CA1085977A - Process for carrying out ion exchange reactions - Google Patents

Process for carrying out ion exchange reactions

Info

Publication number: CA1085977A
Authority: CA; Canada
Prior art keywords: acid; regeneration; resin; regenerating agent; solution
Prior art date: 1975-10-01
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA262,570A

Other languages

English (en)

French (fr)

Inventor

Wolfgang Heim

Gunter Prescher

Gerd Schreyer

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Evonik Operations GmbH

Original Assignee

Deutsche Gold und Silber Scheideanstalt

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-10-01

Filing date

1976-10-01

Publication date

1980-09-16

1976-10-01 Application filed by Deutsche Gold und Silber Scheideanstalt filed Critical Deutsche Gold und Silber Scheideanstalt

1980-09-16 Application granted granted Critical

1980-09-16 Publication of CA1085977A publication Critical patent/CA1085977A/en

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 77
238000005342 ion exchange Methods 0.000 title claims abstract description 11
238000006243 chemical reaction Methods 0.000 title description 15
239000011347 resin Substances 0.000 claims abstract description 51
229920005989 resin Polymers 0.000 claims abstract description 51
230000001172 regenerating effect Effects 0.000 claims abstract description 49
230000008929 regeneration Effects 0.000 claims abstract description 18
238000011069 regeneration method Methods 0.000 claims abstract description 18
238000005406 washing Methods 0.000 claims abstract description 8
239000000203 mixture Substances 0.000 claims abstract description 6
239000007788 liquid Substances 0.000 claims abstract description 5
239000003795 chemical substances by application Substances 0.000 claims description 36
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 34
239000002253 acid Substances 0.000 claims description 16
150000001768 cations Chemical class 0.000 claims description 14
229960000443 hydrochloric acid Drugs 0.000 claims description 13
235000011167 hydrochloric acid Nutrition 0.000 claims description 13
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
CYUUZGXOQDCCGH-UHFFFAOYSA-N dodecyl dodecanoate Chemical compound CCCCCCCCCCCCOC(=O)CCCCCCCCCCC CYUUZGXOQDCCGH-UHFFFAOYSA-N 0.000 claims description 4
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 3
239000001632 sodium acetate Substances 0.000 claims description 3
235000017281 sodium acetate Nutrition 0.000 claims description 3
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
159000000000 sodium salts Chemical class 0.000 claims description 2
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 2
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims 1
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims 1
239000011976 maleic acid Substances 0.000 claims 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims 1
239000000243 solution Substances 0.000 description 36
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
150000001875 compounds Chemical class 0.000 description 8
150000002500 ions Chemical class 0.000 description 7
239000011734 sodium Substances 0.000 description 7
230000001627 detrimental effect Effects 0.000 description 6
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
150000001450 anions Chemical class 0.000 description 3
MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
150000001447 alkali salts Chemical class 0.000 description 2
230000003247 decreasing effect Effects 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
150000007524 organic acids Chemical class 0.000 description 2
235000005985 organic acids Nutrition 0.000 description 2
229910052708 sodium Inorganic materials 0.000 description 2
239000011780 sodium chloride Substances 0.000 description 2
RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
XTEGARKTQYYJKE-UHFFFAOYSA-N chloric acid Chemical compound OCl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-N 0.000 description 1
229940005991 chloric acid Drugs 0.000 description 1
238000010586 diagram Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000012457 nonaqueous media Substances 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
238000011084 recovery Methods 0.000 description 1
239000012266 salt solution Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
229910001415 sodium ion Inorganic materials 0.000 description 1
239000002351 wastewater Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/05—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Chemical Kinetics & Catalysis (AREA)
Treatment Of Water By Ion Exchange (AREA)
Catalysts (AREA)
Treatment Of Liquids With Adsorbents In General (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

CA262,570A 1975-10-01 1976-10-01 Process for carrying out ion exchange reactions Expired CA1085977A (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DEP2543733.6-41		1975-10-01
DE2543733A DE2543733C2 (de)	1975-10-01	1975-10-01	Verfahren zur Durchführung von Ionenaustauschreaktionen

Publications (1)

Publication Number	Publication Date
CA1085977A true CA1085977A (en)	1980-09-16

Family

ID=5957915

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA262,570A Expired CA1085977A (en)	1975-10-01	1976-10-01	Process for carrying out ion exchange reactions

Country Status (12)

