CA1050730A - Methode de preparation de l'acide nitrique - Google Patents

Methode de preparation de l'acide nitrique

Info

Publication number: CA1050730A
Authority: CA; Canada
Prior art keywords: stream; zone; nitric acid; stripper; reactor
Prior art date: 1974-04-05
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA223,744A

Other languages

English (en)

Other versions

CA223744S (en

Inventor

Stanford T. Holbrook

James M. Applegate

Wayne A. Proell

Clifford E. Selin

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

American Hydrocarbon Co

Original Assignee

American Hydrocarbon Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1974-04-05

Filing date

1975-04-03

Publication date

1979-03-20

1975-04-03 Application filed by American Hydrocarbon Co filed Critical American Hydrocarbon Co

1979-03-20 Application granted granted Critical

1979-03-20 Publication of CA1050730A publication Critical patent/CA1050730A/fr

Status Expired legal-status Critical Current

Links

GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 title claims abstract description 105
229910017604 nitric acid Inorganic materials 0.000 title claims abstract description 105
238000000034 method Methods 0.000 title claims abstract description 49
238000002360 preparation method Methods 0.000 title claims abstract description 5
MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 claims abstract description 149
238000006243 chemical reaction Methods 0.000 claims abstract description 62
239000007788 liquid Substances 0.000 claims abstract description 46
229910001868 water Inorganic materials 0.000 claims abstract description 27
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 54
239000000047 product Substances 0.000 claims description 28
229910021529 ammonia Inorganic materials 0.000 claims description 27
JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 claims description 19
239000007795 chemical reaction product Substances 0.000 claims description 16
MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 claims description 14
230000003647 oxidation Effects 0.000 claims description 12
238000007254 oxidation reaction Methods 0.000 claims description 12
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 5
229910001882 dioxygen Inorganic materials 0.000 claims description 5
238000012423 maintenance Methods 0.000 claims description 5
239000007800 oxidant agent Substances 0.000 claims 8
238000010924 continuous production Methods 0.000 claims 2
239000000543 intermediate Substances 0.000 claims 2
239000001301 oxygen Substances 0.000 abstract description 14
229910052760 oxygen Inorganic materials 0.000 abstract description 14
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 11
239000007789 gas Substances 0.000 description 82
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 53
239000002253 acid Substances 0.000 description 29
229910052757 nitrogen Inorganic materials 0.000 description 27
229960005419 nitrogen Drugs 0.000 description 27
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 16
239000003054 catalyst Substances 0.000 description 10
239000000539 dimer Substances 0.000 description 9
239000000203 mixture Substances 0.000 description 9
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 8
238000012856 packing Methods 0.000 description 8
229910052697 platinum Inorganic materials 0.000 description 7
229910001220 stainless steel Inorganic materials 0.000 description 7
239000010935 stainless steel Substances 0.000 description 7
239000007864 aqueous solution Substances 0.000 description 6
230000003197 catalytic effect Effects 0.000 description 6
238000001816 cooling Methods 0.000 description 6
GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 5
238000004458 analytical method Methods 0.000 description 5
238000010438 heat treatment Methods 0.000 description 5
239000000243 solution Substances 0.000 description 5
229910002089 NOx Inorganic materials 0.000 description 4
WFPZPJSADLPSON-UHFFFAOYSA-N dinitrogen tetraoxide Chemical compound [O-][N+](=O)[N+]([O-])=O WFPZPJSADLPSON-UHFFFAOYSA-N 0.000 description 4
230000035484 reaction time Effects 0.000 description 4
