CA1325221C - Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses - Google Patents

Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses

Info

Publication number: CA1325221C
Authority: CA; Canada
Prior art keywords: oil; slurry; phospholipids; solids; bearing material
Prior art date: 1986-04-23
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA000616368A

Other languages

English (en)

Inventor

Hans R. Strop

Richard R. Perry

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1986-04-23

Filing date

1992-05-06

Publication date

1993-12-14

1986-04-23 Priority claimed from US06/855,127 external-priority patent/US4808426A/en

1992-05-06 Application filed by Individual filed Critical Individual

1992-05-06 Priority to CA000616368A priority Critical patent/CA1325221C/fr

1993-12-14 Application granted granted Critical

1993-12-14 Publication of CA1325221C publication Critical patent/CA1325221C/fr

2007-04-22 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

150000003904 phospholipids Chemical class 0.000 title claims abstract description 97
238000000034 method Methods 0.000 title claims abstract description 55
239000000463 material Substances 0.000 title claims abstract description 38
230000008569 process Effects 0.000 title claims abstract description 33
238000000605 extraction Methods 0.000 title claims description 20
238000007670 refining Methods 0.000 claims abstract description 40
239000003153 chemical reaction reagent Substances 0.000 claims abstract description 39
238000002156 mixing Methods 0.000 claims abstract description 16
239000003921 oil Substances 0.000 claims description 225
235000019198 oils Nutrition 0.000 claims description 224
239000002002 slurry Substances 0.000 claims description 88
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 77
235000010469 Glycine max Nutrition 0.000 claims description 59
244000068988 Glycine max Species 0.000 claims description 55
239000007787 solid Substances 0.000 claims description 39
240000008042 Zea mays Species 0.000 claims description 28
235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 28
235000002017 Zea mays subsp mays Nutrition 0.000 claims description 28
235000005822 corn Nutrition 0.000 claims description 28
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical group OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 25
235000015112 vegetable and seed oil Nutrition 0.000 claims description 20
239000008158 vegetable oil Substances 0.000 claims description 20
238000000227 grinding Methods 0.000 claims description 16
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
238000005406 washing Methods 0.000 claims description 7
241000196324 Embryophyta Species 0.000 claims description 6
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 4
238000010438 heat treatment Methods 0.000 claims description 4
DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 3
238000001704 evaporation Methods 0.000 claims description 3
235000011121 sodium hydroxide Nutrition 0.000 claims description 3
229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
235000011152 sodium sulphate Nutrition 0.000 claims description 3
BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 2
229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 2
235000019796 monopotassium phosphate Nutrition 0.000 claims description 2
238000005191 phase separation Methods 0.000 claims description 2
WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 claims description 2
229910000342 sodium bisulfate Inorganic materials 0.000 claims description 2
229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 2
239000007790 solid phase Substances 0.000 claims description 2
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 2
229910000406 trisodium phosphate Inorganic materials 0.000 claims description 2
235000019801 trisodium phosphate Nutrition 0.000 claims description 2
239000003352 sequestering agent Substances 0.000 claims 3
108091006629 SLC13A2 Proteins 0.000 claims 2
XLYOFNOQVPJJNP-ZSJDYOACSA-N heavy water Substances [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 claims 2
239000007836 KH2PO4 Substances 0.000 claims 1
229910004835 Na2B4O7 Inorganic materials 0.000 claims 1
239000007832 Na2SO4 Substances 0.000 claims 1
229910000397 disodium phosphate Inorganic materials 0.000 claims 1
235000019800 disodium phosphate Nutrition 0.000 claims 1
UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 claims 1
235000011007 phosphoric acid Nutrition 0.000 claims 1
GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 claims 1
235000017550 sodium carbonate Nutrition 0.000 claims 1
235000011149 sulphuric acid Nutrition 0.000 claims 1
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 32
