CA1173602A - Methode de production de pate speciale super-alpha par cuisson multi-etagee, y compris la prehydrolise en milieu acide - Google Patents
Methode de production de pate speciale super-alpha par cuisson multi-etagee, y compris la prehydrolise en milieu acideInfo
- Publication number
- CA1173602A CA1173602A CA000391377A CA391377A CA1173602A CA 1173602 A CA1173602 A CA 1173602A CA 000391377 A CA000391377 A CA 000391377A CA 391377 A CA391377 A CA 391377A CA 1173602 A CA1173602 A CA 1173602A
- Authority
- CA
- Canada
- Prior art keywords
- wood
- hydrolysate
- cook
- dry matter
- recited
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 30
- 239000002253 acid Substances 0.000 title claims abstract description 15
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims abstract description 6
- 239000000413 hydrolysate Substances 0.000 claims abstract description 24
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 claims abstract description 23
- 230000007062 hydrolysis Effects 0.000 claims abstract description 20
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 20
- 239000002023 wood Substances 0.000 claims abstract description 20
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims abstract description 9
- 238000012993 chemical processing Methods 0.000 claims abstract description 3
- 150000007524 organic acids Chemical class 0.000 claims description 11
- 235000005985 organic acids Nutrition 0.000 claims description 11
- 238000001704 evaporation Methods 0.000 claims description 10
- 230000008020 evaporation Effects 0.000 claims description 10
- 150000002772 monosaccharides Chemical class 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 8
- 150000002016 disaccharides Chemical class 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 241000283690 Bos taurus Species 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 238000001311 chemical methods and process Methods 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 108010009736 Protein Hydrolysates Proteins 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims description 2
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 claims 8
- 239000004155 Chlorine dioxide Substances 0.000 claims 4
- 235000019398 chlorine dioxide Nutrition 0.000 claims 4
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000012545 processing Methods 0.000 abstract description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 229920002488 Hemicellulose Polymers 0.000 description 6
- 150000007513 acids Chemical class 0.000 description 6
- RAHZWNYVWXNFOC-UHFFFAOYSA-N sulfur dioxide Inorganic materials O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 5
- 150000004676 glycans Chemical class 0.000 description 4
- 229920005610 lignin Polymers 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000005017 polysaccharide Substances 0.000 description 4
- 239000011122 softwood Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 229920001282 polysaccharide Polymers 0.000 description 3
- 235000000346 sugar Nutrition 0.000 description 3
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- 229920000297 Rayon Polymers 0.000 description 2
- 230000009102 absorption Effects 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N formic acid Substances OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 150000002402 hexoses Chemical class 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 150000002972 pentoses Chemical class 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- 240000005020 Acaciella glauca Species 0.000 description 1
- 235000018185 Betula X alpestris Nutrition 0.000 description 1
- 235000018212 Betula X uliginosa Nutrition 0.000 description 1
- 244000089654 Betula populifolia Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 238000002835 absorbance Methods 0.000 description 1
- 230000003851 biochemical process Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229910001902 chlorine oxide Inorganic materials 0.000 description 1
- MAYPHUUCLRDEAZ-UHFFFAOYSA-N chlorine peroxide Chemical compound ClOOCl MAYPHUUCLRDEAZ-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000009089 cytolysis Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 239000007849 furan resin Substances 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002482 oligosaccharides Polymers 0.000 description 1
- 150000004804 polysaccharides Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
- 150000003742 xyloses Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/32—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from hydrolysates of wood or straw
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/22—Other features of pulping processes
- D21C3/26—Multistage processes
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Animal Husbandry (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Molecular Biology (AREA)
- Zoology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Food Science & Technology (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Paper (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI803802 | 1980-12-08 | ||
| FI803802A FI63267B (fi) | 1980-12-08 | 1980-12-08 | Foerfarande foer framstaellning av specialcellulosa med hoegt alfatal genom flerstegskokning innefattande syrafoerhydrolys |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1173602A true CA1173602A (fr) | 1984-09-04 |
Family
ID=8513967
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000391377A Expired CA1173602A (fr) | 1980-12-08 | 1981-12-02 | Methode de production de pate speciale super-alpha par cuisson multi-etagee, y compris la prehydrolise en milieu acide |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS57121688A (fr) |
| CA (1) | CA1173602A (fr) |
| FI (1) | FI63267B (fr) |
| FR (1) | FR2495654B1 (fr) |
| SE (1) | SE8107247L (fr) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010046532A1 (fr) | 2008-10-21 | 2010-04-29 | Danisco A/S | Procédé de production de xylose et de pâte pour transformation chimique |
| US8262854B2 (en) | 2006-02-10 | 2012-09-11 | Metso Paper, Inc. | Method for recovering hydrolysis products |
| WO2017142445A1 (fr) * | 2016-02-16 | 2017-08-24 | Valmet Ab | Procédé de récupération d'hydrolysat concentré après l'hydrolyse de matière de cellulose |
| WO2020204793A1 (fr) | 2019-04-01 | 2020-10-08 | Valmet Ab | Procédé d'extraction d'hémicellulose d'une matière lignocellulosique |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4436586A (en) * | 1982-01-22 | 1984-03-13 | Kamyr, Inc. | Method of producing kraft pulp using an acid prehydrolysis and pre-extraction |
| CN1099501C (zh) * | 1999-09-21 | 2003-01-22 | 中国科学院广州化学研究所 | 一种桉树溶解浆粕的制浆方法 |
| US9260818B2 (en) * | 2007-05-23 | 2016-02-16 | Andritz Inc. | Single vessel reactor system for hydrolysis and digestion of wood chips with chemical enhanced wash method |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE442623A (fr) * | 1939-12-13 | |||
| SE389520B (sv) * | 1973-09-03 | 1976-11-08 | Kamyr Ab | Apparat for kontinuerlig utvinning av hydrolysat ur finfordelat fibermaterial |
-
1980
- 1980-12-08 FI FI803802A patent/FI63267B/fi not_active Application Discontinuation
-
1981
- 1981-12-02 CA CA000391377A patent/CA1173602A/fr not_active Expired
- 1981-12-03 SE SE8107247A patent/SE8107247L/ unknown
- 1981-12-04 FR FR8122762A patent/FR2495654B1/fr not_active Expired
- 1981-12-08 JP JP56196428A patent/JPS57121688A/ja active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8262854B2 (en) | 2006-02-10 | 2012-09-11 | Metso Paper, Inc. | Method for recovering hydrolysis products |
| WO2010046532A1 (fr) | 2008-10-21 | 2010-04-29 | Danisco A/S | Procédé de production de xylose et de pâte pour transformation chimique |
| WO2017142445A1 (fr) * | 2016-02-16 | 2017-08-24 | Valmet Ab | Procédé de récupération d'hydrolysat concentré après l'hydrolyse de matière de cellulose |
| CN108699768A (zh) * | 2016-02-16 | 2018-10-23 | 维美德公司 | 用于在纤维素材料水解后回收浓缩水解产物的方法 |
| EP3417102A4 (fr) * | 2016-02-16 | 2019-10-30 | Valmet AB | Procédé de récupération d'hydrolysat concentré après l'hydrolyse de matière de cellulose |
| CN108699768B (zh) * | 2016-02-16 | 2020-10-27 | 维美德公司 | 用于在纤维素材料水解后回收浓缩水解产物的方法 |
| US10947669B2 (en) | 2016-02-16 | 2021-03-16 | Valmet Ab | Method for recovering concentrated hydrolysate after hydrolysis of cellulose material |
| WO2020204793A1 (fr) | 2019-04-01 | 2020-10-08 | Valmet Ab | Procédé d'extraction d'hémicellulose d'une matière lignocellulosique |
| EP3947809A4 (fr) * | 2019-04-01 | 2023-01-04 | Valmet Ab | Procédé d'extraction d'hémicellulose d'une matière lignocellulosique |
Also Published As
| Publication number | Publication date |
|---|---|
| FI63267B (fi) | 1983-01-31 |
| SE8107247L (sv) | 1982-06-09 |
| FR2495654A1 (fr) | 1982-06-11 |
| FR2495654B1 (fr) | 1986-07-04 |
| FI803802L (fi) | 1982-06-09 |
| JPS57121688A (en) | 1982-07-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEC | Expiry (correction) | ||
| MKEX | Expiry |