CA1091846A - Procede de production d'articles moules, d'enduits, de pellicules et de liaisons - Google Patents

Procede de production d'articles moules, d'enduits, de pellicules et de liaisons

Info

Publication number: CA1091846A
Authority: CA; Canada
Prior art keywords: din; weight; moulded; resin; parts
Prior art date: 1976-01-13
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA243,442A

Other languages

English (en)

Inventor

Johannes Blahak

Lothar Preis

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Bayer AG

Original Assignee

Bayer AG

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-01-13

Filing date

1976-01-13

Publication date

1980-12-16

1976-01-13 Application filed by Bayer AG filed Critical Bayer AG

1976-01-13 Priority to CA243,442A priority Critical patent/CA1091846A/fr

1980-12-16 Application granted granted Critical

1980-12-16 Publication of CA1091846A publication Critical patent/CA1091846A/fr

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 16
238000004519 manufacturing process Methods 0.000 title claims abstract description 11
238000000576 coating method Methods 0.000 title abstract description 8
125000000217 alkyl group Chemical group 0.000 claims abstract description 7
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 6
229910052739 hydrogen Inorganic materials 0.000 claims abstract description 6
239000001257 hydrogen Substances 0.000 claims abstract description 6
229920000647 polyepoxide Polymers 0.000 claims description 31
150000002118 epoxides Chemical group 0.000 claims description 19
238000006243 chemical reaction Methods 0.000 claims description 14
238000001816 cooling Methods 0.000 claims description 11
229920000642 polymer Polymers 0.000 claims description 5
150000004984 aromatic diamines Chemical class 0.000 claims description 3
239000011541 reaction mixture Substances 0.000 claims description 2
125000004209 (C1-C8) alkyl group Chemical group 0.000 claims 1
239000000376 reactant Substances 0.000 claims 1
239000000047 product Substances 0.000 abstract description 31
125000003118 aryl group Chemical group 0.000 abstract description 16
239000007795 chemical reaction product Substances 0.000 abstract description 4
150000004985 diamines Chemical class 0.000 abstract description 2
239000004971 Cross linker Substances 0.000 abstract 1
238000010438 heat treatment Methods 0.000 description 23
229920005989 resin Polymers 0.000 description 21
239000011347 resin Substances 0.000 description 21
239000000203 mixture Substances 0.000 description 18
239000000463 material Substances 0.000 description 14
239000000155 melt Substances 0.000 description 14
229920000768 polyamine Polymers 0.000 description 14
239000003822 epoxy resin Substances 0.000 description 13
238000003756 stirring Methods 0.000 description 12
238000003860 storage Methods 0.000 description 11
239000003795 chemical substances by application Substances 0.000 description 10
230000002035 prolonged effect Effects 0.000 description 10
150000001875 compounds Chemical class 0.000 description 9
229910052751 metal Inorganic materials 0.000 description 9
239000007788 liquid Substances 0.000 description 8
239000002184 metal Substances 0.000 description 8
239000007787 solid Substances 0.000 description 8
241000428199 Mustelinae Species 0.000 description 7
229910052757 nitrogen Inorganic materials 0.000 description 7
BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 6
239000002253 acid Substances 0.000 description 6
150000001412 amines Chemical class 0.000 description 6
-1 epoxide compounds Chemical class 0.000 description 6
238000000465 moulding Methods 0.000 description 6
150000002148 esters Chemical class 0.000 description 5
150000002989 phenols Chemical class 0.000 description 5
PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 4
150000004982 aromatic amines Chemical class 0.000 description 4
238000006735 epoxidation reaction Methods 0.000 description 4
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 3
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 3
229920001577 copolymer Polymers 0.000 description 3
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
239000004848 polyfunctional curative Substances 0.000 description 3
MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
NPSJHQMIVNJLNN-UHFFFAOYSA-N 2-ethylhexyl 4-nitrobenzoate Chemical compound CCCCC(CC)COC(=O)C1=CC=C([N+]([O-])=O)C=C1 NPSJHQMIVNJLNN-UHFFFAOYSA-N 0.000 description 2
239000004808 2-ethylhexylester Substances 0.000 description 2
