CA1044982A - Detergent powder production - Google Patents

Detergent powder production

Info

Publication number: CA1044982A
Authority: CA; Canada
Prior art keywords: slurry; process according; further improvement; sodium; comprises incorporating
Prior art date: 1974-05-09
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA226,577A

Other languages

English (en)

French (fr)

Other versions

CA226577S (en

Inventor

Stewart C. Gray

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Unilever PLC

Original Assignee

Unilever PLC

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1974-05-09

Filing date

1975-05-08

Publication date

1978-12-26

1975-05-08 Application filed by Unilever PLC filed Critical Unilever PLC

1978-12-26 Application granted granted Critical

1978-12-26 Publication of CA1044982A publication Critical patent/CA1044982A/en

Status Expired legal-status Critical Current

Links

239000000843 powder Substances 0.000 title claims abstract description 33
239000003599 detergent Substances 0.000 title claims abstract description 13
238000004519 manufacturing process Methods 0.000 title claims abstract description 5
239000002002 slurry Substances 0.000 claims abstract description 27
239000000463 material Substances 0.000 claims abstract description 18
238000000034 method Methods 0.000 claims abstract description 15
239000002736 nonionic surfactant Substances 0.000 claims abstract description 9
KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims abstract description 8
229910001948 sodium oxide Inorganic materials 0.000 claims abstract description 5
239000004115 Sodium Silicate Substances 0.000 claims abstract description 4
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 4
229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 4
238000006701 autoxidation reaction Methods 0.000 claims description 15
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 claims description 4
238000001694 spray drying Methods 0.000 claims description 4
239000003760 tallow Substances 0.000 claims description 4
239000000377 silicon dioxide Substances 0.000 claims description 3
229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
239000004480 active ingredient Substances 0.000 claims description 2
229910052681 coesite Inorganic materials 0.000 claims description 2
229910052906 cristobalite Inorganic materials 0.000 claims description 2
235000012239 silicon dioxide Nutrition 0.000 claims description 2
229910052682 stishovite Inorganic materials 0.000 claims description 2
229910052905 tridymite Inorganic materials 0.000 claims description 2
238000002347 injection Methods 0.000 claims 1
239000007924 injection Substances 0.000 claims 1
239000011149 active material Substances 0.000 abstract description 2
239000002585 base Substances 0.000 description 11
239000000203 mixture Substances 0.000 description 8
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
239000004615 ingredient Substances 0.000 description 5
239000000344 soap Substances 0.000 description 5
235000013162 Cocos nucifera Nutrition 0.000 description 4
244000060011 Cocos nucifera Species 0.000 description 4
150000001298 alcohols Chemical class 0.000 description 4
239000003638 chemical reducing agent Substances 0.000 description 4
150000003839 salts Chemical class 0.000 description 4
-1 sulpho Chemical class 0.000 description 4
125000000217 alkyl group Chemical group 0.000 description 3
235000019832 sodium triphosphate Nutrition 0.000 description 3
239000007921 spray Substances 0.000 description 3
241000905957 Channa melasoma Species 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
229910019142 PO4 Inorganic materials 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
239000004133 Sodium thiosulphate Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000000945 filler Substances 0.000 description 2
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
239000010452 phosphate Substances 0.000 description 2
229920001983 poloxamer Polymers 0.000 description 2
229910052708 sodium Inorganic materials 0.000 description 2
239000011734 sodium Substances 0.000 description 2
ZZNDQCACFUJAKJ-UHFFFAOYSA-N 1-phenyltridecan-1-one Chemical compound CCCCCCCCCCCCC(=O)C1=CC=CC=C1 ZZNDQCACFUJAKJ-UHFFFAOYSA-N 0.000 description 1
241000640882 Condea Species 0.000 description 1
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 1
239000004435 Oxo alcohol Substances 0.000 description 1
239000002253 acid Substances 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
239000003513 alkali Substances 0.000 description 1
150000004996 alkyl benzenes Chemical class 0.000 description 1
125000000129 anionic group Chemical group 0.000 description 1
239000003945 anionic surfactant Substances 0.000 description 1
239000003963 antioxidant agent Substances 0.000 description 1
235000006708 antioxidants Nutrition 0.000 description 1
229940118783 capric diethanolamide Drugs 0.000 description 1
239000002738 chelating agent Substances 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
235000019864 coconut oil Nutrition 0.000 description 1
239000003240 coconut oil Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
238000009472 formulation Methods 0.000 description 1
230000002401 inhibitory effect Effects 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
BPXGKRUSMCVZAF-UHFFFAOYSA-N n,n-bis(2-hydroxyethyl)decanamide Chemical compound CCCCCCCCCC(=O)N(CCO)CCO BPXGKRUSMCVZAF-UHFFFAOYSA-N 0.000 description 1
FZQAYFWUOCXLKJ-UHFFFAOYSA-N n,n-bis(2-hydroxyethyl)octanamide Chemical compound CCCCCCCC(=O)N(CCO)CCO FZQAYFWUOCXLKJ-UHFFFAOYSA-N 0.000 description 1
SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 1
WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 1
239000002304 perfume Substances 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
229960001922 sodium perborate Drugs 0.000 description 1
229940048086 sodium pyrophosphate Drugs 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulphite Substances [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 1
235000010265 sodium sulphite Nutrition 0.000 description 1
AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 1
235000019345 sodium thiosulphate Nutrition 0.000 description 1
YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 description 1
241000894007 species Species 0.000 description 1
230000003019 stabilising effect Effects 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1
235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
JSPLKZUTYZBBKA-UHFFFAOYSA-N trioxidane Chemical compound OOO JSPLKZUTYZBBKA-UHFFFAOYSA-N 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
238000005406 washing Methods 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
- C11D1/523—Carboxylic alkylolamides, or dialkylolamides, or hydroxycarboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain one hydroxy group per alkyl group
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/835—Mixtures of non-ionic with cationic compounds
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0042—Reducing agents
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/044—Hydroxides or bases
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Detergent Compositions (AREA)

