CA1328561C - Methode pour la preparation de titane metallique et appareillage a cette fin - Google Patents
Methode pour la preparation de titane metallique et appareillage a cette finInfo
- Publication number
- CA1328561C CA1328561C CA000571625A CA571625A CA1328561C CA 1328561 C CA1328561 C CA 1328561C CA 000571625 A CA000571625 A CA 000571625A CA 571625 A CA571625 A CA 571625A CA 1328561 C CA1328561 C CA 1328561C
- Authority
- CA
- Canada
- Prior art keywords
- titanium
- product
- reaction vessel
- reducing metal
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 119
- 239000010936 titanium Substances 0.000 title claims abstract description 116
- 229910052719 titanium Inorganic materials 0.000 title claims abstract description 116
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 238000006243 chemical reaction Methods 0.000 claims abstract description 195
- 229910052751 metal Inorganic materials 0.000 claims abstract description 69
- 239000002184 metal Substances 0.000 claims abstract description 68
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims abstract description 36
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims abstract description 22
- 238000002844 melting Methods 0.000 claims abstract description 22
- 230000008018 melting Effects 0.000 claims abstract description 22
- 239000000047 product Substances 0.000 claims description 55
- 239000003795 chemical substances by application Substances 0.000 claims description 54
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical group [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 53
- 239000011777 magnesium Substances 0.000 claims description 53
- 229910052749 magnesium Inorganic materials 0.000 claims description 53
- 238000000034 method Methods 0.000 claims description 30
- 239000006227 byproduct Substances 0.000 claims description 28
- 239000007788 liquid Substances 0.000 claims description 27
- 238000001816 cooling Methods 0.000 claims description 11
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 238000004581 coalescence Methods 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 238000009835 boiling Methods 0.000 abstract description 5
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 74
- 229910001629 magnesium chloride Inorganic materials 0.000 description 37
- 238000010438 heat treatment Methods 0.000 description 36
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 14
- 230000005674 electromagnetic induction Effects 0.000 description 14
- 229910052786 argon Inorganic materials 0.000 description 7
- 239000007789 gas Substances 0.000 description 6
- 239000002826 coolant Substances 0.000 description 5
- 239000000376 reactant Substances 0.000 description 5
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000006698 induction Effects 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 229910010293 ceramic material Inorganic materials 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000010574 gas phase reaction Methods 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910001507 metal halide Inorganic materials 0.000 description 2
- 150000005309 metal halides Chemical class 0.000 description 2
- 239000012768 molten material Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- -1 alumina Chemical compound 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000012777 electrically insulating material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 229910052735 hafnium Inorganic materials 0.000 description 1
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 description 1
- 239000003779 heat-resistant material Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229910001338 liquidmetal Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- 239000010955 niobium Substances 0.000 description 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- ZWYDDDAMNQQZHD-UHFFFAOYSA-L titanium(ii) chloride Chemical compound [Cl-].[Cl-].[Ti+2] ZWYDDDAMNQQZHD-UHFFFAOYSA-L 0.000 description 1
- YONPGGFAJWQGJC-UHFFFAOYSA-K titanium(iii) chloride Chemical compound Cl[Ti](Cl)Cl YONPGGFAJWQGJC-UHFFFAOYSA-K 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17701487A JPS6421021A (en) | 1987-07-17 | 1987-07-17 | Production of metallic titanium |
| JP62-177014 | 1987-07-17 | ||
| JP62-190186 | 1987-07-31 | ||
| JP62190186A JP2554888B2 (ja) | 1987-07-31 | 1987-07-31 | 金属チタンの製造法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1328561C true CA1328561C (fr) | 1994-04-19 |
Family
ID=26497701
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000571625A Expired - Fee Related CA1328561C (fr) | 1987-07-17 | 1988-07-08 | Methode pour la preparation de titane metallique et appareillage a cette fin |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP0299791B1 (fr) |
| AU (1) | AU618541B2 (fr) |
| CA (1) | CA1328561C (fr) |
| DE (1) | DE3875411T2 (fr) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7445658B2 (en) | 1994-08-01 | 2008-11-04 | Uchicago Argonne, Llc | Titanium and titanium alloys |
| KR100241134B1 (ko) * | 1994-08-01 | 2000-03-02 | 리차드 피. 앤더슨 | 금속 및 다른 원소들의 제조방법 |
| US7435282B2 (en) | 1994-08-01 | 2008-10-14 | International Titanium Powder, Llc | Elemental material and alloy |
| US5958106A (en) * | 1994-08-01 | 1999-09-28 | International Titanium Powder, L.L.C. | Method of making metals and other elements from the halide vapor of the metal |
