CA2307137A1 - Procede de fabrication de preformes en fibres de carbone - Google Patents
Procede de fabrication de preformes en fibres de carbone Download PDFInfo
- Publication number
- CA2307137A1 CA2307137A1 CA002307137A CA2307137A CA2307137A1 CA 2307137 A1 CA2307137 A1 CA 2307137A1 CA 002307137 A CA002307137 A CA 002307137A CA 2307137 A CA2307137 A CA 2307137A CA 2307137 A1 CA2307137 A1 CA 2307137A1
- Authority
- CA
- Canada
- Prior art keywords
- yarn
- tow
- yarns
- fibers
- carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 77
- 238000000034 method Methods 0.000 title claims abstract description 38
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 34
- 238000003763 carbonization Methods 0.000 claims abstract description 37
- 238000005336 cracking Methods 0.000 claims abstract description 20
- 239000007833 carbon precursor Substances 0.000 claims abstract description 12
- 230000009466 transformation Effects 0.000 claims abstract description 11
- 239000002243 precursor Substances 0.000 claims description 23
- 238000010438 heat treatment Methods 0.000 claims description 20
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 19
- 239000004917 carbon fiber Substances 0.000 claims description 19
- 229920002239 polyacrylonitrile Polymers 0.000 claims description 12
- 239000002131 composite material Substances 0.000 claims description 8
- 238000009941 weaving Methods 0.000 claims description 8
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 5
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 3
- 229920002678 cellulose Polymers 0.000 claims description 3
- 239000001913 cellulose Substances 0.000 claims description 3
- 239000012700 ceramic precursor Substances 0.000 claims description 3
- 238000007669 thermal treatment Methods 0.000 abstract 1
- 239000004744 fabric Substances 0.000 description 8
- 239000004753 textile Substances 0.000 description 6
- 229920000742 Cotton Polymers 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000012535 impurity Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 238000009434 installation Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000011295 pitch Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 230000001131 transforming effect Effects 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000011337 anisotropic pitch Substances 0.000 description 1
- 238000010000 carbonizing Methods 0.000 description 1
- 230000001427 coherent effect Effects 0.000 description 1
- 210000001520 comb Anatomy 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 230000001066 destructive effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 239000002296 pyrolytic carbon Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16D—COUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
- F16D69/00—Friction linings; Attachment thereof; Selection of coacting friction substances or surfaces
- F16D69/02—Composition of linings ; Methods of manufacturing
- F16D69/023—Composite materials containing carbon and carbon fibres or fibres made of carbonizable material
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
- C04B35/83—Carbon fibres in a carbon matrix
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
- D01F11/14—Chemical after-treatment of artificial filaments or the like during manufacture of carbon with organic compounds, e.g. macromolecular compounds
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G1/00—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics
- D02G1/02—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics by twisting, fixing the twist and backtwisting, i.e. by imparting false twist
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J1/00—Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
- D02J1/22—Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
- D02J1/222—Stretching in a gaseous atmosphere or in a fluid bed
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J13/00—Heating or cooling the yarn, thread, cord, rope, or the like, not specific to any one of the processes provided for in this subclass
- D02J13/001—Heating or cooling the yarn, thread, cord, rope, or the like, not specific to any one of the processes provided for in this subclass in a tube or vessel
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H13/00—Other non-woven fabrics
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/002—Inorganic yarns or filaments
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/10—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically
- D04H3/105—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically by needling
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Composite Materials (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Fibers (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Woven Fabrics (AREA)
Abstract
