CA2306157A1 - Preparation of dihydroxydiphenyl-copolycarbonates by melt re-esterification - Google Patents

Preparation of dihydroxydiphenyl-copolycarbonates by melt re-esterification Download PDF

Info

Publication number: CA2306157A1
Authority: CA; Canada
Prior art keywords: mol; alkyl; copolycarbonates; preparation; accordance
Prior art date: 1997-10-10
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Abandoned

Application number

CA002306157A

Other languages

English (en)

French (fr)

Inventor

Annett Konig

Rolf Wehrmann

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Bayer AG

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1997-10-10

Filing date

1998-09-30

Publication date

1999-04-22

1998-09-30 Application filed by Individual filed Critical Individual

1999-04-22 Publication of CA2306157A1 publication Critical patent/CA2306157A1/en

Status Abandoned legal-status Critical Current

Links

238000002360 preparation method Methods 0.000 title claims abstract description 11
238000005886 esterification reaction Methods 0.000 title 1
238000000034 method Methods 0.000 claims abstract description 21
239000004417 polycarbonate Substances 0.000 claims abstract description 18
229920000515 polycarbonate Polymers 0.000 claims abstract description 18
239000003054 catalyst Substances 0.000 claims abstract description 9
239000000155 melt Substances 0.000 claims abstract description 4
150000002780 morpholines Chemical class 0.000 claims abstract description 3
150000003053 piperidines Chemical class 0.000 claims abstract description 3
239000000126 substance Substances 0.000 claims description 5
XKZQKPRCPNGNFR-UHFFFAOYSA-N 2-(3-hydroxyphenyl)phenol Chemical compound OC1=CC=CC(C=2C(=CC=CC=2)O)=C1 XKZQKPRCPNGNFR-UHFFFAOYSA-N 0.000 claims description 4
HTLZVHNRZJPSMI-UHFFFAOYSA-N N-ethylpiperidine Chemical compound CCN1CCCCC1 HTLZVHNRZJPSMI-UHFFFAOYSA-N 0.000 claims description 4
125000001118 alkylidene group Chemical group 0.000 claims description 4
230000000295 complement effect Effects 0.000 claims description 2
125000002993 cycloalkylene group Chemical group 0.000 claims description 2
238000004128 high performance liquid chromatography Methods 0.000 claims description 2
238000004519 manufacturing process Methods 0.000 claims description 2
238000007127 saponification reaction Methods 0.000 claims description 2
229920001169 thermoplastic Polymers 0.000 claims description 2
239000004416 thermosoftening plastic Substances 0.000 claims description 2
125000006273 (C1-C3) alkyl group Chemical group 0.000 claims 1
125000006833 (C1-C5) alkylene group Chemical group 0.000 claims 1
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 11
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 9
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
-1 alkyl phosphites Chemical class 0.000 description 6
150000005690 diesters Chemical class 0.000 description 5
239000000203 mixture Substances 0.000 description 5
RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 description 4
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
NHTMVDHEPJAVLT-UHFFFAOYSA-N Isooctane Chemical compound CC(C)CC(C)(C)C NHTMVDHEPJAVLT-UHFFFAOYSA-N 0.000 description 4
239000003513 alkali Substances 0.000 description 4
125000000217 alkyl group Chemical group 0.000 description 4
229910052799 carbon Inorganic materials 0.000 description 4
JVSWJIKNEAIKJW-UHFFFAOYSA-N dimethyl-hexane Natural products CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 description 4
239000000835 fiber Substances 0.000 description 4
239000000463 material Substances 0.000 description 4
YCWSUKQGVSGXJO-NTUHNPAUSA-N nifuroxazide Chemical group C1=CC(O)=CC=C1C(=O)N\N=C\C1=CC=C([N+]([O-])=O)O1 YCWSUKQGVSGXJO-NTUHNPAUSA-N 0.000 description 4
239000000243 solution Substances 0.000 description 4
238000006243 chemical reaction Methods 0.000 description 3
150000002500 ions Chemical class 0.000 description 3
238000005809 transesterification reaction Methods 0.000 description 3
229910019142 PO4 Inorganic materials 0.000 description 2
238000000149 argon plasma sintering Methods 0.000 description 2
YXVFYQXJAXKLAK-UHFFFAOYSA-N biphenyl-4-ol Chemical compound C1=CC(O)=CC=C1C1=CC=CC=C1 YXVFYQXJAXKLAK-UHFFFAOYSA-N 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
238000009833 condensation Methods 0.000 description 2
230000005494 condensation Effects 0.000 description 2
ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 2
238000001746 injection moulding Methods 0.000 description 2
230000016507 interphase Effects 0.000 description 2
238000002955 isolation Methods 0.000 description 2
229910052757 nitrogen Inorganic materials 0.000 description 2
150000002989 phenols Chemical class 0.000 description 2
229910000064 phosphane Inorganic materials 0.000 description 2
235000021317 phosphate Nutrition 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
230000035882 stress Effects 0.000 description 2
238000009864 tensile test Methods 0.000 description 2
KXIXHISTUVHOCY-UHFFFAOYSA-N 1-propan-2-ylpiperidine Chemical compound CC(C)N1CCCCC1 KXIXHISTUVHOCY-UHFFFAOYSA-N 0.000 description 1
VTDIWMPYBAVEDY-UHFFFAOYSA-N 1-propylpiperidine Chemical compound CCCN1CCCCC1 VTDIWMPYBAVEDY-UHFFFAOYSA-N 0.000 description 1
CJWNFAKWHDOUKL-UHFFFAOYSA-N 2-(2-phenylpropan-2-yl)phenol Chemical compound C=1C=CC=C(O)C=1C(C)(C)C1=CC=CC=C1 CJWNFAKWHDOUKL-UHFFFAOYSA-N 0.000 description 1
AUNGWUPUJSKFFU-UHFFFAOYSA-N 4-[1-(4-hydroxyphenyl)-3,5,5-trimethylcyclohex-3-en-1-yl]phenol Chemical compound OC1=CC=C(C=C1)C1(CC(C=C(C1)C)(C)C)C1=CC=C(C=C1)O AUNGWUPUJSKFFU-UHFFFAOYSA-N 0.000 description 1
HVCNXQOWACZAFN-UHFFFAOYSA-N 4-ethylmorpholine Chemical compound CCN1CCOCC1 HVCNXQOWACZAFN-UHFFFAOYSA-N 0.000 description 1
XLZMWNWNBXSZKF-UHFFFAOYSA-N 4-propan-2-ylmorpholine Chemical compound CC(C)N1CCOCC1 XLZMWNWNBXSZKF-UHFFFAOYSA-N 0.000 description 1
NMILGIZTAZXMTM-UHFFFAOYSA-N 4-propylmorpholine Chemical compound CCCN1CCOCC1 NMILGIZTAZXMTM-UHFFFAOYSA-N 0.000 description 1
229930185605 Bisphenol Natural products 0.000 description 1
VOWWYDCFAISREI-UHFFFAOYSA-N Bisphenol AP Chemical compound C=1C=C(O)C=CC=1C(C=1C=CC(O)=CC=1)(C)C1=CC=CC=C1 VOWWYDCFAISREI-UHFFFAOYSA-N 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
230000032683 aging Effects 0.000 description 1
229910001854 alkali hydroxide Inorganic materials 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
229910001413 alkali metal ion Inorganic materials 0.000 description 1
150000001447 alkali salts Chemical class 0.000 description 1
229910001420 alkaline earth metal ion Inorganic materials 0.000 description 1
125000002947 alkylene group Chemical group 0.000 description 1
150000003863 ammonium salts Chemical class 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
239000002585 base Substances 0.000 description 1
230000005540 biological transmission Effects 0.000 description 1
125000006267 biphenyl group Chemical group 0.000 description 1
VCCBEIPGXKNHFW-UHFFFAOYSA-N biphenyl-4,4'-diol Chemical group C1=CC(O)=CC=C1C1=CC=C(O)C=C1 VCCBEIPGXKNHFW-UHFFFAOYSA-N 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
238000005336 cracking Methods 0.000 description 1
238000013500 data storage Methods 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
238000001125 extrusion Methods 0.000 description 1
239000002657 fibrous material Substances 0.000 description 1
238000011010 flushing procedure Methods 0.000 description 1
239000003365 glass fiber Substances 0.000 description 1
150000002366 halogen compounds Chemical class 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
239000013067 intermediate product Substances 0.000 description 1
238000011068 loading method Methods 0.000 description 1
239000011707 mineral Substances 0.000 description 1
125000000896 monocarboxylic acid group Chemical group 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
239000000049 pigment Substances 0.000 description 1
238000006068 polycondensation reaction Methods 0.000 description 1
229920000098 polyolefin Polymers 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
229920002635 polyurethane Polymers 0.000 description 1
239000004814 polyurethane Substances 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000011814 protection agent Substances 0.000 description 1
239000010453 quartz Substances 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
239000012779 reinforcing material Substances 0.000 description 1
238000010517 secondary reaction Methods 0.000 description 1
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
239000003381 stabilizer Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/04—Aromatic polycarbonates
- C08G64/06—Aromatic polycarbonates not containing aliphatic unsaturation
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
- C08G64/307—General preparatory processes using carbonates and phenols

