CA2150949C - Process for the refining of edible oils - Google Patents

Process for the refining of edible oils Download PDF

Info

Publication number: CA2150949C
Authority: CA; Canada
Prior art keywords: oil; heat treatment; acid; temperature; flavour
Prior art date: 1992-12-03
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA002150949A

Other languages

English (en)

French (fr)

Inventor

Josef Petrus Van Dalen

Karel P. A. M. Van Putte

Ronald Frederick Van Slooten

Arend Zwanenburg

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Unilever PLC

Original Assignee

Unilever PLC

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1992-12-03

Filing date

1993-11-16

Publication date

2000-07-18

1993-11-16 Application filed by Unilever PLC filed Critical Unilever PLC

2000-07-18 Application granted granted Critical

2000-07-18 Publication of CA2150949C publication Critical patent/CA2150949C/en

2013-11-16 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 32
238000007670 refining Methods 0.000 title claims abstract description 16
239000008157 edible vegetable oil Substances 0.000 title description 7
239000000796 flavoring agent Substances 0.000 claims abstract description 27
235000019634 flavors Nutrition 0.000 claims abstract description 26
238000010438 heat treatment Methods 0.000 claims abstract description 16
238000011282 treatment Methods 0.000 claims abstract description 16
UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims abstract description 7
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
239000000126 substance Substances 0.000 claims description 15
239000002253 acid Substances 0.000 claims description 11
239000000203 mixture Substances 0.000 claims description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 8
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
239000007789 gas Substances 0.000 claims description 6
239000000654 additive Substances 0.000 claims description 5
230000000996 additive effect Effects 0.000 claims description 5
150000007513 acids Chemical class 0.000 claims description 4
235000021588 free fatty acids Nutrition 0.000 claims description 4
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 4
229910052757 nitrogen Inorganic materials 0.000 claims description 4
BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 2
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
235000011054 acetic acid Nutrition 0.000 claims description 2
BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 2
239000003963 antioxidant agent Substances 0.000 claims description 2
230000003078 antioxidant effect Effects 0.000 claims description 2
235000015165 citric acid Nutrition 0.000 claims description 2
239000000284 extract Substances 0.000 claims description 2
239000004310 lactic acid Substances 0.000 claims description 2
235000014655 lactic acid Nutrition 0.000 claims description 2
239000001630 malic acid Substances 0.000 claims description 2
235000011090 malic acid Nutrition 0.000 claims description 2
238000007254 oxidation reaction Methods 0.000 claims description 2
239000011975 tartaric acid Substances 0.000 claims description 2
235000002906 tartaric acid Nutrition 0.000 claims description 2
235000006708 antioxidants Nutrition 0.000 claims 1
230000003647 oxidation Effects 0.000 claims 1
239000003921 oil Substances 0.000 abstract description 64
235000019198 oils Nutrition 0.000 abstract description 64
235000019482 Palm oil Nutrition 0.000 abstract description 4
235000019486 Sunflower oil Nutrition 0.000 abstract description 4
239000002540 palm oil Substances 0.000 abstract description 4
239000002600 sunflower oil Substances 0.000 abstract description 4
239000004006 olive oil Substances 0.000 abstract description 2
235000008390 olive oil Nutrition 0.000 abstract description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
239000000523 sample Substances 0.000 description 7
239000013074 reference sample Substances 0.000 description 6
238000001914 filtration Methods 0.000 description 4
238000004061 bleaching Methods 0.000 description 3
235000021466 carotenoid Nutrition 0.000 description 3
150000001747 carotenoids Chemical class 0.000 description 3
239000010779 crude oil Substances 0.000 description 3
239000000047 product Substances 0.000 description 3
238000000746 purification Methods 0.000 description 3
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
238000001816 cooling Methods 0.000 description 2
238000000354 decomposition reaction Methods 0.000 description 2
230000003247 decreasing effect Effects 0.000 description 2
238000001035 drying Methods 0.000 description 2
230000000694 effects Effects 0.000 description 2
150000002978 peroxides Chemical class 0.000 description 2
239000007787 solid Substances 0.000 description 2
UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 description 1
241001465754 Metazoa Species 0.000 description 1
241001494479 Pecora Species 0.000 description 1
235000019484 Rapeseed oil Nutrition 0.000 description 1
239000003463 adsorbent Substances 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000001299 aldehydes Chemical class 0.000 description 1
238000007664 blowing Methods 0.000 description 1
150000001746 carotenes Chemical class 0.000 description 1
235000005473 carotenes Nutrition 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 1
238000004332 deodorization Methods 0.000 description 1
230000001877 deodorizing effect Effects 0.000 description 1
230000002542 deteriorative effect Effects 0.000 description 1
239000000839 emulsion Substances 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000008268 mayonnaise Substances 0.000 description 1
235000010746 mayonnaise Nutrition 0.000 description 1
PSGAAPLEWMOORI-PEINSRQWSA-N medroxyprogesterone acetate Chemical compound C([C@@]12C)CC(=O)C=C1[C@@H](C)C[C@@H]1[C@@H]2CC[C@]2(C)[C@@](OC(C)=O)(C(C)=O)CC[C@H]21 PSGAAPLEWMOORI-PEINSRQWSA-N 0.000 description 1
238000005374 membrane filtration Methods 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
230000008447 perception Effects 0.000 description 1
150000003904 phospholipids Chemical class 0.000 description 1
239000004033 plastic Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
235000014059 processed cheese Nutrition 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
239000004307 sodium orthophenyl phenol Substances 0.000 description 1
239000002594 sorbent Substances 0.000 description 1
235000010384 tocopherol Nutrition 0.000 description 1
229960001295 tocopherol Drugs 0.000 description 1
229930003799 tocopherol Natural products 0.000 description 1
239000011732 tocopherol Substances 0.000 description 1
231100000167 toxic agent Toxicity 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 1
238000005406 washing Methods 0.000 description 1
GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
- C11B3/14—Refining fats or fatty oils by distillation with the use of indifferent gases or vapours, e.g. steam
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter

Landscapes

Life Sciences & Earth Sciences (AREA)
Chemical & Material Sciences (AREA)
Microbiology (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Edible Oils And Fats (AREA)
Fats And Perfumes (AREA)

CA002150949A 1992-12-03 1993-11-16 Process for the refining of edible oils Expired - Fee Related CA2150949C (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
EP92203750		1992-12-03
EP92203750.2		1992-12-03
PCT/EP1993/003213 WO1994012596A1 (en)	1992-12-03	1993-11-16	Process for the refining of edible oils

Publications (1)

Publication Number	Publication Date
CA2150949C true CA2150949C (en)	2000-07-18

Family

ID=8211097

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002150949A Expired - Fee Related CA2150949C (en)	1992-12-03	1993-11-16	Process for the refining of edible oils

Country Status (11)

Country	Link
EP (1)	EP0672096B1 (de)
AT (1)	ATE152761T1 (de)
AU (1)	AU672858B2 (de)
CA (1)	CA2150949C (de)
DE (1)	DE69310543T2 (de)
DK (1)	DK0672096T3 (de)
ES (1)	ES2102806T3 (de)
MY (1)	MY131379A (de)
TR (1)	TR28200A (de)
WO (1)	WO1994012596A1 (de)
ZA (1)	ZA938754B (de)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH07247495A (ja) *	1994-03-09	1995-09-26	Fuji Oil Co Ltd	高カロテン含有油脂の製造法
AUPN023994A0 (en) *	1994-12-23	1995-01-27	Stotter, Gail Dawn	A process for deodorising tea tree oil
IT1296002B1 (it) *	1995-04-06	1999-06-03	Paolo Bonazelli	Olio extra-vergine di oliva solidificato in modo da ottenere una elevata espansione volumetrica e relativo procedimento produttivo
WO1996036684A1 (en) *	1995-05-16	1996-11-21	Unilever N.V.	Method for refining an edible oil
WO1996041852A1 (en) *	1995-06-12	1996-12-27	Unilever N.V.	Mild refining of triglyceride oil
BR9813703A (pt)	1997-12-19	2000-10-10	Unilever Nv	Composição de pasta espalhável contendo óleo, e, processos para refinar um azeite de oliveira, e para a manufatura de uma composição alimentìcia.
US6426423B1 (en)	1998-11-20	2002-07-30	I.P. Holdings	Methods for treating phosphatide-containing mixtures
US6423857B1 (en)	1998-11-20	2002-07-23	I.P. Holdings	Methods for recovering fatty acids
US6441209B1 (en)	1998-11-20	2002-08-27	Ip Holdings, L.L.C.	Method for treating organic acid-treated phosphatides
US6844458B2 (en)	1998-11-20	2005-01-18	Ip Holdings, L.L.C.	Vegetable oil refining
US6172248B1 (en) *	1998-11-20	2001-01-09	Ip Holdings, L.L.C.	Methods for refining vegetable oils and byproducts thereof
PT1013753E (pt) *	1998-12-22	2006-06-30	Unilever Nv	Refinacao de um oleo vegetal
US6750359B1 (en)	2001-09-04	2004-06-15	Ip Holdings, L.L.C.	Methods for treating deodorizer distillate
ATE430802T1 (de)	2003-08-21	2009-05-15	Monsanto Technology Llc	Fettsäuredesaturasen aus primula
BRPI0509944A (pt)	2004-04-16	2007-09-25	Monsanto Technology Llc	expressão de dessaturases de ácido graxo em milho
TWI397582B (zh)	2004-11-04	2013-06-01	Monsanto Technology Llc	油組合物之製備方法
US20090300972A1 (en) *	2006-02-28	2009-12-10	Massoud Jalalpoor	Physical Refining Process Using Adsorbent Particles for the Production of Biodiesel Fuel
AU2007226680B2 (en)	2006-03-10	2013-10-24	Monsanto Technology Llc	Soybean seed and oil compositions and methods of making same
WO2009025542A1 (en) *	2008-02-26	2009-02-26	Ruslee Hussain	Improved process of refining crude vegetable oil and animal fats for biodiesel feedstock
US9480271B2 (en)	2009-09-15	2016-11-01	Monsanto Technology Llc	Soybean seed and oil compositions and methods of making same
CN115253780B (zh) *	2022-08-10	2024-01-30	广西壮族自治区林业科学研究院	一种保持茶油原风味的生香设备及方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS51109908A (ja) *	1975-03-22	1976-09-29	Asahi Denka Kogyo Kk	Paamuyunoseiseiho
JPS51109907A (ja) *	1975-03-22	1976-09-29	Asahi Denka Kogyo Kk	Paamuyunoseiseiho
JPS5488904A (en) *	1977-12-27	1979-07-14	Nisshin Oil Mills Ltd:The	Preparation of palm oil
DE3771670D1 (de) *	1986-11-13	1991-08-29	Cambrian Eng Group Ltd	Verfahren zum entschleimen von triglyceridoelen.
AU632272B2 (en) *	1988-03-11	1992-12-24	Malaysian Palm Oil Board	Refining of edible oil
DE3839017A1 (de) *	1988-11-18	1990-05-23	Henkel Kgaa	Verfahren zum destillativen abtrennen unerwuenschter bestandteile natuerlicher fette/oele und ihrer derivate
ES2013206A6 (es) *	1989-06-29	1990-04-16	Espan Carburos Metal	Procedimiento de desodorizacion de aceites y grasas.

1993
- 1993-11-16 AT AT94901805T patent/ATE152761T1/de not_active IP Right Cessation
- 1993-11-16 AU AU56246/94A patent/AU672858B2/en not_active Ceased
- 1993-11-16 EP EP94901805A patent/EP0672096B1/de not_active Expired - Lifetime
- 1993-11-16 DK DK94901805.5T patent/DK0672096T3/da active
- 1993-11-16 ES ES94901805T patent/ES2102806T3/es not_active Expired - Lifetime
- 1993-11-16 CA CA002150949A patent/CA2150949C/en not_active Expired - Fee Related
- 1993-11-16 WO PCT/EP1993/003213 patent/WO1994012596A1/en not_active Ceased
- 1993-11-16 DE DE69310543T patent/DE69310543T2/de not_active Expired - Fee Related
- 1993-11-23 ZA ZA938754A patent/ZA938754B/xx unknown
- 1993-11-30 TR TR01088/93A patent/TR28200A/xx unknown
- 1993-12-01 MY MYPI93002547A patent/MY131379A/en unknown

Also Published As

Publication number	Publication date
DE69310543D1 (de)	1997-06-12
EP0672096A1 (de)	1995-09-20
DE69310543T2 (de)	1997-09-04
MY131379A (en)	2007-08-30
ZA938754B (en)	1995-05-23
WO1994012596A1 (en)	1994-06-09
DK0672096T3 (da)	1997-11-03
ATE152761T1 (de)	1997-05-15
EP0672096B1 (de)	1997-05-07
AU672858B2 (en)	1996-10-17
ES2102806T3 (es)	1997-08-01
AU5624694A (en)	1994-06-22
TR28200A (tr)	1996-02-08

Legal Events

Date	Code	Title	Description
1995-08-23	EEER	Examination request
2010-11-16	MKLA	Lapsed

Publication	Publication Date	Title
CA2150949C (en)	2000-07-18	Process for the refining of edible oils
US5696278A (en)	1997-12-09	Degumming of crude glyceride oils not exposed to prior enzymatic activity
EP1171555B1 (de)	2004-06-16	Verfahren zur entfernung freier fettsäuren aus fetten und ölen biologischen ursprungs oder deren dämpferkondensaten
CA1340533C (en)	1999-05-11	Marine/vegetable oil blend and products made therefrom
US5315021A (en)	1994-05-24	Process for removing chlorophyll color impurities from vegetable oils
EP0833882B1 (de)	2002-01-16	Schonendes raffinieren von triglyceridölen
JP2676043B2 (ja)	1997-11-12	シリカヒドロゲルを用いるグリセリド油の精製方法
JPS63191899A (ja)	1988-08-09	トリグリセリド油の脱ガム化方法
US5492709A (en)	1996-02-20	Process for protecting a fat against oxidation
US5585130A (en)	1996-12-17	Concentration of antioxidants in fats
CA2052046A1 (en)	1992-03-26	Process for refining glyceride oil
EP0116408A2 (de)	1984-08-22	Raffinieren von Triglycerid-Ölen in Anwesenheit von Alkalimetall-Borhydriden
GB2241503A (en)	1991-09-04	Edible fatty composition containing bleached fish oils
WO1996036684A1 (en)	1996-11-21	Method for refining an edible oil
US5449797A (en)	1995-09-12	Process for the removal of soap from glyceride oils and/or wax esters using an amorphous adsorbent
US5210242A (en)	1993-05-11	Process for soap splitting using a high temperature treatment
JPH07197076A (ja)	1995-08-01	食用植物原油の精製法
CN111683537A (zh)	2020-09-18	无不需要的污染物的棕榈油
RU2784487C2 (ru)	2022-11-28	Пальмовое масло без нежелательных загрязнителей
JPH07197075A (ja)	1995-08-01	食用植物原油の精製法
Martincic et al.	2001	Separation processes in oil refining technology