238000012545 processing Methods 0.000 abstract description 28
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 24
239000011575 calcium Substances 0.000 abstract description 24
239000011574 phosphorus Substances 0.000 abstract description 24
229910052698 phosphorus Inorganic materials 0.000 abstract description 24
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract description 21
229910052791 calcium Inorganic materials 0.000 abstract description 21
239000011777 magnesium Substances 0.000 abstract description 20
229910052749 magnesium Inorganic materials 0.000 abstract description 20
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 18
229910052742 iron Inorganic materials 0.000 abstract description 16
229910021654 trace metal Inorganic materials 0.000 abstract description 3
239000000047 product Substances 0.000 description 34
238000012360 testing method Methods 0.000 description 33
238000002360 preparation method Methods 0.000 description 31
235000021588 free fatty acids Nutrition 0.000 description 25
239000000203 mixture Substances 0.000 description 22
239000010779 crude oil Substances 0.000 description 18
235000005687 corn oil Nutrition 0.000 description 16
239000002285 corn oil Substances 0.000 description 16
229910000147 aluminium phosphate Inorganic materials 0.000 description 12
238000010411 cooking Methods 0.000 description 12
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 12
239000000126 substance Substances 0.000 description 12
102000004190 Enzymes Human genes 0.000 description 11
229940088598 enzyme Drugs 0.000 description 11
229910052753 mercury Inorganic materials 0.000 description 11
108090000790 Enzymes Proteins 0.000 description 10
238000006243 chemical reaction Methods 0.000 description 10
239000012153 distilled water Substances 0.000 description 10
235000012054 meals Nutrition 0.000 description 10
238000011282 treatment Methods 0.000 description 9
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
229910052751 metal Inorganic materials 0.000 description 8
239000002184 metal Substances 0.000 description 8
150000002739 metals Chemical class 0.000 description 8
239000012071 phase Substances 0.000 description 8
239000000243 solution Substances 0.000 description 8
244000046052 Phaseolus vulgaris Species 0.000 description 7
235000010627 Phaseolus vulgaris Nutrition 0.000 description 7
235000013305 food Nutrition 0.000 description 7
239000002245 particle Substances 0.000 description 7
235000012424 soybean oil Nutrition 0.000 description 7
239000003549 soybean oil Substances 0.000 description 7
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 6
238000013459 approach Methods 0.000 description 6
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
230000014759 maintenance of location Effects 0.000 description 6
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
239000001509 sodium citrate Substances 0.000 description 6
NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 6
230000008901 benefit Effects 0.000 description 5
239000000796 flavoring agent Substances 0.000 description 5
235000019634 flavors Nutrition 0.000 description 5
239000002244 precipitate Substances 0.000 description 5
238000003825 pressing Methods 0.000 description 5
235000018102 proteins Nutrition 0.000 description 5
102000004169 proteins and genes Human genes 0.000 description 5
108090000623 proteins and genes Proteins 0.000 description 5
150000003839 salts Chemical class 0.000 description 5
239000011734 sodium Substances 0.000 description 5
229920002472 Starch Polymers 0.000 description 4
239000002253 acid Substances 0.000 description 4
239000000470 constituent Substances 0.000 description 4
230000006378 damage Effects 0.000 description 4
230000009849 deactivation Effects 0.000 description 4
238000010586 diagram Methods 0.000 description 4
230000005484 gravity Effects 0.000 description 4
238000009877 rendering Methods 0.000 description 4
230000002441 reversible effect Effects 0.000 description 4
239000000344 soap Substances 0.000 description 4
239000011780 sodium chloride Substances 0.000 description 4
235000019698 starch Nutrition 0.000 description 4
238000003860 storage Methods 0.000 description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 3
238000009874 alkali refining Methods 0.000 description 3
239000012298 atmosphere Substances 0.000 description 3
230000027455 binding Effects 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
238000004332 deodorization Methods 0.000 description 3
238000001035 drying Methods 0.000 description 3
239000012065 filter cake Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
238000012986 modification Methods 0.000 description 3
230000004048 modification Effects 0.000 description 3