Country	Link
JP (1)	JPS5244776A (2)
AT (1)	AT352642B (2)
BE (1)	BE835086A (2)
CA (1)	CA1085977A (2)
DE (2)	DE2560444C2 (2)
ES (1)	ES451664A1 (2)
FR (1)	FR2333563A1 (2)
GB (1)	GB1552856A (2)
IN (1)	IN145788B (2)
NL (1)	NL7610905A (2)
SE (1)	SE7610884L (2)
ZA (1)	ZA765763B (2)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE393044C (de) *	1920-10-10	1924-03-28	Permutit Akt Ges	Verfahren und Vorrichtung zum Regenerieren von basenaustauschendem Filtermaterial
NL72488C (2) *	1942-06-19

1975
- 1975-10-01 DE DE19752560444 patent/DE2560444C2/de not_active Expired
- 1975-10-01 DE DE2543733A patent/DE2543733C2/de not_active Expired
- 1975-10-22 AT AT805475A patent/AT352642B/de not_active IP Right Cessation
- 1975-10-30 BE BE6045242A patent/BE835086A/xx not_active IP Right Cessation
1976
- 1976-09-18 ES ES451664A patent/ES451664A1/es not_active Expired
- 1976-09-27 ZA ZA765763A patent/ZA765763B/xx unknown
- 1976-09-30 SE SE7610884A patent/SE7610884L/xx not_active Application Discontinuation
- 1976-10-01 CA CA262,570A patent/CA1085977A/en not_active Expired
- 1976-10-01 FR FR7629677A patent/FR2333563A1/fr active Granted
- 1976-10-01 GB GB40801/76A patent/GB1552856A/en not_active Expired
- 1976-10-01 NL NL7610905A patent/NL7610905A/xx not_active Application Discontinuation
- 1976-10-01 JP JP51118428A patent/JPS5244776A/ja active Pending
- 1976-10-15 IN IN1886/CAL/76A patent/IN145788B/en unknown

Also Published As

Publication number	Publication date
SE7610884L (sv)	1977-04-02
JPS5244776A (en)	1977-04-08
BE835086A (fr)	1976-04-30
DE2543733C2 (de)	1983-02-03
DE2560444C2 (de)	1985-01-03
ATA805475A (de)	1979-02-15
ZA765763B (en)	1977-08-31
AT352642B (de)	1979-09-25
GB1552856A (en)	1979-09-19
FR2333563B1 (2)	1980-10-10
IN145788B (2)	1978-12-23
FR2333563A1 (fr)	1977-07-01
ES451664A1 (es)	1977-08-16
DE2543733A1 (de)	1977-04-07
NL7610905A (nl)	1977-04-05

Legal Events

Date	Code	Title	Description
1997-09-16	MKEX	Expiry

Publication	Publication Date	Title
US2366651A (en)	1945-01-02	Regeneration of ionic exchangers
US2267841A (en)	1941-12-30	Method of and apparatus for treating water
US4176056A (en)	1979-11-27	Cyclic operation of a bed of mixed ion exchange resins
JPS6248539B2 (2)	1987-10-14
US2736635A (en)	1956-02-28	Method of producing sulfite cooking liquors and recovering valuable constituents therefrom
US2897051A (en)	1959-07-28	Treatment of solutions comprising similarly charged monovalent and polyvalent ions to concentrate the polyvalent ions
US20050115905A1 (en)	2005-06-02	Nitrate removal
US4184948A (en)	1980-01-22	Water softening method using thermally regenerable ion exchange resin
US4857202A (en)	1989-08-15	Sodium-selective cation exchange resins for ammonia-cycle condensate polishing
US3083167A (en)	1963-03-26	Manufacture and stabilization of colloidal silicic acid
US3312617A (en)	1967-04-04	Ion exchange method and apparatus
US4427639A (en)	1984-01-24	Ion exchange process
US3160585A (en)	1964-12-08	Method of reducing the scale forming element on surfaces of an evaporator
US3975267A (en)	1976-08-17	Liquid treating system
US5104500A (en)	1992-04-14	Ion exchange removal of impurities from chlorate process liquors
JP3375154B2 (ja)	2003-02-10	フッ素含有水用処理装置
IL33003A (en)	1972-11-28	Method of uranium235enrichment by ion exchange
JPH06340563A (ja)	1994-12-13	ビスフェノールａ製造用反応器
US3522002A (en)	1970-07-28	Treatment of spent hydrochloric acid pickle liquor for recovery of hydrochloric acid
JP3810167B2 (ja)	2006-08-16	ビスフェノールａ製造用触媒の再生方法
SU1104178A1 (ru)	1984-07-23	Способ извлечени сурьмы
KR20020093010A (ko)	2002-12-12	시아나이드 염 제조 방법
SU973483A1 (ru)	1982-11-15	Способ извлечени рени из ренийсодержащих материалов
SU1458405A1 (ru)	1989-02-15	Способ десорбции меди и никел с катионита
CA1085068A (en)	1980-09-02	Ion exchange process