CA2308932A1 - Processus de production de granules d'agent de surface - Google Patents

Processus de production de granules d'agent de surface Download PDF

Info

Publication number: CA2308932A1
Authority: CA; Canada
Prior art keywords: granules; acid; surfactant; surfactants; zeolite
Prior art date: 1999-05-22
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Abandoned

Application number

CA 2308932

Other languages

English (en)

Inventor

Keiwan Ebrahimzadeh

Andreas Lietzmann

Kathleen Paatz

Wilfried Raehse

Markus Semrau

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Henkel AG and Co KGaA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1999-05-22

Filing date

2000-05-18

Publication date

2000-11-22

2000-05-18 Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA

2000-11-22 Publication of CA2308932A1 publication Critical patent/CA2308932A1/fr

Status Abandoned legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 56
239000008187 granular material Substances 0.000 title claims abstract description 42
239000004094 surface-active agent Substances 0.000 title claims abstract description 25
238000004519 manufacturing process Methods 0.000 title claims abstract description 16
239000000203 mixture Substances 0.000 claims abstract description 48
239000003599 detergent Substances 0.000 claims abstract description 31
239000002736 nonionic surfactant Substances 0.000 claims abstract description 27
239000007788 liquid Substances 0.000 claims abstract description 18
239000004615 ingredient Substances 0.000 claims abstract description 11
229920001515 polyalkylene glycol Polymers 0.000 claims abstract description 9
239000007787 solid Substances 0.000 claims abstract description 8
239000002904 solvent Substances 0.000 claims abstract description 8
239000010457 zeolite Substances 0.000 claims description 41
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 29
239000002253 acid Substances 0.000 claims description 24
229910021536 Zeolite Inorganic materials 0.000 claims description 23
150000003839 salts Chemical class 0.000 claims description 19
150000007513 acids Chemical class 0.000 claims description 14
239000012013 faujasite Substances 0.000 claims description 14
150000004760 silicates Chemical class 0.000 claims description 13
238000010521 absorption reaction Methods 0.000 claims description 12
239000000843 powder Substances 0.000 claims description 9
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
239000002202 Polyethylene glycol Substances 0.000 claims description 7
239000007844 bleaching agent Substances 0.000 claims description 7
229920001223 polyethylene glycol Polymers 0.000 claims description 7
125000004432 carbon atom Chemical group C* 0.000 claims description 6
239000003112 inhibitor Substances 0.000 claims description 6
239000003945 anionic surfactant Substances 0.000 claims description 4
102000004190 Enzymes Human genes 0.000 claims description 3
108090000790 Enzymes Proteins 0.000 claims description 3
239000012190 activator Substances 0.000 claims description 3
239000006260 foam Substances 0.000 claims description 3
238000002156 mixing Methods 0.000 claims description 3
230000003287 optical effect Effects 0.000 claims description 3
229910019142 PO4 Inorganic materials 0.000 claims description 2
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 2
235000021317 phosphate Nutrition 0.000 claims description 2
150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 2
150000003138 primary alcohols Chemical class 0.000 claims description 2
125000002947 alkylene group Chemical group 0.000 claims 1
239000002245 particle Substances 0.000 abstract description 17
238000001228 spectrum Methods 0.000 abstract description 3
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 19
239000000047 product Substances 0.000 description 18
-1 alkyl poly-glycosides Chemical class 0.000 description 16
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 15
239000003921 oil Substances 0.000 description 14
235000019198 oils Nutrition 0.000 description 14
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 12
238000005469 granulation Methods 0.000 description 12
230000003179 granulation Effects 0.000 description 12
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 9
239000000126 substance Substances 0.000 description 9
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 8
WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 8
229920002245 Dextrose equivalent Polymers 0.000 description 7
ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 7