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Polyesters Or Polycarbonates (AREA)
Compositions Of Macromolecular Compounds (AREA)

CA002306157A 1997-10-10 1998-09-30 Preparation of dihydroxydiphenyl-copolycarbonates by melt re-esterification Abandoned CA2306157A1 (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DE19744693A DE19744693A1 (de)	1997-10-10	1997-10-10	Verfahren zur Herstellung von speziellen Copolycarbonaten durch Schmelzumesterung
DE19744693.0		1997-10-10
PCT/EP1998/006212 WO1999019380A1 (de)	1997-10-10	1998-09-30	Herstellung von dihydroxydiphenyl-copolycarbonaten durch schmelzumesterung

Publications (1)

Publication Number	Publication Date
CA2306157A1 true CA2306157A1 (en)	1999-04-22

Family

ID=7845093

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002306157A Abandoned CA2306157A1 (en)	1997-10-10	1998-09-30	Preparation of dihydroxydiphenyl-copolycarbonates by melt re-esterification

Country Status (13)

Country	Link
EP (1)	EP1023357A1 (id)
JP (1)	JP2001520242A (id)
KR (1)	KR20010031016A (id)
CN (1)	CN1266442A (id)
AU (1)	AU9541798A (id)
BR (1)	BR9812888A (id)
CA (1)	CA2306157A1 (id)
DE (1)	DE19744693A1 (id)
ID (1)	ID24573A (id)
IL (1)	IL135003A0 (id)
NO (1)	NO20001167L (id)
TW (1)	TW426704B (id)
WO (1)	WO1999019380A1 (id)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6740714B2 (en) *	2001-07-20	2004-05-25	Bayer Aktiengesellschaft	Polycarbonate blends

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2004510025A (ja) *	2000-09-26	2004-04-02	バイエル　アクチェンゲゼルシャフト	コポリカーボネート組成物、その使用およびそれを含有する成形部品
JP2002114841A (ja) *	2000-10-06	2002-04-16	Mitsui Chemicals Inc	光学部品
JP2002114842A (ja) *	2000-10-06	2002-04-16	Mitsui Chemicals Inc	ポリカーボネート樹脂、及びそれを含んで構成される光学部品
JP4514080B2 (ja) *	2000-12-28	2010-07-28	三井化学株式会社	ポリカーボネート樹脂組成物、及びそれを含んで構成される光学部品
US6608163B2 (en)	2001-01-17	2003-08-19	General Electric Company	Polycarbonate copolymers having improved hydrolytic stability
US7183371B2 (en) *	2004-11-01	2007-02-27	General Electric Company	Method for making polycarbonate
CN102464545A (zh)	2010-11-11	2012-05-23	中国石油天然气股份有限公司	一种乙烯齐聚制备1-辛烯的方法
TWI693244B (zh) *	2015-01-20	2020-05-11	德商科思創德意志股份有限公司	藉由轉酯化方法製備高耐熱之［共］聚碳酸酯
WO2023149329A1 (ja) *	2022-02-07	2023-08-10	三菱ケミカル株式会社	ポリカーボネート樹脂組成物

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2735775A1 (de) *	1977-08-09	1979-02-22	Bayer Ag	Verfahren zur herstellung von polycarbonaten
JPS61264020A (ja) *	1985-05-17	1986-11-21	Idemitsu Kosan Co Ltd	芳香族ポリカ−ボネ−トおよびその製造方法
DE3919046A1 (de) *	1989-06-10	1990-12-20	Bayer Ag	Neue thermotrope polycarbonate, verfahren zu ihrer herstellung und ihre verwendung zur herstellung von formkoerpern, filamenten, fasern und folien
JPH05117382A (ja) *	1991-10-29	1993-05-14	Nippon G Ii Plast Kk	共重合ポリカーボネート、その製造方法およびそれからなる組成物
US5475079A (en) *	1993-04-28	1995-12-12	Daicel Chemical Industries, Ltd.	(CO) polycarbonate composition and process for preparing the same
JPH08165341A (ja) *	1994-12-15	1996-06-25	Idemitsu Kosan Co Ltd	ポリカーボネートの製造方法

1997
- 1997-10-10 DE DE19744693A patent/DE19744693A1/de not_active Withdrawn
1998
- 1998-09-21 TW TW087115670A patent/TW426704B/zh not_active IP Right Cessation
- 1998-09-30 EP EP98948996A patent/EP1023357A1/de not_active Withdrawn
- 1998-09-30 KR KR1020007003823A patent/KR20010031016A/ko not_active Withdrawn
- 1998-09-30 WO PCT/EP1998/006212 patent/WO1999019380A1/de not_active Ceased
- 1998-09-30 IL IL13500398A patent/IL135003A0/xx unknown
- 1998-09-30 AU AU95417/98A patent/AU9541798A/en not_active Abandoned
- 1998-09-30 BR BR9812888-4A patent/BR9812888A/pt not_active IP Right Cessation
- 1998-09-30 JP JP2000515948A patent/JP2001520242A/ja active Pending
- 1998-09-30 CN CN98808044A patent/CN1266442A/zh active Pending
- 1998-09-30 CA CA002306157A patent/CA2306157A1/en not_active Abandoned
- 1998-09-30 ID IDW20000622D patent/ID24573A/id unknown
2000
- 2000-03-07 NO NO20001167A patent/NO20001167L/no not_active Application Discontinuation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6740714B2 (en) *	2001-07-20	2004-05-25	Bayer Aktiengesellschaft	Polycarbonate blends

Also Published As

Publication number	Publication date
JP2001520242A (ja)	2001-10-30
ID24573A (id)	2000-07-27
NO20001167D0 (no)	2000-03-07
NO20001167L (no)	2000-03-07
TW426704B (en)	2001-03-21
IL135003A0 (en)	2001-05-20
EP1023357A1 (de)	2000-08-02
WO1999019380A1 (de)	1999-04-22
DE19744693A1 (de)	1999-04-15
KR20010031016A (ko)	2001-04-16
AU9541798A (en)	1999-05-03
CN1266442A (zh)	2000-09-13
BR9812888A (pt)	2000-08-08

Legal Events

Date	Code	Title	Description
2003-09-30	FZDE	Discontinued

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US6066700A (en)	2000-05-23	Process for the production of polysiloxane/polycarbonate block co-condensation products
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EP0351168A2 (en)	1990-01-17	Process for preparing polycarbonates
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KR101690835B1 (ko)	2016-12-28	디올 단량체, 이의 폴리카보네이트 및 이를 포함하는 물품
KR20010031016A (ko)	2001-04-16	용융 재에스테르화 반응을 통한디히드록시디페닐-코폴리카르보네이트의 제조방법
WO1996029366A1 (en)	1996-09-26	Blends of diaryl fluorene carbonate polymers with bisphenol a carbonate polymers
EP3825344B1 (en)	2022-06-08	Copolycarbonate, and polycarbonate composition comprising same
JPH0578469A (ja)	1993-03-30	ポリカーボネートの製造方法
US6222004B1 (en)	2001-04-24	Branched polycarbonate resin
EP1521806B1 (en)	2008-01-09	Thermoplastic polycarbonate compositions having high toughness
NL1007516C2 (nl)	1998-11-25	Werkwijze voor de bereiding van speciale copolycarbonaten door omestering in de smelt.
KR101735888B1 (ko)	2017-05-15	디올계 화합물, 이의 폴리카보네이트 및 이를 포함하는 물품
US5618906A (en)	1997-04-08	Process for the production of thermoplastic polycarbonates
KR102432074B1 (ko)	2022-08-16	폴리에스테르 올리고머 및 그 제조방법, 및 이 올리고머를 포함하는 내스크래치성이 향상된 폴리에스테르-폴리카보네이트 블록 공중합체 및 그 제조방법
US20040230024A1 (en)	2004-11-18	Polycarbonate resin
MXPA00003439A (en)	2001-05-07	Preparation of dihydroxydiphenyl-copolycarbonates by melt re-esterification
HK1030615A (en)	2001-05-11	Preparation of dihydroxydiphenyl-copolycarbonates by meltre-esterification

CA2306157A1 - Preparation of dihydroxydiphenyl-copolycarbonates by melt re-esterification - Google Patents

Info

Links

Classifications

Landscapes

Applications Claiming Priority (3)

Publications (1)

Family

ID=7845093

Family Applications (1)

Country Status (13)

Cited By (1)

Families Citing this family (9)

Family Cites Families (6)

Cited By (1)

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