KHUIRIRTZCOEMK-UHFFFAOYSA-N 2-methylpropyl 3,5-diamino-4-chlorobenzoate Chemical compound CC(C)COC(=O)C1=CC(N)=C(Cl)C(N)=C1 KHUIRIRTZCOEMK-UHFFFAOYSA-N 0.000 description 2
HSBOCPVKJMBWTF-UHFFFAOYSA-N 4-[1-(4-aminophenyl)ethyl]aniline Chemical compound C=1C=C(N)C=CC=1C(C)C1=CC=C(N)C=C1 HSBOCPVKJMBWTF-UHFFFAOYSA-N 0.000 description 2
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
MQJKPEGWNLWLTK-UHFFFAOYSA-N Dapsone Chemical compound C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=C1 MQJKPEGWNLWLTK-UHFFFAOYSA-N 0.000 description 2
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
JRPRCOLKIYRSNH-UHFFFAOYSA-N bis(oxiran-2-ylmethyl) benzene-1,2-dicarboxylate Chemical compound C=1C=CC=C(C(=O)OCC2OC2)C=1C(=O)OCC1CO1 JRPRCOLKIYRSNH-UHFFFAOYSA-N 0.000 description 2
PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 description 2
WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 2
238000005266 casting Methods 0.000 description 2
239000003054 catalyst Substances 0.000 description 2
YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 2
238000004132 cross linking Methods 0.000 description 2
GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical class C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 2
239000000975 dye Substances 0.000 description 2
150000002170 ethers Chemical class 0.000 description 2
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
239000011152 fibreglass Substances 0.000 description 2
239000000945 filler Substances 0.000 description 2
125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 2
125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
KYZHGEFMXZOSJN-UHFFFAOYSA-N isobutyl benzoate Chemical compound CC(C)COC(=O)C1=CC=CC=C1 KYZHGEFMXZOSJN-UHFFFAOYSA-N 0.000 description 2
125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 2
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
150000002576 ketones Chemical class 0.000 description 2
238000002156 mixing Methods 0.000 description 2
239000000049 pigment Substances 0.000 description 2
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
238000005245 sintering Methods 0.000 description 2
239000002904 solvent Substances 0.000 description 2
229940113165 trimethylolpropane Drugs 0.000 description 2
OZCRKDNRAAKDAN-HNQUOIGGSA-N (e)-but-1-ene-1,4-diol Chemical compound OCC\C=C\O OZCRKDNRAAKDAN-HNQUOIGGSA-N 0.000 description 1
BOJZPUPAXYETRK-UHFFFAOYSA-N 1,1-diphenylethane-1,2-diamine Chemical compound C=1C=CC=CC=1C(N)(CN)C1=CC=CC=C1 BOJZPUPAXYETRK-UHFFFAOYSA-N 0.000 description 1
VYXHVRARDIDEHS-UHFFFAOYSA-N 1,5-cyclooctadiene Chemical compound C1CC=CCCC=C1 VYXHVRARDIDEHS-UHFFFAOYSA-N 0.000 description 1
239000004912 1,5-cyclooctadiene Substances 0.000 description 1
LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 1
HECLRDQVFMWTQS-RGOKHQFPSA-N 1755-01-7 Chemical compound C1[C@H]2[C@@H]3CC=C[C@@H]3[C@@H]1C=C2 HECLRDQVFMWTQS-RGOKHQFPSA-N 0.000 description 1
STMDPCBYJCIZOD-UHFFFAOYSA-N 2-(2,4-dinitroanilino)-4-methylpentanoic acid Chemical compound CC(C)CC(C(O)=O)NC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O STMDPCBYJCIZOD-UHFFFAOYSA-N 0.000 description 1
DPYGXXBYDWQPRQ-UHFFFAOYSA-N 2-methylpropyl 3,5-diamino-4-methylbenzoate Chemical compound CC(C)COC(=O)C1=CC(N)=C(C)C(N)=C1 DPYGXXBYDWQPRQ-UHFFFAOYSA-N 0.000 description 1
UPZSGWVELOYWER-UHFFFAOYSA-N 3,5-diamino-4-chlorobenzoic acid Chemical compound NC1=CC(C(O)=O)=CC(N)=C1Cl UPZSGWVELOYWER-UHFFFAOYSA-N 0.000 description 1
YBRVSVVVWCFQMG-UHFFFAOYSA-N 4,4'-diaminodiphenylmethane Chemical compound C1=CC(N)=CC=C1CC1=CC=C(N)C=C1 YBRVSVVVWCFQMG-UHFFFAOYSA-N 0.000 description 1
VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical compound C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 description 1
MIFGCULLADMRTF-UHFFFAOYSA-N 4-[(4-hydroxy-3-methylphenyl)methyl]-2-methylphenol Chemical compound C1=C(O)C(C)=CC(CC=2C=C(C)C(O)=CC=2)=C1 MIFGCULLADMRTF-UHFFFAOYSA-N 0.000 description 1
WFCQTAXSWSWIHS-UHFFFAOYSA-N 4-[bis(4-hydroxyphenyl)methyl]phenol Chemical compound C1=CC(O)=CC=C1C(C=1C=CC(O)=CC=1)C1=CC=C(O)C=C1 WFCQTAXSWSWIHS-UHFFFAOYSA-N 0.000 description 1
229910015900 BF3 Inorganic materials 0.000 description 1
241000543381 Cliftonia monophylla Species 0.000 description 1
238000005698 Diels-Alder reaction Methods 0.000 description 1
OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
239000003377 acid catalyst Substances 0.000 description 1
238000007259 addition reaction Methods 0.000 description 1
239000000654 additive Substances 0.000 description 1
239000000853 adhesive Substances 0.000 description 1
230000001070 adhesive effect Effects 0.000 description 1