| RU2201984C2 (ru) * | 2001-07-16 | 2003-04-10 | Открытое акционерное общество "АВИСМА титано-магниевый комбинат" | Способ получения губчатого титана |
| RU2208653C1 (ru) * | 2001-11-26 | 2003-07-20 | Открытое акционерное общество "АВИСМА титано-магниевый комбинат" | Способ получения губчатого титана и устройство для его осуществления |
| CA2497999A1 (fr) | 2002-09-07 | 2004-03-18 | International Titanium Powder, Llc. | Procede et dispositif pour la separation de titane dans une suspension de titane |
| AU2003263082A1 (en) | 2002-10-07 | 2004-05-04 | International Titanium Powder, Llc. | System and method of producing metals and alloys |
| RU2238342C1 (ru) * | 2003-02-11 | 2004-10-20 | Открытое акционерное общество "АВИСМА титано-магниевый комбинат" | Способ получения титана губчатого и устройство для его осуществления |
| US20070017319A1 (en) | 2005-07-21 | 2007-01-25 | International Titanium Powder, Llc. | Titanium alloy |
| JP2009511739A (ja) | 2005-10-06 | 2009-03-19 | インターナショナル・タイテイニアム・パウダー・リミテッド・ライアビリティ・カンパニー | ホウ化チタン |
| RU2310001C1 (ru) * | 2006-03-07 | 2007-11-10 | Открытое Акционерное Общество "Российский научно-исследовательский и проектный институт титана и магния" (ОАО "РИТМ") | Устройство для магниетермического получения губчатого титана |
| LV13528B (en) * | 2006-09-25 | 2007-03-20 | Ervins Blumbergs | Method and apparatus for continuous producing of metallic tifanium and titanium-bases alloys |
| US7753989B2 (en) | 2006-12-22 | 2010-07-13 | Cristal Us, Inc. | Direct passivation of metal powder |
| US9127333B2 (en) | 2007-04-25 | 2015-09-08 | Lance Jacobsen | Liquid injection of VCL4 into superheated TiCL4 for the production of Ti-V alloy powder |
| RU2358028C1 (ru) * | 2007-12-24 | 2009-06-10 | Открытое Акционерное Общество "Российский научно-исследовательский и проектный институт титана и магния" (ОАО "РИТМ") | Устройство для магниетермического получения губчатого титана |
| RU2413780C1 (ru) * | 2010-03-31 | 2011-03-10 | Открытое Акционерное Общество "Российский научно-исследовательский и проектный институт титана и магния" (ОАО "РИТМ") | Устройство для получения губчатого титана |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2816828A (en) * | 1956-06-20 | 1957-12-17 | Nat Res Corp | Method of producing refractory metals |
| US3847596A (en) * | 1968-02-28 | 1974-11-12 | Halomet Ag | Process of obtaining metals from metal halides |
| US3775091A (en) * | 1969-02-27 | 1973-11-27 | Interior | Induction melting of metals in cold, self-lined crucibles |
| LU81469A1 (fr) * | 1979-07-05 | 1981-02-03 | Luniversite Libre Bruxelles | Procede et installation pour la production de metaux reactifs par reduction de leurs halogenures |
| US4442083A (en) * | 1982-11-04 | 1984-04-10 | Stauffer Chemical Company | Method of desulfurizing waste gases containing sulfur dioxide |
| US4442082A (en) * | 1982-12-27 | 1984-04-10 | Sri International | Process for obtaining silicon from fluosilicic acid |
| JPS6089529A (ja) * | 1983-10-21 | 1985-05-20 | Mitsubishi Metal Corp | 金属チタンの製造法 |
-
1988
- 1988-07-08 CA CA000571625A patent/CA1328561C/fr not_active Expired - Fee Related
- 1988-07-14 AU AU19044/88A patent/AU618541B2/en not_active Ceased
- 1988-07-15 EP EP88306510A patent/EP0299791B1/fr not_active Expired - Lifetime
- 1988-07-15 DE DE8888306510T patent/DE3875411T2/de not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| AU1904488A (en) | 1989-01-19 |
| DE3875411T2 (de) | 1993-04-08 |
| EP0299791B1 (fr) | 1992-10-21 |
| DE3875411D1 (de) | 1992-11-26 |
| AU618541B2 (en) | 1992-01-02 |
| EP0299791A1 (fr) | 1989-01-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1328561C (fr) | Methode pour la preparation de titane metallique et appareillage a cette fin | |
| US4902341A (en) | Method for producing titanium alloy | |
| CA1104836A (fr) | Traduction non-disponible | |
| EP0219581B1 (fr) | Coulée bimétallique de lingot | |
| CA1153210A (fr) | Procede et appareil pour preparer des metaux reactifs allies ou non par reduction de leurs halogenures | |
| US3775091A (en) | Induction melting of metals in cold, self-lined crucibles | |
| US4139438A (en) | Arc heater production of silicon involving alkali or alkaline-earth metals | |
| CA1329990C (fr) | Methode de fusion par induction de metaux et d'alliages reactifs | |
| EP0160779B1 (fr) | Procédé et installation pour la production de titane à partir de tétrachlorure de titane | |
| US6074545A (en) | Process for the electrolytic production of metals | |
| CA1102886A (fr) | Traduction non-disponible | |
| US7381366B2 (en) | Apparatus for the production or refining of metals, and related processes | |
| US5336378A (en) | Method and apparatus for producing a high-purity titanium | |
| EP0068782B1 (fr) | Améliorations dans les cellules de réduction électrolytique | |
| JPS63192543A (ja) | 金属の連続鋳造装置及び該装置の操作方法 | |
| CA1065415A (fr) | Production du titane et du zirconium avec chauffage a l'arc electrique | |
| US4162291A (en) | Liquid silicon casting control mechanism | |
| US2753254A (en) | Method of producing refractory metal | |
| JP2630417B2 (ja) | シリコン鋳造装置 | |
| EP0209593B1 (fr) | Methode de coulee continue | |
| JP2689520B2 (ja) | 金属チタンの製造方法 | |
| JPH02185931A (ja) | 金属チタンの製造方法 | |
| JP2554888B2 (ja) | 金属チタンの製造法 | |
| US4242136A (en) | Process for producing metallic zirconium | |
| JPS5942060B2 (ja) | 金属Ｔｉの製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |