CA1207268A - Methode de separation de l'eau et des solides en presence dans le petrole brut - Google Patents

Methode de separation de l'eau et des solides en presence dans le petrole brut

Info

Publication number: CA1207268A
Authority: CA; Canada
Prior art keywords: crude oil; crude; blended; water; oil
Prior art date: 1982-07-13
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000417687A

Other languages

English (en)

Inventor

Donald C. Roylance

Clifford P. Ronden

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Husky Oil Operations Ltd

Original Assignee

Husky Oil Operations Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-07-13

Filing date

1982-12-14

Publication date

1986-07-08

1982-12-14 Application filed by Husky Oil Operations Ltd filed Critical Husky Oil Operations Ltd

1986-07-08 Application granted granted Critical

1986-07-08 Publication of CA1207268A publication Critical patent/CA1207268A/fr

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 61
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 69
239000007787 solid Substances 0.000 title claims description 17
239000003208 petroleum Substances 0.000 title abstract description 3
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 49
229910052717 sulfur Inorganic materials 0.000 claims abstract description 47
239000011593 sulfur Substances 0.000 claims abstract description 47
239000000654 additive Substances 0.000 claims abstract description 29
239000000295 fuel oil Substances 0.000 claims abstract description 25
238000011084 recovery Methods 0.000 claims abstract description 11
239000007762 w/o emulsion Substances 0.000 claims abstract description 6
239000003921 oil Substances 0.000 claims description 53
239000010779 crude oil Substances 0.000 claims description 38
239000000839 emulsion Substances 0.000 claims description 34
230000000996 additive effect Effects 0.000 claims description 25
230000005484 gravity Effects 0.000 claims description 25
239000000470 constituent Substances 0.000 claims description 22
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 21
239000008186 active pharmaceutical agent Substances 0.000 claims description 21
239000003795 chemical substances by application Substances 0.000 claims description 21
238000000926 separation method Methods 0.000 claims description 20
238000002156 mixing Methods 0.000 claims description 18
238000010438 heat treatment Methods 0.000 claims description 12
229930195733 hydrocarbon Natural products 0.000 claims description 11
150000002430 hydrocarbons Chemical class 0.000 claims description 11
239000004215 Carbon black (E152) Substances 0.000 claims description 10
230000003068 static effect Effects 0.000 claims description 10
229910052784 alkaline earth metal Inorganic materials 0.000 claims description 9
150000001342 alkaline earth metals Chemical class 0.000 claims description 9
150000001875 compounds Chemical class 0.000 claims description 9
239000003085 diluting agent Substances 0.000 claims description 9
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 8
229910052783 alkali metal Inorganic materials 0.000 claims description 8
150000001340 alkali metals Chemical class 0.000 claims description 8
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 7
239000002245 particle Substances 0.000 claims description 7
150000002484 inorganic compounds Chemical class 0.000 claims description 6
229910010272 inorganic material Inorganic materials 0.000 claims description 6
239000007788 liquid Substances 0.000 claims description 6
FCMYSEXCLRFWBP-UHFFFAOYSA-N [NH4+].[NH4+].[O-]S(=O)S([O-])=O Chemical class [NH4+].[NH4+].[O-]S(=O)S([O-])=O FCMYSEXCLRFWBP-UHFFFAOYSA-N 0.000 claims description 3
229910003480 inorganic solid Inorganic materials 0.000 claims 2
239000006185 dispersion Substances 0.000 claims 1
150000004679 hydroxides Chemical class 0.000 claims 1
238000004064 recycling Methods 0.000 claims 1
AOSFMYBATFLTAQ-UHFFFAOYSA-N 1-amino-3-(benzimidazol-1-yl)propan-2-ol Chemical compound C1=CC=C2N(CC(O)CN)C=NC2=C1 AOSFMYBATFLTAQ-UHFFFAOYSA-N 0.000 abstract description 7
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 39
239000012071 phase Substances 0.000 description 24
239000000203 mixture Substances 0.000 description 18
239000000523 sample Substances 0.000 description 18
238000011282 treatment Methods 0.000 description 16
239000007864 aqueous solution Substances 0.000 description 10
230000000368 destabilizing effect Effects 0.000 description 10
238000002149 energy-dispersive X-ray emission spectroscopy Methods 0.000 description 10
238000004458 analytical method Methods 0.000 description 8
239000000463 material Substances 0.000 description 8
238000013019 agitation Methods 0.000 description 7
239000000243 solution Substances 0.000 description 7
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 description 6
238000006243 chemical reaction Methods 0.000 description 5
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
239000012153 distilled water Substances 0.000 description 4
239000012528 membrane Substances 0.000 description 4
238000010795 Steam Flooding Methods 0.000 description 3
230000003113 alkalizing effect Effects 0.000 description 3
230000000694 effects Effects 0.000 description 3
238000007667 floating Methods 0.000 description 3
229910000037 hydrogen sulfide Inorganic materials 0.000 description 3
238000002360 preparation method Methods 0.000 description 3
230000000087 stabilizing effect Effects 0.000 description 3
239000004094 surface-active agent Substances 0.000 description 3
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical class [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
238000004566 IR spectroscopy Methods 0.000 description 2
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
238000002441 X-ray diffraction Methods 0.000 description 2
229940037003 alum Drugs 0.000 description 2
235000011114 ammonium hydroxide Nutrition 0.000 description 2
239000004927 clay Substances 0.000 description 2
ZLCCLBKPLLUIJC-UHFFFAOYSA-L disodium tetrasulfane-1,4-diide Chemical compound [Na+].[Na+].[S-]SS[S-] ZLCCLBKPLLUIJC-UHFFFAOYSA-L 0.000 description 2
VDQVEACBQKUUSU-UHFFFAOYSA-M disodium;sulfanide Chemical compound [Na+].[Na+].[SH-] VDQVEACBQKUUSU-UHFFFAOYSA-M 0.000 description 2
238000001035 drying Methods 0.000 description 2
239000010442 halite Substances 0.000 description 2
150000007529 inorganic bases Chemical class 0.000 description 2
238000000399 optical microscopy Methods 0.000 description 2
239000011148 porous material Substances 0.000 description 2
239000010453 quartz Substances 0.000 description 2
238000007670 refining Methods 0.000 description 2
235000002639 sodium chloride Nutrition 0.000 description 2
229910052979 sodium sulfide Inorganic materials 0.000 description 2
230000006641 stabilisation Effects 0.000 description 2
238000011105 stabilization Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
238000000954 titration curve Methods 0.000 description 2
238000009827 uniform distribution Methods 0.000 description 2
239000008096 xylene Substances 0.000 description 2
-1 i.e. Substances 0.000 description 1
QNRATNLHPGXHMA-XZHTYLCXSA-N (r)-(6-ethoxyquinolin-4-yl)-[(2s,4s,5r)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]methanol;hydrochloride Chemical compound Cl.C([C@H]([C@H](C1)CC)C2)CN1[C@@H]2[C@H](O)C1=CC=NC2=CC=C(OCC)C=C21 QNRATNLHPGXHMA-XZHTYLCXSA-N 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
XUKUURHRXDUEBC-KAYWLYCHSA-N Atorvastatin Chemical compound C=1C=CC=CC=1C1=C(C=2C=CC(F)=CC=2)N(CC[C@@H](O)C[C@@H](O)CC(O)=O)C(C(C)C)=C1C(=O)NC1=CC=CC=C1 XUKUURHRXDUEBC-KAYWLYCHSA-N 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
235000006679 Mentha X verticillata Nutrition 0.000 description 1
235000002899 Mentha suaveolens Nutrition 0.000 description 1
235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
ZGSDJMADBJCNPN-UHFFFAOYSA-N [S-][NH3+] Chemical class [S-][NH3+] ZGSDJMADBJCNPN-UHFFFAOYSA-N 0.000 description 1
239000003513 alkali Substances 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
229940075397 calomel Drugs 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
238000012512 characterization method Methods 0.000 description 1
230000007797 corrosion Effects 0.000 description 1
238000005260 corrosion Methods 0.000 description 1
238000001514 detection method Methods 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000007865 diluting Methods 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical compound Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
238000006073 displacement reaction Methods 0.000 description 1
238000009826 distribution Methods 0.000 description 1
GRWZHXKQBITJKP-UHFFFAOYSA-N dithionous acid Chemical class OS(=O)S(O)=O GRWZHXKQBITJKP-UHFFFAOYSA-N 0.000 description 1
229940079593 drug Drugs 0.000 description 1
239000003814 drug Substances 0.000 description 1
238000004945 emulsification Methods 0.000 description 1
230000001747 exhibiting effect Effects 0.000 description 1
238000000605 extraction Methods 0.000 description 1
238000010191 image analysis Methods 0.000 description 1
238000011065 in-situ storage Methods 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
229920000592 inorganic polymer Polymers 0.000 description 1
238000009434 installation Methods 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
238000011068 loading method Methods 0.000 description 1
238000005259 measurement Methods 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
238000011192 particle characterization Methods 0.000 description 1
238000003909 pattern recognition Methods 0.000 description 1
229920000515 polycarbonate Polymers 0.000 description 1
239000004417 polycarbonate Substances 0.000 description 1
239000012047 saturated solution Substances 0.000 description 1
238000004626 scanning electron microscopy Methods 0.000 description 1
238000000550 scanning electron microscopy energy dispersive X-ray spectroscopy Methods 0.000 description 1
238000010008 shearing Methods 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 1
238000010561 standard procedure Methods 0.000 description 1
150000003464 sulfur compounds Chemical class 0.000 description 1
239000010414 supernatant solution Substances 0.000 description 1
239000013589 supplement Substances 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1
238000001771 vacuum deposition Methods 0.000 description 1

Landscapes

Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

CA000417687A 1982-07-13 1982-12-14 Methode de separation de l'eau et des solides en presence dans le petrole brut Expired CA1207268A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US39793582A	1982-07-13	1982-07-13
US397,935		1982-07-13

Publications (1)

Publication Number	Publication Date
CA1207268A true CA1207268A (fr)	1986-07-08

Family

ID=23573288

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000417687A Expired CA1207268A (fr)	1982-07-13	1982-12-14	Methode de separation de l'eau et des solides en presence dans le petrole brut

Country Status (1)

Country	Link
CA (1)	CA1207268A (fr)

1982
- 1982-12-14 CA CA000417687A patent/CA1207268A/fr not_active Expired

Legal Events

Date	Code	Title	Description
2003-07-08	MKEX	Expiry

Publication	Publication Date	Title
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US6214213B1 (en)	2001-04-10	Solvent process for bitumen seperation from oil sands froth
EP0134088B1 (fr)	1989-03-01	Traitement de pétroles bruts visqueux
US4392944A (en)	1983-07-12	Alkali recycle process for recovery of heavy oils and bitumens
US8603326B2 (en)	2013-12-10	Systems, methods and compositions for the separation and recovery of hydrocarbons from particulate matter
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US4722781A (en)	1988-02-02	Desalting process
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CA1207268A (fr)	1986-07-08	Methode de separation de l'eau et des solides en presence dans le petrole brut
WO1990009507A1 (fr)	1990-08-23	Extraction d'huile a partir de deblais de forage contamines par des hydrocarbures
US3468789A (en)	1969-09-23	Processing of viscous oil emulsions
CN104169397B (zh)	2016-08-31	从油砂中回收沥青的方法
CA1149304A (fr)	1983-07-05	Procede de rupture d'emulsion de sables bitumineux
DE69817080T2 (de)	2004-06-17	Verfahren zur Verminderung des Sauregehalts von Rohöl
US3245466A (en)	1966-04-12	Breaking oil-in-water emulsions and removal of solid matter from the oil
CA1150173A (fr)	1983-07-19	Procede pour resoudre des emulsions dans des liquides issus du traitement sur place de sables bitumineux