CA226,577A 1974-05-09 1975-05-08 Detergent powder production Expired CA1044982A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GB20449/74A GB1506392A (en)	1974-05-09	1974-05-09	Detergent powder production

Publications (1)

Publication Number	Publication Date
CA1044982A true CA1044982A (en)	1978-12-26

Family

ID=10146143

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA226,577A Expired CA1044982A (en)	1974-05-09	1975-05-08	Detergent powder production

Country Status (9)

Country	Link
JP (1)	JPS5837360B2 (de)
AT (1)	AT374824B (de)
CA (1)	CA1044982A (de)
DE (1)	DE2520187A1 (de)
FR (1)	FR2279844A1 (de)
GB (1)	GB1506392A (de)
IT (1)	IT1032832B (de)
SE (1)	SE446879B (de)
ZA (1)	ZA752882B (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4797225A (en) *	1986-09-08	1989-01-10	Colgate-Palmolive Company	Nonaqueous liquid nonionic laundry detergent composition containing an alkali metal dithionite or sulfite reduction bleaching agent and method of use
CN104120046A (zh) *	2013-04-28	2014-10-29	临沂市晞迪助剂有限公司	洗涤添加剂
EP3969555A1 (de)	2019-06-21	2022-03-23	Ecolab USA, Inc.	Feste nichtionische tensidzusammensetzungen

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NO121968C (de) *	1966-06-23	1977-06-13	Mo Och Domsjoe Ab
US3664961A (en) *	1970-03-31	1972-05-23	Procter & Gamble	Enzyme detergent composition containing coagglomerated perborate bleaching agent

1974
- 1974-05-09 GB GB20449/74A patent/GB1506392A/en not_active Expired
1975
- 1975-05-05 ZA ZA00752882A patent/ZA752882B/xx unknown
- 1975-05-06 DE DE19752520187 patent/DE2520187A1/de not_active Ceased
- 1975-05-06 AT AT0345875A patent/AT374824B/de not_active IP Right Cessation
- 1975-05-06 SE SE7505282A patent/SE446879B/xx not_active IP Right Cessation
- 1975-05-07 IT IT68171/75A patent/IT1032832B/it active
- 1975-05-07 FR FR7514394A patent/FR2279844A1/fr active Granted
- 1975-05-08 JP JP50055331A patent/JPS5837360B2/ja not_active Expired
- 1975-05-08 CA CA226,577A patent/CA1044982A/en not_active Expired

Also Published As

Publication number	Publication date
FR2279844A1 (fr)	1976-02-20
JPS5837360B2 (ja)	1983-08-16
IT1032832B (it)	1979-06-20
SE446879B (sv)	1986-10-13
ATA345875A (de)	1977-09-15
JPS50154302A (de)	1975-12-12
AT374824B (de)	1984-06-12
FR2279844B1 (de)	1980-01-25
ZA752882B (en)	1976-12-29
DE2520187A1 (de)	1975-11-27
GB1506392A (en)	1978-04-05
SE7505282L (sv)	1975-11-10

Publication	Publication Date	Title
CA1236368A (en)	1988-05-10	Process for the preparation of a powder detergent composition of high bulk density
CA2248991C (en)	2001-10-30	Powder detergent composition and method of making
US4243544A (en)	1981-01-06	Production of alumino-silicate-containing detergent composition
EP0040091A1 (de)	1981-11-18	Schaumunterdrückende Granulate zur Verwendung in Reinigungsmischungen
US3576748A (en)	1971-04-27	Free-flowing granular detergent compositions containing nta and soap
CA1122094A (en)	1982-04-20	Built liquid detergent composition
US3986987A (en)	1976-10-19	Light-density, low phosphate, puffed borax-containing detergent compositions
US2625514A (en)	1953-01-13	Noncaking abrasive detergent compositions
US4126586A (en)	1978-11-21	Process of spray drying nonionic surfactant-containing detergents also containing a cationic nitrogen compound
US4155882A (en)	1979-05-22	Process for preparing particulate detergent compositions containing nonionic surfactants
EP0520582B1 (de)	1998-02-04	Verfahren zur Herstellung von sprühgetrockneten Waschmittelzusammensetzungen auf Zeolithbasis
JPH11514033A (ja)	1999-11-30	洗剤組成物を製造する方法
US4198308A (en)	1980-04-15	Manufacture of free-flowing fabric softening detergent
CA2248994C (en)	2001-05-15	Free-flowing agglomerated nonionic surfactant detergent composition and process for making same
US5540866A (en)	1996-07-30	Dishwashing power including alkyl benzene sulphonates and magnesium or calcium
EP0119746B1 (de)	1986-06-25	Verfahren zur Herstellung von Detergenspulver
US5739095A (en)	1998-04-14	Solid peroxyhydrate bleach/detergent composition and method of preparing same
CA1266216A (en)	1990-02-27	Detergent composition and process for its production
US4083813A (en)	1978-04-11	Process for making granular detergent composition
JPS5837360B2 (ja)	1983-08-16	センザイフンマツノセイゾウホウホウ
JPS6018717B2 (ja)	1985-05-11	粒状洗剤組成物
EP0328190B1 (de)	1994-05-04	Waschmittelzusammensetzung in Teilchenform
GB1595293A (en)	1981-08-12	Process for preparing detergent powders containing nonionic surfactants
US3415752A (en)	1968-12-10	Detergent compositions
JPS6118959B2 (de)	1986-05-15