238000006386 neutralization reaction Methods 0.000 description 3
230000036961 partial effect Effects 0.000 description 3
238000009928 pasteurization Methods 0.000 description 3
230000001376 precipitating effect Effects 0.000 description 3
230000009467 reduction Effects 0.000 description 3
238000000926 separation method Methods 0.000 description 3
239000002904 solvent Substances 0.000 description 3
238000000638 solvent extraction Methods 0.000 description 3
239000008107 starch Substances 0.000 description 3
231100000331 toxic Toxicity 0.000 description 3
230000002588 toxic effect Effects 0.000 description 3
239000005418 vegetable material Substances 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
241000894006 Bacteria Species 0.000 description 2
244000060011 Cocos nucifera Species 0.000 description 2
235000013162 Cocos nucifera Nutrition 0.000 description 2
KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 2
241000233866 Fungi Species 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
102000004882 Lipase Human genes 0.000 description 2
108090001060 Lipase Proteins 0.000 description 2
239000004367 Lipase Substances 0.000 description 2
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 2
108010046334 Urease Proteins 0.000 description 2
230000004075 alteration Effects 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
238000011021 bench scale process Methods 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
238000004061 bleaching Methods 0.000 description 2
239000007844 bleaching agent Substances 0.000 description 2
230000000903 blocking effect Effects 0.000 description 2
150000001669 calcium Chemical class 0.000 description 2
239000002738 chelating agent Substances 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
238000005336 cracking Methods 0.000 description 2
238000009826 distribution Methods 0.000 description 2
230000008020 evaporation Effects 0.000 description 2
239000011552 falling film Substances 0.000 description 2
239000010408 film Substances 0.000 description 2
229910001385 heavy metal Inorganic materials 0.000 description 2
238000006703 hydration reaction Methods 0.000 description 2
239000012535 impurity Substances 0.000 description 2
235000019421 lipase Nutrition 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
235000013372 meat Nutrition 0.000 description 2
239000000693 micelle Substances 0.000 description 2
230000003472 neutralizing effect Effects 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
238000003672 processing method Methods 0.000 description 2
230000002829 reductive effect Effects 0.000 description 2
229910052708 sodium Inorganic materials 0.000 description 2
239000001632 sodium acetate Substances 0.000 description 2
235000017281 sodium acetate Nutrition 0.000 description 2
230000001954 sterilising effect Effects 0.000 description 2
238000004659 sterilization and disinfection Methods 0.000 description 2
239000004094 surface-active agent Substances 0.000 description 2
238000012546 transfer Methods 0.000 description 2
QGLWBTPVKHMVHM-KTKRTIGZSA-N (z)-octadec-9-en-1-amine Chemical compound CCCCCCCC\C=C/CCCCCCCCN QGLWBTPVKHMVHM-KTKRTIGZSA-N 0.000 description 1
PORPENFLTBBHSG-MGBGTMOVSA-N 1,2-dihexadecanoyl-sn-glycerol-3-phosphate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP(O)(O)=O)OC(=O)CCCCCCCCCCCCCCC PORPENFLTBBHSG-MGBGTMOVSA-N 0.000 description 1
235000003276 Apios tuberosa Nutrition 0.000 description 1
244000105624 Arachis hypogaea Species 0.000 description 1
240000002791 Brassica napus Species 0.000 description 1
235000004977 Brassica sinapistrum Nutrition 0.000 description 1
241000426451 Camponotus modoc Species 0.000 description 1
241000237074 Centris Species 0.000 description 1
KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
240000000885 Citrullus colocynthis Species 0.000 description 1
235000015844 Citrullus colocynthis Nutrition 0.000 description 1
229920002261 Corn starch Polymers 0.000 description 1
108010082495 Dietary Plant Proteins Proteins 0.000 description 1
239000004471 Glycine Substances 0.000 description 1
240000008415 Lactuca sativa Species 0.000 description 1
241001465754 Metazoa Species 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
108010019160 Pancreatin Proteins 0.000 description 1
108091005804 Peptidases Proteins 0.000 description 1
102000035195 Peptidases Human genes 0.000 description 1
239000004365 Protease Substances 0.000 description 1
108010073771 Soybean Proteins Proteins 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
244000170226 Voandzeia subterranea Species 0.000 description 1
235000013030 Voandzeia subterranea Nutrition 0.000 description 1
230000001133 acceleration Effects 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
