07-19 Procede d'epuration des fumees et des gaz et de productin d'acide sulfurique Expired CA1034739A (fr)

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
FR7327426A FR2238669B1 (da)	1973-07-26	1973-07-26
FR7416616A FR2271170B2 (da)	1973-07-26	1974-05-14
FR7420910A FR2274556A2 (fr)	1973-07-26	1974-06-17	Procede d'epuration des fumees et des gaz et de production d'acide sulfurique
FR7422251A FR2276260A2 (fr)	1973-07-26	1974-06-26	Procede d'epuration des fume

Publications (1)

Publication Number	Publication Date
CA1034739A true CA1034739A (fr)	1978-07-18

Family

ID=27446234

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA205,374A Expired CA1034739A (fr)	1973-07-26	1974-07-19	Procede d'epuration des fumees et des gaz et de productin d'acide sulfurique

Country Status (16)

Country	Link
JP (1)	JPS5232863B2 (da)
BE (1)	BE817789A (da)
BR (1)	BR7406151D0 (da)
CA (1)	CA1034739A (da)
CH (1)	CH599046A5 (da)
DE (1)	DE2435611C3 (da)
DK (1)	DK146120C (da)
FR (4)	FR2238669B1 (da)
GB (1)	GB1451554A (da)
IE (1)	IE39808B1 (da)
IT (1)	IT1016693B (da)
LU (1)	LU70575A1 (da)
NL (1)	NL162568C (da)
NO (1)	NO136077C (da)
RO (1)	RO65912A (da)
SE (1)	SE417397B (da)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2713992A1 (de) *	1977-03-30	1978-10-12	Kernforschungsanlage Juelich	Verfahren zur reinigung eines schwefeldioxid enthaltenden abgases
DE3629766A1 (de) *	1986-09-02	1988-03-17	Bayer Ag	Verfahren zur reinigung und wiederaufheizung von abgasen
DE3629765A1 (de) *	1986-09-02	1988-03-03	Bayer Ag	Verfahren zur reinigung von abgasen
JP3870867B2 (ja)	2002-07-19	2007-01-24	東洋製罐株式会社	熱可塑性樹脂容器の製造方法

1973
- 1973-07-26 FR FR7327426A patent/FR2238669B1/fr not_active Expired
1974
- 1974-05-14 FR FR7416616A patent/FR2271170B2/fr not_active Expired
- 1974-06-17 FR FR7420910A patent/FR2274556A2/fr active Granted
- 1974-06-26 FR FR7422251A patent/FR2276260A2/fr active Granted
- 1974-07-09 CH CH941674A patent/CH599046A5/xx not_active IP Right Cessation
- 1974-07-15 IE IE1493/74A patent/IE39808B1/xx unknown
- 1974-07-18 BE BE1006082A patent/BE817789A/xx not_active IP Right Cessation
- 1974-07-19 GB GB3217974A patent/GB1451554A/en not_active Expired
- 1974-07-19 LU LU70575A patent/LU70575A1/xx unknown
- 1974-07-19 CA CA205,374A patent/CA1034739A/fr not_active Expired
- 1974-07-24 DK DK399274A patent/DK146120C/da not_active IP Right Cessation
- 1974-07-24 DE DE2435611A patent/DE2435611C3/de not_active Expired
- 1974-07-24 NO NO742700A patent/NO136077C/no unknown
- 1974-07-24 RO RO7479871A patent/RO65912A/ro unknown
- 1974-07-24 SE SE7409601A patent/SE417397B/xx unknown
- 1974-07-25 JP JP49084683A patent/JPS5232863B2/ja not_active Expired
- 1974-07-25 BR BR6151/74A patent/BR7406151D0/pt unknown
- 1974-07-25 IT IT69365/74A patent/IT1016693B/it active
- 1974-07-26 NL NL7410136.A patent/NL162568C/xx not_active IP Right Cessation

Also Published As

Publication number	Publication date
NL7410136A (nl)	1975-01-28
GB1451554A (en)	1976-10-06
FR2276260A2 (fr)	1976-01-23
NO136077B (da)	1977-04-12
FR2274556A2 (fr)	1976-01-09
FR2274556B2 (da)	1978-12-01
FR2238669A1 (da)	1975-02-21
BR7406151D0 (pt)	1975-04-22
SE417397B (sv)	1981-03-16
IE39808B1 (en)	1979-01-03
FR2238669B1 (da)	1978-10-27
NL162568C (nl)	1980-06-16
FR2276260B2 (da)	1978-12-01
DE2435611C3 (de)	1978-09-28
FR2271170A2 (da)	1975-12-12
SE7409601L (da)	1975-01-27
NO742700L (da)	1975-02-24
NO136077C (no)	1977-07-20
LU70575A1 (da)	1975-05-21
NL162568B (nl)	1980-01-15
DK146120B (da)	1983-07-04
DK399274A (da)	1975-03-10
RO65912A (ro)	1980-05-15
IE39808L (en)	1975-01-26
DE2435611B2 (de)	1978-01-26
IT1016693B (it)	1977-06-20
CH599046A5 (da)	1978-05-12
JPS5232863B2 (da)	1977-08-24
BE817789A (fr)	1975-01-20
FR2271170B2 (da)	1978-12-01
DK146120C (da)	1983-12-05
DE2435611A1 (de)	1975-02-06
JPS5071576A (da)	1975-06-13

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CA1034739A (fr)	1978-07-18	Procede d'epuration des fumees et des gaz et de productin d'acide sulfurique
FR2585584A1 (fr)	1987-02-06	Desulfuration/denitrification des gaz de carneau en utilisant des additifs de chelates metalliques
JP6614774B2 (ja)	2019-12-04	触媒を用いた廃ガスからのＣＯ２及びＮＯｘ除去方法
FR2594707A1 (fr)	1987-08-28	Procede et appareillage pour reduire la teneur en sels inactifs de solutions residuaires de centrales nucleaires
NO138435B (no)	1978-05-29	Anordning for stoeping av metall.
JPH02237620A (ja)	1990-09-20	硫化水素除去方法
US3987149A (en)	1976-10-19	Method for removing sulfur dioxide from exhaust gas
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