Pour fabriquer une préforme en fibres de carbone, on utilise au moins un fil ou câble formé de fibres continues issues de fibres de précurseur de carbone ayant subi une carbonisation intermédiaire telle que les fibres ont un taux de carbone compris entre 70 % et 90 % et présenteront une résistance à une rupture en traction au moins égale à 3 000 MPa après que leur carbonisation ait été complétée sans nécessairement être mises en tension, et on utilise le fil ou câble légèrement retordu pour fabriquer la préforme, avant de soumettre celle-ci à un traitement thermique afin de compléter la transformation des fibres discontinues en fibres de carbone. Le fil ou câble de départ peut être soumis à une opération d'étirage-craquage de manière à obtenir un fil ou câble formé de fibres discontinues dont la cohésion nécessaire est assurée par une légère retorsion, ou par guipage.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR97/13424 | 1997-10-27 | ||
| FR9713424A FR2770233B1 (fr) | 1997-10-27 | 1997-10-27 | Procede de fabrication de preformes en fibres de carbone |
| PCT/FR1998/002298 WO1999022052A1 (fr) | 1997-10-27 | 1998-10-27 | Procede de fabrication de preformes en fibres de carbone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2307137A1 true CA2307137A1 (fr) | 1999-05-06 |
Family
ID=9512669
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002307137A Abandoned CA2307137A1 (fr) | 1997-10-27 | 1998-10-27 | Procede de fabrication de preformes en fibres de carbone |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP1025295A1 (fr) |
| JP (1) | JP2001521073A (fr) |
| CN (1) | CN1092723C (fr) |
| CA (1) | CA2307137A1 (fr) |
| FR (1) | FR2770233B1 (fr) |
| WO (1) | WO1999022052A1 (fr) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2842192B1 (fr) * | 2002-07-12 | 2004-10-01 | Snecma Propulsion Solide | Procede et installation pour l'obtention de produits en carbone a partir de produits en precurseur de carbone |
| US6783851B2 (en) * | 2002-08-07 | 2004-08-31 | Albany International Techniweave, Inc. | Pitch based graphite fabrics and needled punched felts for fuel cell gas diffusion layer substrates and high thermal conductivity reinforced composites |
| ES2373640T3 (es) * | 2007-06-12 | 2012-02-07 | Hexcel Reinforcements | Procedimiento de fabricación de un material compuesto en el que al menos se coloca un hilo retorcido y el material compuesto que se obtiene de este modo. |
| CN101245503B (zh) * | 2008-03-01 | 2011-07-27 | 威海拓展纤维有限公司 | 碳纤维的生产方法 |
| FR2953826B1 (fr) * | 2009-12-16 | 2019-10-11 | Safran Landing Systems | Procede de fabrication d'une piece de friction a base de materiau composite c/c |
| CN102041597B (zh) * | 2010-11-16 | 2012-08-08 | 江苏澳盛复合材料科技有限公司 | 一种碳纤维布及其在汽车耐摩擦部件上的应用 |
| CN103274714B (zh) * | 2013-06-05 | 2014-09-17 | 东南大学 | 一种改进的二维陶瓷基复合材料Z-pin方法 |
| FR3025810B1 (fr) * | 2014-09-12 | 2016-12-09 | Herakles | Procede de fabrication d'une structure fibreuse |
| JP6607026B2 (ja) * | 2015-12-22 | 2019-11-20 | 株式会社豊田自動織機 | 繊維強化複合材 |
| WO2017207068A1 (fr) * | 2016-06-03 | 2017-12-07 | Schunk Kohlenstofftechnik Gmbh | Procédé de production d'une plaque de support et plaque de support |
| CN110616493B (zh) * | 2019-09-23 | 2021-09-10 | 潘魏豪 | 一种柔性导电碳布的制造方法 |
| CN111455522A (zh) * | 2020-04-02 | 2020-07-28 | 广州蓝墨科技有限公司 | 一种抗静电面料的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4728395A (en) * | 1984-10-12 | 1988-03-01 | Stackpole Fibers Company, Inc. | Controlled resistivity carbon fiber paper and fabric sheet products and method of manufacture |
| CA1327258C (fr) * | 1988-02-16 | 1994-03-01 | James Toner Paul Jr. | Procede pour l'obtention de fibres de carbone pre-etirees |
| CN2057177U (zh) * | 1989-05-04 | 1990-05-16 | 中国科学院山西煤炭化学研究所 | 预氧化纤维生产装置 |
| FR2669940B1 (fr) * | 1990-12-03 | 1994-10-21 | Europ Propulsion | Fil forme a partir de fibres refractaires ou de leurs precurseurs et son application a la fabrication de pieces en materiau composite. |
| GB9122997D0 (en) * | 1991-10-30 | 1991-12-18 | Curran Dennis J G | Ceramic fibres |
-
1997
- 1997-10-27 FR FR9713424A patent/FR2770233B1/fr not_active Expired - Fee Related
-
1998
- 1998-10-27 JP JP2000518137A patent/JP2001521073A/ja active Pending
- 1998-10-27 CN CN98810543A patent/CN1092723C/zh not_active Expired - Fee Related
- 1998-10-27 WO PCT/FR1998/002298 patent/WO1999022052A1/fr not_active Ceased
- 1998-10-27 EP EP98952798A patent/EP1025295A1/fr not_active Withdrawn
- 1998-10-27 CA CA002307137A patent/CA2307137A1/fr not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP1025295A1 (fr) | 2000-08-09 |
| FR2770233A1 (fr) | 1999-04-30 |
| WO1999022052A1 (fr) | 1999-05-06 |
| CN1092723C (zh) | 2002-10-16 |
| FR2770233B1 (fr) | 2000-01-14 |
| CN1277642A (zh) | 2000-12-20 |
| JP2001521073A (ja) | 2001-11-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Dead |