238000010521 absorption reaction Methods 0.000 description 3
239000012141 concentrate Substances 0.000 description 3
241000196324 Embryophyta Species 0.000 description 2
SNIOPGDIGTZGOP-UHFFFAOYSA-N Nitroglycerin Chemical compound [O-][N+](=O)OCC(O[N+]([O-])=O)CO[N+]([O-])=O SNIOPGDIGTZGOP-UHFFFAOYSA-N 0.000 description 2
238000004587 chromatography analysis Methods 0.000 description 2
238000010960 commercial process Methods 0.000 description 2
238000010891 electric arc Methods 0.000 description 2
230000000977 initiatory effect Effects 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
230000014759 maintenance of location Effects 0.000 description 2
238000012986 modification Methods 0.000 description 2
230000004048 modification Effects 0.000 description 2
229940073020 nitrol Drugs 0.000 description 2
239000001272 nitrous oxide Substances 0.000 description 2
230000001590 oxidative effect Effects 0.000 description 2
239000000376 reactant Substances 0.000 description 2
230000000717 retained effect Effects 0.000 description 2
230000000630 rising effect Effects 0.000 description 2
BPPVUXSMLBXYGG-UHFFFAOYSA-N 4-[3-(4,5-dihydro-1,2-oxazol-3-yl)-2-methyl-4-methylsulfonylbenzoyl]-2-methyl-1h-pyrazol-3-one Chemical compound CC1=C(C(=O)C=2C(N(C)NC=2)=O)C=CC(S(C)(=O)=O)=C1C1=NOCC1 BPPVUXSMLBXYGG-UHFFFAOYSA-N 0.000 description 1
241000180579 Arca Species 0.000 description 1
241000003910 Baronia <angiosperm> Species 0.000 description 1
101100134058 Caenorhabditis elegans nth-1 gene Proteins 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
241001091551 Clio Species 0.000 description 1
PDNNQADNLPRFPG-UHFFFAOYSA-N N.[O] Chemical compound N.[O] PDNNQADNLPRFPG-UHFFFAOYSA-N 0.000 description 1
101100296026 Streptomyces rimosus oxyE gene Proteins 0.000 description 1
239000002250 absorbent Substances 0.000 description 1
230000002745 absorbent Effects 0.000 description 1
-1 air Chemical compound 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000004061 bleaching Methods 0.000 description 1
238000009835 boiling Methods 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
230000002301 combined effect Effects 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000003795 desorption Methods 0.000 description 1
238000011161 development Methods 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
239000003344 environmental pollutant Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
230000005484 gravity Effects 0.000 description 1
CCJHDZZUWZIVJF-UHFFFAOYSA-N iodo nitrate Chemical compound [O-][N+](=O)OI CCJHDZZUWZIVJF-UHFFFAOYSA-N 0.000 description 1
229910000473 manganese(VI) oxide Inorganic materials 0.000 description 1
XITQUSLLOSKDTB-UHFFFAOYSA-N nitrofen Chemical compound C1=CC([N+](=O)[O-])=CC=C1OC1=CC=C(Cl)C=C1Cl XITQUSLLOSKDTB-UHFFFAOYSA-N 0.000 description 1
229910000069 nitrogen hydride Inorganic materials 0.000 description 1
229940099990 ogen Drugs 0.000 description 1
231100000719 pollutant Toxicity 0.000 description 1
230000004224 protection Effects 0.000 description 1
229910052703 rhodium Inorganic materials 0.000 description 1
239000010948 rhodium Substances 0.000 description 1
MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
239000007921 spray Substances 0.000 description 1
230000000153 supplemental effect Effects 0.000 description 1
208000006379 syphilis Diseases 0.000 description 1
239000011800 void material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/24—Nitric oxide (NO)
- C01B21/26—Preparation by catalytic or non-catalytic oxidation of ammonia

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Physical Or Chemical Processes And Apparatus (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Treating Waste Gases (AREA)

CA223,744A 1974-04-05 1975-04-03 Methode de preparation de l'acide nitrique Expired CA1050730A (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US45817374A	1974-04-05	1974-04-05

Publications (1)

Publication Number	Publication Date
CA1050730A true CA1050730A (fr)	1979-03-20

Family

ID=23819675

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA223,744A Expired CA1050730A (fr)	1974-04-05	1975-04-03	Methode de preparation de l'acide nitrique

Country Status (6)

Country	Link
JP (1)	JPS514095A (fr)
CA (1)	CA1050730A (fr)
DE (1)	DE2514839A1 (fr)
FR (1)	FR2274557A1 (fr)
NL (1)	NL7504061A (fr)
NO (1)	NO751143L (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN117839568A (zh) *	2024-03-08	2024-04-09	交城县三喜化工有限公司	一种生产硝酸用负压提升装置

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
RU2186021C2 (ru) *	1999-12-14	2002-07-27	Закрытое акционерное общество "Куйбышевазот"	Система управления процессом получения гидроксиламинсульфата

1975
- 1975-04-03 CA CA223,744A patent/CA1050730A/fr not_active Expired
- 1975-04-03 NO NO751143A patent/NO751143L/no unknown
- 1975-04-04 NL NL7504061A patent/NL7504061A/xx not_active Application Discontinuation
- 1975-04-04 FR FR7510674A patent/FR2274557A1/fr active Granted
- 1975-04-04 DE DE19752514839 patent/DE2514839A1/de not_active Withdrawn
- 1975-04-05 JP JP50040835A patent/JPS514095A/ja active Pending

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN117839568A (zh) *	2024-03-08	2024-04-09	交城县三喜化工有限公司	一种生产硝酸用负压提升装置
CN117839568B (zh) *	2024-03-08	2024-05-07	交城县三喜化工有限公司	一种生产硝酸用负压提升装置

Also Published As

Publication number	Publication date
DE2514839A1 (de)	1975-10-23
NO751143L (fr)	1975-10-07
JPS514095A (fr)	1976-01-13
FR2274557B1 (fr)	1979-02-09
NL7504061A (nl)	1975-10-07
FR2274557A1 (fr)	1976-01-09

Publication	Publication Date	Title
Luck et al.	1989	Selective catalytic reduction of NOx emitted by nitric acid plants
US4280990A (en)	1981-07-28	High pressure process for recovery of sulphur from gases
US10364215B2 (en)	2019-07-30	Zero emission urea process and plant
US4643887A (en)	1987-02-17	Production of sulfur trioxide, sulfuric acid and oleum
US4973457A (en)	1990-11-27	Method for the reduction of nitrogen oxide
US6214311B1 (en)	2001-04-10	Process for direct reduction of sulfur compounds to elemental sulfur in combination with the claus process
US4062928A (en)	1977-12-13	Process for the preparation of nitric acid
US4183906A (en)	1980-01-15	Oxygen-enrichment columnar absorption process for making nitric acid
CA1050730A (fr)	1979-03-20	Methode de preparation de l'acide nitrique
WO2020169465A1 (fr)	2020-08-27	Tour de blanchiment et procédé de production d'acide nitrique
US4298589A (en)	1981-11-03	Split axial flow converter in ammonia synthesis
US4151265A (en)	1979-04-24	Method and apparatus for removing nitrogen oxides from a gas stream
CA1069675A (fr)	1980-01-15	Conversion des oxydes d'azote
CA1050733A (fr)	1979-03-20	Extraction dans les gaz du dioxyde de soufre et des oxydes d'azote
CA2200996A1 (fr)	1997-10-01	Introduction d'oxygene dans la production d'acide nitrique
LU82074A1 (fr)	1980-08-08	Reduction catalytique d'oxydes d'azote par l'ammoniac en presence de clinoptilolite
CA1119780A (fr)	1982-03-16	Methode d'elimination des oxydes d'azote dans un circuit de gaz
AU2001256312B2 (en)	2005-11-10	Method for the catalytic conversion of gases with a high sulfur dioxide content
US6610259B1 (en)	2003-08-26	High efficiency catalytic carbon monoxide conversion process
RU2127224C1 (ru)	1999-03-10	Способ производства азотной кислоты
US4036934A (en)	1977-07-19	Preparation of nitric acid
RU2174946C1 (ru)	2001-10-20	Способ производства азотной кислоты
SU793931A1 (ru)	1981-01-07	Способ получени элементарнойСЕРы
CH645614A5 (it)	1984-10-15	Procedimento per eliminare l'esplosivita dei gas di spurgo da impianti per la produzione di urea.
RU2003134689A (ru)	2005-08-10	Способ получения гидроксиламинсульфата