150000001298 alcohols Chemical class 0.000 description 7
229920000642 polymer Polymers 0.000 description 7
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 6
229920001353 Dextrin Polymers 0.000 description 6
239000004375 Dextrin Substances 0.000 description 6
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
239000011230 binding agent Substances 0.000 description 6
229920001577 copolymer Polymers 0.000 description 6
235000019425 dextrin Nutrition 0.000 description 6
235000014113 dietary fatty acids Nutrition 0.000 description 6
239000000194 fatty acid Substances 0.000 description 6
229930195729 fatty acid Natural products 0.000 description 6
239000011734 sodium Substances 0.000 description 6
125000000217 alkyl group Chemical group 0.000 description 5
239000000178 monomer Substances 0.000 description 5
229920005646 polycarboxylate Polymers 0.000 description 5
229910052708 sodium Inorganic materials 0.000 description 5
239000007858 starting material Substances 0.000 description 5
RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 4
HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 4
RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 4
KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 4
239000001361 adipic acid Substances 0.000 description 4
235000011037 adipic acid Nutrition 0.000 description 4
JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 4
KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 4
238000006243 chemical reaction Methods 0.000 description 4
239000000470 constituent Substances 0.000 description 4
238000001035 drying Methods 0.000 description 4
150000002191 fatty alcohols Chemical class 0.000 description 4
239000010419 fine particle Substances 0.000 description 4
159000000000 sodium salts Chemical class 0.000 description 4
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 3
DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 description 3
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
239000004115 Sodium Silicate Substances 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
229920002125 Sokalan® Polymers 0.000 description 3
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 3
238000005054 agglomeration Methods 0.000 description 3
230000002776 aggregation Effects 0.000 description 3
150000001720 carbohydrates Chemical class 0.000 description 3
150000001735 carboxylic acids Chemical class 0.000 description 3
239000012876 carrier material Substances 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
230000000694 effects Effects 0.000 description 3
230000007062 hydrolysis Effects 0.000 description 3
238000006460 hydrolysis reaction Methods 0.000 description 3
229910052500 inorganic mineral Inorganic materials 0.000 description 3
239000011707 mineral Substances 0.000 description 3
239000012074 organic phase Substances 0.000 description 3
239000011148 porous material Substances 0.000 description 3
235000019351 sodium silicates Nutrition 0.000 description 3
235000002906 tartaric acid Nutrition 0.000 description 3
239000011975 tartaric acid Substances 0.000 description 3
238000012360 testing method Methods 0.000 description 3
239000011800 void material Substances 0.000 description 3
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 2
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical class NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 2
RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 2
IMROMDMJAWUWLK-UHFFFAOYSA-N Ethenol Chemical compound OC=C IMROMDMJAWUWLK-UHFFFAOYSA-N 0.000 description 2
VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 2
125000003158 alcohol group Chemical group 0.000 description 2
150000008051 alkyl sulfates Chemical class 0.000 description 2
239000007795 chemical reaction product Substances 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
239000003085 diluting agent Substances 0.000 description 2
238000009826 distribution Methods 0.000 description 2
238000002474 experimental method Methods 0.000 description 2
238000001125 extrusion Methods 0.000 description 2
150000004665 fatty acids Chemical class 0.000 description 2
238000009472 formulation Methods 0.000 description 2
238000005227 gel permeation chromatography Methods 0.000 description 2
239000000174 gluconic acid Substances 0.000 description 2
235000012208 gluconic acid Nutrition 0.000 description 2
150000004676 glycans Chemical class 0.000 description 2
LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
229910001683 gmelinite Inorganic materials 0.000 description 2