239000000654 additive Substances 0.000 description 1
238000005054 agglomeration Methods 0.000 description 1
230000002776 aggregation Effects 0.000 description 1
239000003513 alkali Substances 0.000 description 1
125000000129 anionic group Chemical group 0.000 description 1
239000002585 base Substances 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
239000002981 blocking agent Substances 0.000 description 1
210000000988 bone and bone Anatomy 0.000 description 1
229910021538 borax Inorganic materials 0.000 description 1
-1 calcium phosphatidates Chemical class 0.000 description 1
239000005018 casein Substances 0.000 description 1
BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
235000021240 caseins Nutrition 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
125000002091 cationic group Chemical group 0.000 description 1
239000003518 caustics Substances 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
230000008859 change Effects 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
238000004891 communication Methods 0.000 description 1
230000000536 complexating effect Effects 0.000 description 1
230000001143 conditioned effect Effects 0.000 description 1
230000003750 conditioning effect Effects 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
239000008162 cooking oil Substances 0.000 description 1
239000008120 corn starch Substances 0.000 description 1
235000012343 cottonseed oil Nutrition 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
238000013461 design Methods 0.000 description 1
238000001784 detoxification Methods 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
235000013399 edible fruits Nutrition 0.000 description 1
230000000694 effects Effects 0.000 description 1
150000002191 fatty alcohols Chemical class 0.000 description 1
235000007924 ground bean Nutrition 0.000 description 1
238000003306 harvesting Methods 0.000 description 1
230000036571 hydration Effects 0.000 description 1
BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
230000000670 limiting effect Effects 0.000 description 1
150000002632 lipids Chemical class 0.000 description 1
239000004973 liquid crystal related substance Substances 0.000 description 1
235000013310 margarine Nutrition 0.000 description 1
239000003264 margarine Substances 0.000 description 1
235000010755 mineral Nutrition 0.000 description 1
239000011707 mineral Substances 0.000 description 1
125000000896 monocarboxylic acid group Chemical group 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
235000008935 nutritious Nutrition 0.000 description 1
229940055695 pancreatin Drugs 0.000 description 1
235000020232 peanut Nutrition 0.000 description 1
150000002978 peroxides Chemical class 0.000 description 1
PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 description 1
150000003018 phosphorus compounds Chemical class 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
239000001103 potassium chloride Substances 0.000 description 1
235000011164 potassium chloride Nutrition 0.000 description 1
230000000063 preceeding effect Effects 0.000 description 1
238000002203 pretreatment Methods 0.000 description 1
WPPDXAHGCGPUPK-UHFFFAOYSA-N red 2 Chemical compound C1=CC=CC=C1C(C1=CC=CC=C11)=C(C=2C=3C4=CC=C5C6=CC=C7C8=C(C=9C=CC=CC=9)C9=CC=CC=C9C(C=9C=CC=CC=9)=C8C8=CC=C(C6=C87)C(C=35)=CC=2)C4=C1C1=CC=CC=C1 WPPDXAHGCGPUPK-UHFFFAOYSA-N 0.000 description 1
235000012045 salad Nutrition 0.000 description 1
239000012266 salt solution Substances 0.000 description 1
238000007127 saponification reaction Methods 0.000 description 1
238000004904 shortening Methods 0.000 description 1
238000004513 sizing Methods 0.000 description 1
HELHAJAZNSDZJO-OLXYHTOASA-L sodium L-tartrate Chemical compound [Na+].[Na+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O HELHAJAZNSDZJO-OLXYHTOASA-L 0.000 description 1
ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 description 1
229940039790 sodium oxalate Drugs 0.000 description 1
239000001488 sodium phosphate Substances 0.000 description 1
229940048086 sodium pyrophosphate Drugs 0.000 description 1
239000001433 sodium tartrate Substances 0.000 description 1
229960002167 sodium tartrate Drugs 0.000 description 1
235000011004 sodium tartrates Nutrition 0.000 description 1
235000010339 sodium tetraborate Nutrition 0.000 description 1
229940001941 soy protein Drugs 0.000 description 1
235000020238 sunflower seed Nutrition 0.000 description 1
239000000725 suspension Substances 0.000 description 1
238000005496 tempering Methods 0.000 description 1
235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
238000001238 wet grinding Methods 0.000 description 1
238000009736 wetting Methods 0.000 description 1

