CA2183774A1 - Procede de cristallisation de substances chimiques - Google Patents
Procede de cristallisation de substances chimiquesInfo
- Publication number
- CA2183774A1 CA2183774A1 CA002183774A CA2183774A CA2183774A1 CA 2183774 A1 CA2183774 A1 CA 2183774A1 CA 002183774 A CA002183774 A CA 002183774A CA 2183774 A CA2183774 A CA 2183774A CA 2183774 A1 CA2183774 A1 CA 2183774A1
- Authority
- CA
- Canada
- Prior art keywords
- particles
- container
- molten mass
- process according
- molten
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000000034 method Methods 0.000 title claims abstract description 50
- 238000002425 crystallisation Methods 0.000 title claims abstract description 10
- 239000000126 substance Substances 0.000 title claims abstract description 9
- 239000002245 particle Substances 0.000 claims abstract description 54
- 239000007787 solid Substances 0.000 claims abstract description 6
- 238000000605 extraction Methods 0.000 claims abstract description 3
- 230000008025 crystallization Effects 0.000 claims description 8
- 238000000746 purification Methods 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- 238000009792 diffusion process Methods 0.000 claims description 2
- 238000000151 deposition Methods 0.000 claims 1
- 238000007711 solidification Methods 0.000 claims 1
- 230000008023 solidification Effects 0.000 claims 1
- 239000003337 fertilizer Substances 0.000 abstract description 4
- 239000013078 crystal Substances 0.000 description 11
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 239000012297 crystallization seed Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- 229920006254 polymer film Polymers 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Fertilizers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
- Glanulating (AREA)
Abstract
Selon un procédé de cristallisation de substances chimiques, celles-ci sont d'abord fondues et introduites dans un récipient dans lequel elles se cristallisent par extraction de chaleur, puis traversent le récipient et sont prélevées sous forme d'un produit. Le procédé se caractérise en ce que l'on répartit uniformément dans le récipient de petites particules, notamment de la même taille, au moins en partie solides. La masse fondue se cristallise sur ces particules pendant qu'elles sont transportées à travers le récipient. L'invention sert à produire des engrais en pastilles.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP4445880.0 | 1994-12-22 | ||
| DE4445880A DE4445880A1 (de) | 1994-12-22 | 1994-12-22 | Verfahren zum Reinigen chemischer Substanzen |
| DE19507316A DE19507316A1 (de) | 1994-12-22 | 1995-03-02 | Verfahren zur Kristallisation chemischer Substanzen |
| DE19507316.9 | 1995-03-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2183774A1 true CA2183774A1 (fr) | 1996-06-27 |
Family
ID=25943149
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002183774A Abandoned CA2183774A1 (fr) | 1994-12-22 | 1995-11-30 | Procede de cristallisation de substances chimiques |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP0746535A1 (fr) |
| JP (1) | JPH10500066A (fr) |
| KR (1) | KR970701162A (fr) |
| AU (1) | AU4300596A (fr) |
| CA (1) | CA2183774A1 (fr) |
| DE (1) | DE19507316A1 (fr) |
| WO (1) | WO1996019421A1 (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6242639B1 (en) | 1996-09-13 | 2001-06-05 | Basf Aktiengesellschaft | Preparation of neopentyl glycol hydroxyprivalate granules |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2006237137B8 (en) * | 2005-04-18 | 2011-12-22 | Stamicarbon B.V. | Process for the production of urea-comprising particles |
| US7985393B2 (en) * | 2009-03-31 | 2011-07-26 | Uop Llc | Pastillation of ammonium sulfate nitrate |
| CN111558332A (zh) * | 2020-03-27 | 2020-08-21 | 浙江三圣科技有限公司 | 一种大颗粒复合肥造粒成型装置 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1592796B2 (de) * | 1963-05-22 | 1973-04-26 | Verenigde Kunstmestfabneken Mekog Albatros N V , Utrecht (Niederlande) | Duengemittel mit einem ueberzug aus kohlenwasserstoffen |
| DE1792150A1 (de) * | 1968-07-27 | 1971-10-14 | Chemie Appbau Mainz Schmahl & | Verfahren zur Herstellung von schwefelhaltigen Duengemittel-Granulaten mit einer harten,abriebfesten Oberflaechenschicht |
| DE1941460C3 (de) * | 1969-08-14 | 1973-10-04 | Gebr. Kaiser, 4150 Krefeld-Uerdingen | Verfahren und Vorrichtung zur Er zeugung von Granalien aus einer in einer in einer Schmelzgutwanne befindlichen Schmelze |
| US4857098A (en) * | 1987-08-11 | 1989-08-15 | Pursell Industries | Sulfur-coated fertilizer granules and process of making same |
-
1995
- 1995-03-02 DE DE19507316A patent/DE19507316A1/de not_active Ceased
- 1995-11-30 AU AU43005/96A patent/AU4300596A/en not_active Abandoned
- 1995-11-30 KR KR1019960704587A patent/KR970701162A/ko not_active Ceased
- 1995-11-30 JP JP8519454A patent/JPH10500066A/ja active Pending
- 1995-11-30 EP EP95941633A patent/EP0746535A1/fr not_active Withdrawn
- 1995-11-30 CA CA002183774A patent/CA2183774A1/fr not_active Abandoned
- 1995-11-30 WO PCT/EP1995/004708 patent/WO1996019421A1/fr not_active Ceased
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6242639B1 (en) | 1996-09-13 | 2001-06-05 | Basf Aktiengesellschaft | Preparation of neopentyl glycol hydroxyprivalate granules |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH10500066A (ja) | 1998-01-06 |
| KR970701162A (ko) | 1997-03-17 |
| AU4300596A (en) | 1996-07-10 |
| EP0746535A1 (fr) | 1996-12-11 |
| WO1996019421A1 (fr) | 1996-06-27 |
| DE19507316A1 (de) | 1996-09-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| FZDE | Dead |