CA2003352A1 - Preparation de caprolactame - Google Patents
Preparation de caprolactameInfo
- Publication number
- CA2003352A1 CA2003352A1 CA2003352A CA2003352A CA2003352A1 CA 2003352 A1 CA2003352 A1 CA 2003352A1 CA 2003352 A CA2003352 A CA 2003352A CA 2003352 A CA2003352 A CA 2003352A CA 2003352 A1 CA2003352 A1 CA 2003352A1
- Authority
- CA
- Canada
- Prior art keywords
- caprolactam
- under
- liquid
- ammonia
- liquid phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title abstract 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- 239000012429 reaction media Substances 0.000 abstract 2
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 229910052707 ruthenium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP3843791.0 | 1988-12-24 | ||
| DE3843791A DE3843791A1 (de) | 1988-12-24 | 1988-12-24 | Verfahren zur herstellung von caprolactam |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2003352A1 true CA2003352A1 (fr) | 1990-06-24 |
| CA2003352C CA2003352C (fr) | 1999-05-04 |
Family
ID=6370185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002003352A Expired - Fee Related CA2003352C (fr) | 1988-12-24 | 1989-11-20 | Preparation de caprolactame |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4963672A (fr) |
| EP (1) | EP0376123B1 (fr) |
| JP (1) | JP2755749B2 (fr) |
| CA (1) | CA2003352C (fr) |
| DE (2) | DE3843791A1 (fr) |
| ES (1) | ES2053940T3 (fr) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4434172A1 (de) * | 1994-09-24 | 1996-03-28 | Basf Ag | Verfahren zur Herstellung von D,L-Asparaginsäure |
| MY116498A (en) * | 1995-03-01 | 2004-02-28 | Dsm Ip Assets Bv | Process for the preparation of é - caprolactam |
| US5700934A (en) * | 1995-03-01 | 1997-12-23 | Dsm N.V. | Process for the preparation of epsilon-caprolactam and epsilon-caprolactam precursors |
| US5717089A (en) * | 1995-03-01 | 1998-02-10 | Dsm N.V. | Process for the preparation of E-caprolactam |
| DE19623662A1 (de) * | 1996-06-13 | 1997-12-18 | Basf Ag | Verfahren zur Reinigung von epsilon-Caprolactam |
| KR100459818B1 (ko) | 1996-09-02 | 2004-12-03 | 이. 아이. 두퐁 드 느무르 앤드 컴퍼니 | ε-카프로락탐의 제조방법 |
| EP0826666A1 (fr) * | 1996-09-02 | 1998-03-04 | Dsm N.V. | Procédé de préparation d'epsilon-caprolactame |
| US5877314A (en) * | 1997-02-14 | 1999-03-02 | Dsm N.V. | Process to continuously prepare an aqueous mixture of episilon caprolactum and episilon caprolactum precursors |
| US5977356A (en) * | 1997-07-02 | 1999-11-02 | Industrial Technology Research Institute | Process for preparing caprolactam |
| US5990323A (en) * | 1998-10-23 | 1999-11-23 | Eastman Chemical Company | Preparation of amines |
| DE102008060340A1 (de) | 2008-12-03 | 2010-06-10 | Wolfgang F. Prof. Dr. Hölderich | Herstellung von Lactamen und Carbonsäureamide durch Beckmann-Umlagerung von Oximen in Gegenwart von Nb-Katalysatoren |
| DE102015005238A1 (de) | 2015-04-24 | 2016-10-27 | Wolfgang Hölderich | Herstellung von Lactamen durch Beckmann-Umlagerung von Oximen |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4250093A (en) * | 1979-06-29 | 1981-02-10 | The Standard Oil Company (Ohio) | Process for the preparation of laotams |
| US4356124A (en) * | 1979-10-05 | 1982-10-26 | The Standard Oil Company | Process for the production of pyrrolidones |
| DE3602376A1 (de) * | 1986-01-28 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von (epsilon)-caprolactam |
| DE3602377A1 (de) * | 1986-01-28 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von caprolactam |
| DE3602375A1 (de) * | 1986-01-28 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von (epsilon)-caprolactam |
| DE3643010A1 (de) * | 1986-12-17 | 1988-06-30 | Basf Ag | Verfahren zur herstellung von caprolactam |
-
1988
- 1988-12-24 DE DE3843791A patent/DE3843791A1/de not_active Withdrawn
-
1989
- 1989-11-20 CA CA002003352A patent/CA2003352C/fr not_active Expired - Fee Related
- 1989-12-12 US US07/448,899 patent/US4963672A/en not_active Expired - Lifetime
- 1989-12-19 EP EP89123440A patent/EP0376123B1/fr not_active Expired - Lifetime
- 1989-12-19 DE DE58907777T patent/DE58907777D1/de not_active Expired - Fee Related
- 1989-12-19 ES ES89123440T patent/ES2053940T3/es not_active Expired - Lifetime
- 1989-12-20 JP JP1328565A patent/JP2755749B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE3843791A1 (de) | 1990-07-05 |
| JPH02215768A (ja) | 1990-08-28 |
| ES2053940T3 (es) | 1994-08-01 |
| EP0376123A1 (fr) | 1990-07-04 |
| JP2755749B2 (ja) | 1998-05-25 |
| US4963672A (en) | 1990-10-16 |
| EP0376123B1 (fr) | 1994-06-01 |
| DE58907777D1 (de) | 1994-07-07 |
| CA2003352C (fr) | 1999-05-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |