CA1074284A - Procede chimique de production de zeolite - Google Patents

Procede chimique de production de zeolite

Info

Publication number: CA1074284A
Authority: CA; Canada
Prior art keywords: zeolite; product; metakaolin; temperature; hours
Prior art date: 1976-06-07
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA277,129A

Other languages

English (en)

Inventor

Sebastian M. Laurent

Paul F. Ranken

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Ethyl Corp

Original Assignee

Ethyl Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-06-07

Filing date

1977-04-27

Publication date

1980-03-25

1977-04-27 Application filed by Ethyl Corp filed Critical Ethyl Corp

1980-03-25 Application granted granted Critical

1980-03-25 Publication of CA1074284A publication Critical patent/CA1074284A/fr

Status Expired legal-status Critical Current

Links

238000001311 chemical methods and process Methods 0.000 title 1
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 33
238000000034 method Methods 0.000 claims abstract description 20
239000010457 zeolite Substances 0.000 claims abstract description 20
229910021536 Zeolite Inorganic materials 0.000 claims abstract description 18
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 18
NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 14
229910001868 water Inorganic materials 0.000 claims description 14
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 8
229910052708 sodium Inorganic materials 0.000 claims description 4
239000011734 sodium Substances 0.000 claims description 4
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
229910052782 aluminium Inorganic materials 0.000 claims 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
229910052760 oxygen Inorganic materials 0.000 claims 1
239000001301 oxygen Substances 0.000 claims 1
229910052710 silicon Inorganic materials 0.000 claims 1
239000000047 product Substances 0.000 description 13
238000006243 chemical reaction Methods 0.000 description 6
239000000203 mixture Substances 0.000 description 5
239000012452 mother liquor Substances 0.000 description 5
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
239000005995 Aluminium silicate Substances 0.000 description 3
235000012211 aluminium silicate Nutrition 0.000 description 3
239000011324 bead Substances 0.000 description 3
238000001354 calcination Methods 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
230000002035 prolonged effect Effects 0.000 description 3
239000000376 reactant Substances 0.000 description 3
238000002441 X-ray diffraction Methods 0.000 description 2
239000007864 aqueous solution Substances 0.000 description 2
229910052681 coesite Inorganic materials 0.000 description 2
229910052906 cristobalite Inorganic materials 0.000 description 2
238000002425 crystallisation Methods 0.000 description 2
230000008025 crystallization Effects 0.000 description 2
239000008367 deionised water Substances 0.000 description 2
229910021641 deionized water Inorganic materials 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
239000000377 silicon dioxide Substances 0.000 description 2
235000012239 silicon dioxide Nutrition 0.000 description 2
239000000243 solution Substances 0.000 description 2
229910052682 stishovite Inorganic materials 0.000 description 2
229910052905 tridymite Inorganic materials 0.000 description 2
UIQWBVPFHHQZHH-UHFFFAOYSA-N OOOOOOOOOOOOOO Chemical compound OOOOOOOOOOOOOO UIQWBVPFHHQZHH-UHFFFAOYSA-N 0.000 description 1
BFRXZIMAUMUZJH-UHFFFAOYSA-M [OH-].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] Chemical compound [OH-].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] BFRXZIMAUMUZJH-UHFFFAOYSA-M 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000007717 exclusion Effects 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000012467 final product Substances 0.000 description 1
238000009472 formulation Methods 0.000 description 1
239000002808 molecular sieve Substances 0.000 description 1
238000000634 powder X-ray diffraction Methods 0.000 description 1
238000010926 purge Methods 0.000 description 1
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
239000012265 solid product Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000006228 supernatant Substances 0.000 description 1
238000005406 washing Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
- C01B33/28—Base exchange silicates, e.g. zeolites
- C01B33/2807—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures
- C01B33/2815—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L)

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
General Life Sciences & Earth Sciences (AREA)
Geology (AREA)
Inorganic Chemistry (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)

CA277,129A 1976-06-07 1977-04-27 Procede chimique de production de zeolite Expired CA1074284A (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US69341276A	1976-06-07	1976-06-07

Publications (1)

Publication Number	Publication Date
CA1074284A true CA1074284A (fr)	1980-03-25

Family

ID=24784538

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA277,129A Expired CA1074284A (fr)	1976-06-07	1977-04-27	Procede chimique de production de zeolite

Country Status (6)

Country	Link
JP (1)	JPS5316398A (fr)
BE (1)	BE855280A (fr)
CA (1)	CA1074284A (fr)
DE (1)	DE2725496B2 (fr)
FR (1)	FR2354287A1 (fr)
GB (1)	GB1551503A (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2418771A1 (fr) *	1978-03-02	1979-09-28	Rhone Poulenc Ind	Procede de fabrication d'un silico-aluminate synthetique et produits obtenus
GB8517997D0 (en) *	1985-07-17	1985-08-21	English Clays Lovering Pochin	Synthesing faujasites
DE3835760A1 (de) *	1988-10-20	1990-04-26	Bocklenberg & Motte Bomoro	Kraftfahrzeug-tuerschloss
JP5594710B2 (ja) *	2008-03-19	2014-09-24	公益財団法人鉄道総合技術研究所	リチウム型ゼオライトの製造方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR1264441A (fr) *	1960-08-05	1961-06-19	Grace W R & Co	Procédé de préparation de zéolites synthétiques cristallines
FR1343946A (fr) *	1962-12-12	1963-11-22	Grace W R & Co	Procédé de fabrication d'adsorbants microsélectifs et en particulier de zéolites au sodium
FR83942E (fr) *	1963-06-10	1964-11-06	Grace W R & Co	Procédé de fabrication d'adsorbants micro-sélectifs et en particulier de zéolites au sodium
FR1387304A (fr) *	1963-12-20	1965-01-29	Ministerul Ind Petrolului	Procédé pour obtenir des granules ayant des formes géométriques différentes pour des tamis moléculaires comportant des pores de 4 ou 5 alpha, pour la séparation pa r persorption à lit fixe de phases gazeuses et liquides
US3852105A (en) *	1972-04-07	1974-12-03	Rca Corp	Fabrication of dark heaters

1977
- 1977-04-27 CA CA277,129A patent/CA1074284A/fr not_active Expired
- 1977-06-01 FR FR7716708A patent/FR2354287A1/fr not_active Withdrawn
- 1977-06-01 BE BE178099A patent/BE855280A/fr unknown
- 1977-06-03 GB GB2376177A patent/GB1551503A/en not_active Expired
- 1977-06-06 JP JP6659777A patent/JPS5316398A/ja active Pending
- 1977-06-06 DE DE19772725496 patent/DE2725496B2/de not_active Ceased

Also Published As

Publication number	Publication date
GB1551503A (en)	1979-08-30
FR2354287A1 (fr)	1978-01-06
JPS5316398A (en)	1978-02-15
DE2725496B2 (de)	1978-10-26
DE2725496A1 (de)	1977-12-08
BE855280A (fr)	1977-12-01

Legal Events

Date	Code	Title	Description
1997-03-25	MKEX	Expiry

Publication	Publication Date	Title
AU2019405839B2 (en)	2023-05-18	Zeolite and preparation method therefor
CA1176029B (fr)	1984-10-16	Synthese de produits a base de zincosilicate, de stannosilicate ou de titanosilicate
US4164551A (en)	1979-08-14	Preparation of zeolite
CA1213872A (fr)	1986-11-12	Preparation de zeolites
US4859343A (en)	1989-08-22	Sodium removal from brines
US4542002A (en)	1985-09-17	Silicates with high ion exchange capacity derived from sepiolite and processes for their production
US20080311033A1 (en)	2008-12-18	Process for preparing detergent builder zeolite-a from kimberlite tailings
US4055622A (en)	1977-10-25	Process for the production of zeolitic alkali metal aluminosilicates
EP0092108B1 (fr)	1987-09-23	Procédé pour le traitement d'eau usée acide contenant des composés d'aluminium et de fer
US5202438A (en)	1993-04-13	Process for the synthesis of melamine cyanurate
US4277457A (en)	1981-07-07	Alkali calcium silicates and process for preparation thereof
US5236681A (en)	1993-08-17	Layered silicate
US4659555A (en)	1987-04-21	Process for the preparation of basic copper carbonate
US4401633A (en)	1983-08-30	Two step process for the preparation of zeolite A by hydrothermal treatment of heulandite
US5385714A (en)	1995-01-31	Synthetic, crystalline aluminosilicate, method for its preparation as well as use
JPS5815024A (ja)	1983-01-28	ゼオライトの製造方法
HU181898B (en)	1983-11-28	Semicontinuous industrial process for producing zeolite a
GB1586236A (en)	1981-03-18	Method for producing synthetic sodium aluminosilicate ion-exchange material from calcined kaolin clay
JPS5845111A (ja)	1983-03-16	結晶アルミノ珪酸塩及びその製造法
US4401634A (en)	1983-08-30	Two step process for the preparation of zeolite A by hydrothermal treatment of clinoptilolite
US4294810A (en)	1981-10-13	Alkali calcium silicates and process for preparation thereof
US2076545A (en)	1937-04-13	Method of preparing a decolorizing material
GB2041902A (en)	1980-09-17	Synthetic zeolites
CN103112869B (zh)	2015-04-15	一种利用铝硅滤渣合成l型分子筛的方法
US4380531A (en)	1983-04-19	Process for preparing phosphorus acid from industrial waste materials