150000001299 aldehydes Chemical class 0.000 description 1
125000001931 aliphatic group Chemical group 0.000 description 1
125000003545 alkoxy group Chemical group 0.000 description 1
125000004453 alkoxycarbonyl group Chemical group 0.000 description 1
125000004429 atom Chemical group 0.000 description 1
150000001555 benzenes Chemical class 0.000 description 1
VCCBEIPGXKNHFW-UHFFFAOYSA-N biphenyl-4,4'-diol Chemical group C1=CC(O)=CC=C1C1=CC=C(O)C=C1 VCCBEIPGXKNHFW-UHFFFAOYSA-N 0.000 description 1
XFUOBHWPTSIEOV-UHFFFAOYSA-N bis(oxiran-2-ylmethyl) cyclohexane-1,2-dicarboxylate Chemical compound C1CCCC(C(=O)OCC2OC2)C1C(=O)OCC1CO1 XFUOBHWPTSIEOV-UHFFFAOYSA-N 0.000 description 1
KBWLNCUTNDKMPN-UHFFFAOYSA-N bis(oxiran-2-ylmethyl) hexanedioate Chemical compound C1OC1COC(=O)CCCCC(=O)OCC1CO1 KBWLNCUTNDKMPN-UHFFFAOYSA-N 0.000 description 1
WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical class FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 1
230000031709 bromination Effects 0.000 description 1
238000005893 bromination reaction Methods 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
150000001735 carboxylic acids Chemical class 0.000 description 1
238000005660 chlorination reaction Methods 0.000 description 1
239000000460 chlorine Substances 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
125000001309 chloro group Chemical group Cl* 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
239000008199 coating composition Substances 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
238000010276 construction Methods 0.000 description 1
ZOLLIQAKMYWTBR-RYMQXAEESA-N cyclododecatriene Chemical compound C/1C\C=C\CC\C=C/CC\C=C\1 ZOLLIQAKMYWTBR-RYMQXAEESA-N 0.000 description 1
150000001991 dicarboxylic acids Chemical class 0.000 description 1
150000002009 diols Chemical class 0.000 description 1
ZZTCPWRAHWXWCH-UHFFFAOYSA-N diphenylmethanediamine Chemical compound C=1C=CC=CC=1C(N)(N)C1=CC=CC=C1 ZZTCPWRAHWXWCH-UHFFFAOYSA-N 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000032050 esterification Effects 0.000 description 1
238000005886 esterification reaction Methods 0.000 description 1
238000001125 extrusion Methods 0.000 description 1
239000004744 fabric Substances 0.000 description 1
239000003365 glass fiber Substances 0.000 description 1
229960005150 glycerol Drugs 0.000 description 1
VOZRXNHHFUQHIL-UHFFFAOYSA-N glycidyl methacrylate Chemical compound CC(=C)C(=O)OCC1CO1 VOZRXNHHFUQHIL-UHFFFAOYSA-N 0.000 description 1
125000005843 halogen group Chemical group 0.000 description 1
LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
MUTGBJKUEZFXGO-UHFFFAOYSA-N hexahydrophthalic anhydride Chemical compound C1CCCC2C(=O)OC(=O)C21 MUTGBJKUEZFXGO-UHFFFAOYSA-N 0.000 description 1
238000007654 immersion Methods 0.000 description 1
239000011810 insulating material Substances 0.000 description 1
239000013067 intermediate product Substances 0.000 description 1
ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 1
238000010030 laminating Methods 0.000 description 1
WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 1
150000007522 mineralic acids Chemical class 0.000 description 1
125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
229920003986 novolac Polymers 0.000 description 1
239000003921 oil Substances 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
235000005985 organic acids Nutrition 0.000 description 1
229940059574 pentaerithrityl Drugs 0.000 description 1
WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
229920001223 polyethylene glycol Polymers 0.000 description 1
229940068917 polyethylene glycols Drugs 0.000 description 1
229920001195 polyisoprene Polymers 0.000 description 1
229920005862 polyol Polymers 0.000 description 1
150000003077 polyols Chemical class 0.000 description 1
150000008442 polyphenolic compounds Chemical class 0.000 description 1
235000013824 polyphenols Nutrition 0.000 description 1
125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
DZAHJZSBTYPXIM-UHFFFAOYSA-N propan-2-yl 3,5-diamino-4-methylbenzoate Chemical compound CC(C)OC(=O)C1=CC(N)=C(C)C(N)=C1 DZAHJZSBTYPXIM-UHFFFAOYSA-N 0.000 description 1
239000012779 reinforcing material Substances 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
238000005507 spraying Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
150000005846 sugar alcohols Polymers 0.000 description 1
150000003573 thiols Chemical class 0.000 description 1
229920006305 unsaturated polyester Polymers 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
230000003245 working effect Effects 0.000 description 1