Landscapes

Fats And Perfumes (AREA)

CA000616368A 1986-04-23 1992-05-06 Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses Expired - Fee Related CA1325221C (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA000616368A CA1325221C (fr)	1986-04-23	1992-05-06	Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
US06/855,127 US4808426A (en)	1986-04-23	1986-04-23	Vegetable oil extraction process
US855,127		1986-04-23
CA000535279A CA1304750C (fr)	1986-04-23	1987-04-22	Procede d'extraction de l'huile vegetale
CA000616368A CA1325221C (fr)	1986-04-23	1992-05-06	Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses

Related Parent Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000535279A Division CA1304750C (fr)	1986-04-23	1987-04-22	Procede d'extraction de l'huile vegetale

Publications (1)

Publication Number	Publication Date
CA1325221C true CA1325221C (fr)	1993-12-14

Family

ID=25671316

Family Applications (2)

Application Number	Title	Priority Date	Filing Date
CA000616368A Expired - Fee Related CA1325221C (fr)	1986-04-23	1992-05-06	Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses
CA000616366A Expired - Fee Related CA1325220C (fr)	1986-04-23	1992-05-06	Procede d'extraction d'huile de plantes oleagineuses

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CA000616366A Expired - Fee Related CA1325220C (fr)	1986-04-23	1992-05-06	Procede d'extraction d'huile de plantes oleagineuses

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CA (2)	CA1325221C (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO2020011353A1 (fr) *	2018-07-11	2020-01-16	Zuccardi Jose Miguel	Procédé de traitement d'huile végétale

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CN113826708B (zh) *	2020-12-02	2024-04-26	丰益(上海)生物技术研发中心有限公司	风味油脂及其制备方法
CN112812886A (zh) *	2020-12-31	2021-05-18	海南大学	一种低熔点椰子油制备方法

1992
- 1992-05-06 CA CA000616368A patent/CA1325221C/fr not_active Expired - Fee Related
- 1992-05-06 CA CA000616366A patent/CA1325220C/fr not_active Expired - Fee Related

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO2020011353A1 (fr) *	2018-07-11	2020-01-16	Zuccardi Jose Miguel	Procédé de traitement d'huile végétale

Also Published As

Publication number	Publication date
CA1325220C (fr)	1993-12-14

Legal Events

Date	Code	Title	Description
1997-12-15	MKLA	Lapsed

Publication	Publication Date	Title
CA1304750C (fr)	1992-07-07	Procede d'extraction de l'huile vegetale
US5278325A (en)	1994-01-11	Vegetable oil extraction process
CA1273021A (fr)	1990-08-21	Procede de production d'huiles vegetales demucilaginees et gommes riches en acide phosphatidique
CA2049720C (fr)	2000-05-23	Procede de degommage des huiles vegetales
US5696278A (en)	1997-12-09	Degumming of crude glyceride oils not exposed to prior enzymatic activity
EP1624047B1 (fr)	2006-10-18	Procédé de récupération d'huile
US6127560A (en)	2000-10-03	Method for preparing a lower alkyl ester product from vegetable oil
US4162260A (en)	1979-07-24	Oil purification by adding hydratable phosphatides
EP0269277B1 (fr)	1991-07-24	Procédé de démucilagination d'huiles triglycéridiques
US6111120A (en)	2000-08-29	Method of refining oils and fats
CA1325220C (fr)	1993-12-14	Procede d'extraction d'huile de plantes oleagineuses
US6103918A (en)	2000-08-15	Process of producing glyceride oil having a low content of non-hydratable phosphatides
EP0170242B1 (fr)	1989-10-25	Elimination par étapes de cires d'huiles végétales comestibles
US2939790A (en)	1960-06-07	Treatment of glyceride oils and product obtained thereby
CA1157883A (fr)	1983-11-29	Demucilagination des huiles vegetales brutes par procede chimique
Zufarov et al.	2024	Phospholipids in Cottonseed Oil and Degumming Methods
JPS63146996A (ja)	1988-06-18	植物粗油の製造法
Gregory	1997	Oil Refining
Yongsoo	1988	Extrusion pretreatment to enhance soybean oil extraction
MXPA00002038A (en)	2001-12-04	Process for stabilization of oil from plant materials

CA1325221C - Procede d'extraction d'huile a faible teneur en phospholipides de matieres oleagineuses - Google Patents

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