Landscapes

Epoxy Resins (AREA)

CA243,442A 1976-01-13 1976-01-13 Procede de production d'articles moules, d'enduits, de pellicules et de liaisons Expired CA1091846A (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA243,442A CA1091846A (fr)	1976-01-13	1976-01-13	Procede de production d'articles moules, d'enduits, de pellicules et de liaisons

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CA243,442A CA1091846A (fr)	1976-01-13	1976-01-13	Procede de production d'articles moules, d'enduits, de pellicules et de liaisons

Publications (1)

Publication Number	Publication Date
CA1091846A true CA1091846A (fr)	1980-12-16

Family

ID=4104976

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA243,442A Expired CA1091846A (fr)	1976-01-13	1976-01-13	Procede de production d'articles moules, d'enduits, de pellicules et de liaisons

Country Status (1)

Country	Link
CA (1)	CA1091846A (fr)

1976
- 1976-01-13 CA CA243,442A patent/CA1091846A/fr not_active Expired

Legal Events

Date	Code	Title	Description
1997-12-16	MKEX	Expiry

Publication	Publication Date	Title
EP0618935B1 (fr)	1997-11-12	Resines de polyimide utiles a des temperatures elevees
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JPH09501714A (ja)	1997-02-18	エポキシ‐芳香族アミン樹脂用潜伏性熱硬化促進剤
US3839493A (en)	1974-10-01	Epoxy resin compositions
US4619986A (en)	1986-10-28	Epoxy phthalonitrile polymers
US4560739A (en)	1985-12-24	Triglycidyl compounds of aminophenols
US3481900A (en)	1969-12-02	Use of selected 4,4'-methylenebis (2,6-dialkylanilines) as curing agents for epoxy resins
CA1091846A (fr)	1980-12-16	Procede de production d'articles moules, d'enduits, de pellicules et de liaisons
US3632555A (en)	1972-01-04	Preparation of epoxylated phenolic resins by reacting polymers fro aralkyl ethers and phenols with epihalohydrin
CA1337136C (fr)	1995-09-26	Resines reticulees
JPH0784530B2 (ja)	1995-09-13	繊維強化複合材料
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US3215586A (en)	1965-11-02	Modified epoxidized polybutadiene resin composition
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US3957727A (en)	1976-05-18	Epoxy composition containing acid anhydride compound obtained from nadic methyl anhydride
US4851484A (en)	1989-07-25	Anhydride-based fortifiers for anhydride-cured epoxy resins
JPH0224305A (ja)	1990-01-26	熱硬化性樹脂組成物
USRE29027E (en)	1976-11-02	Reaction products of polyepoxide and excess di-2-oxazoline
KR900004221B1 (ko)	1990-06-18	변성비스말레이미드 수지의 제조방법