125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
235000021388 linseed oil Nutrition 0.000 description 2
239000000944 linseed oil Substances 0.000 description 2
239000002808 molecular sieve Substances 0.000 description 2
MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 description 2
229920001542 oligosaccharide Polymers 0.000 description 2
150000002482 oligosaccharides Chemical class 0.000 description 2
229920000172 poly(styrenesulfonic acid) Polymers 0.000 description 2
229920000058 polyacrylate Polymers 0.000 description 2
229920005862 polyol Polymers 0.000 description 2
229920006324 polyoxymethylene Polymers 0.000 description 2
229920001282 polysaccharide Polymers 0.000 description 2
239000005017 polysaccharide Substances 0.000 description 2
239000002243 precursor Substances 0.000 description 2
239000000344 soap Substances 0.000 description 2
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
238000001694 spray drying Methods 0.000 description 2
238000010561 standard procedure Methods 0.000 description 2
239000003760 tallow Substances 0.000 description 2
ALSTYHKOOCGGFT-KTKRTIGZSA-N (9Z)-octadecen-1-ol Chemical compound CCCCCCCC\C=C/CCCCCCCCO ALSTYHKOOCGGFT-KTKRTIGZSA-N 0.000 description 1
BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
MPJQXAIKMSKXBI-UHFFFAOYSA-N 2,7,9,14-tetraoxa-1,8-diazabicyclo[6.6.2]hexadecane-3,6,10,13-tetrone Chemical compound C1CN2OC(=O)CCC(=O)ON1OC(=O)CCC(=O)O2 MPJQXAIKMSKXBI-UHFFFAOYSA-N 0.000 description 1
CFPOJWPDQWJEMO-UHFFFAOYSA-N 2-(1,2-dicarboxyethoxy)butanedioic acid Chemical class OC(=O)CC(C(O)=O)OC(C(O)=O)CC(O)=O CFPOJWPDQWJEMO-UHFFFAOYSA-N 0.000 description 1
GPQQIEOJFQIALX-UHFFFAOYSA-N 2-[2-(4,7-dioxo-1,3,2-dioxazepan-2-yl)ethyl]-1,3,2-dioxazepane-4,7-dione Chemical compound C1(CCC(=O)ON(CCN2OC(CCC(=O)O2)=O)O1)=O GPQQIEOJFQIALX-UHFFFAOYSA-N 0.000 description 1
XEEYSDHEOQHCDA-UHFFFAOYSA-N 2-methylprop-2-ene-1-sulfonic acid Chemical compound CC(=C)CS(O)(=O)=O XEEYSDHEOQHCDA-UHFFFAOYSA-N 0.000 description 1
229910002012 Aerosil® Inorganic materials 0.000 description 1
WJSLZXMQHNTOBA-UHFFFAOYSA-N C(CCC(=O)O)(=O)O.C(CCC(=O)O)(=O)O.C(CCC(=O)O)(=O)O.OCC(O)CO Chemical class C(CCC(=O)O)(=O)O.C(CCC(=O)O)(=O)O.C(CCC(=O)O)(=O)O.OCC(O)CO WJSLZXMQHNTOBA-UHFFFAOYSA-N 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
229920003043 Cellulose fiber Polymers 0.000 description 1
KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
235000013162 Cocos nucifera Nutrition 0.000 description 1
244000060011 Cocos nucifera Species 0.000 description 1
241000640882 Condea Species 0.000 description 1
RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 1
QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical class [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
229920001503 Glucan Polymers 0.000 description 1
SXRSQZLOMIGNAQ-UHFFFAOYSA-N Glutaraldehyde Chemical compound O=CCCCC=O SXRSQZLOMIGNAQ-UHFFFAOYSA-N 0.000 description 1
239000005909 Kieselgur Substances 0.000 description 1
229920002774 Maltodextrin Polymers 0.000 description 1
WFRXSOIFNFJAFL-UHFFFAOYSA-N P1(OCCCCO1)=O.C(CN)N Chemical compound P1(OCCCCO1)=O.C(CN)N WFRXSOIFNFJAFL-UHFFFAOYSA-N 0.000 description 1
229920002845 Poly(methacrylic acid) Polymers 0.000 description 1
229920000805 Polyaspartic acid Polymers 0.000 description 1
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
229920002472 Starch Polymers 0.000 description 1
ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 1
XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
238000002441 X-ray diffraction Methods 0.000 description 1
239000002250 absorbent Substances 0.000 description 1
230000002745 absorbent Effects 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
229910001420 alkaline earth metal ion Inorganic materials 0.000 description 1
150000003973 alkyl amines Chemical class 0.000 description 1
BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
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235000012211 aluminium silicate Nutrition 0.000 description 1
229910000323 aluminium silicate Inorganic materials 0.000 description 1
150000001408 amides Chemical class 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
229940077388 benzenesulfonate Drugs 0.000 description 1
229920002988 biodegradable polymer Polymers 0.000 description 1
239000004621 biodegradable polymer Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
WQZQEUCNSUNRRW-UHFFFAOYSA-N butanedioic acid propane-1,2,3-triol Chemical class OCC(O)CO.OC(=O)CCC(O)=O.OC(=O)CCC(O)=O WQZQEUCNSUNRRW-UHFFFAOYSA-N 0.000 description 1
229910000019 calcium carbonate Inorganic materials 0.000 description 1
235000010216 calcium carbonate Nutrition 0.000 description 1
235000012241 calcium silicate Nutrition 0.000 description 1
235000014633 carbohydrates Nutrition 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
150000007942 carboxylates Chemical class 0.000 description 1
150000001732 carboxylic acid derivatives Chemical group 0.000 description 1
238000013329 compounding Methods 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
239000008121 dextrose Substances 0.000 description 1
229910003460 diamond Inorganic materials 0.000 description 1
239000010432 diamond Substances 0.000 description 1
150000005690 diesters Chemical class 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
238000002003 electron diffraction Methods 0.000 description 1
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
238000007046 ethoxylation reaction Methods 0.000 description 1
229940071087 ethylenediamine disuccinate Drugs 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000001530 fumaric acid Substances 0.000 description 1
239000008103 glucose Substances 0.000 description 1
229940015043 glyoxal Drugs 0.000 description 1
238000000227 grinding Methods 0.000 description 1
229910001385 heavy metal Inorganic materials 0.000 description 1
229910052739 hydrogen Chemical group 0.000 description 1
239000001257 hydrogen Chemical group 0.000 description 1
125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
238000010348 incorporation Methods 0.000 description 1
229910017053 inorganic salt Inorganic materials 0.000 description 1
125000000686 lactone group Chemical group 0.000 description 1
159000000003 magnesium salts Chemical class 0.000 description 1
239000000391 magnesium silicate Substances 0.000 description 1
235000012243 magnesium silicates Nutrition 0.000 description 1
239000001630 malic acid Substances 0.000 description 1
235000011090 malic acid Nutrition 0.000 description 1
239000000463 material Substances 0.000 description 1
238000005259 measurement Methods 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
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XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
239000007800 oxidant agent Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
239000012071 phase Substances 0.000 description 1
UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 description 1
230000000704 physical effect Effects 0.000 description 1
239000004584 polyacrylic acid Substances 0.000 description 1
235000019353 potassium silicate Nutrition 0.000 description 1
WSHYKIAQCMIPTB-UHFFFAOYSA-M potassium;2-oxo-3-(3-oxo-1-phenylbutyl)chromen-4-olate Chemical compound [K+].[O-]C=1C2=CC=CC=C2OC(=O)C=1C(CC(=O)C)C1=CC=CC=C1 WSHYKIAQCMIPTB-UHFFFAOYSA-M 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
POSICDHOUBKJKP-UHFFFAOYSA-N prop-2-enoxybenzene Chemical compound C=CCOC1=CC=CC=C1 POSICDHOUBKJKP-UHFFFAOYSA-N 0.000 description 1
230000001698 pyrogenic effect Effects 0.000 description 1
230000001603 reducing effect Effects 0.000 description 1
230000011514 reflex Effects 0.000 description 1
238000007493 shaping process Methods 0.000 description 1
239000001509 sodium citrate Substances 0.000 description 1
NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
239000002689 soil Substances 0.000 description 1
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238000003860 storage Methods 0.000 description 1
150000003470 sulfuric acid monoesters Chemical class 0.000 description 1
238000004381 surface treatment Methods 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
235000020357 syrup Nutrition 0.000 description 1
KUCOHFSKRZZVRO-UHFFFAOYSA-N terephthalaldehyde Chemical compound O=CC1=CC=C(C=O)C=C1 KUCOHFSKRZZVRO-UHFFFAOYSA-N 0.000 description 1
238000010998 test method Methods 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
JSPLKZUTYZBBKA-UHFFFAOYSA-N trioxidane Chemical group OOO JSPLKZUTYZBBKA-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
- C11D17/0065—Solid detergents containing builders
- C11D17/0073—Tablets
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols

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Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Detergent Compositions (AREA)

CA 2308932 1999-05-22 2000-05-18 Processus de production de granules d'agent de surface Abandoned CA2308932A1 (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE1999123627 DE19923627A1 (de)	1999-05-22	1999-05-22	Verfahren zur Herstellung von Tensidgranulaten
DE19923627.5		1999-05-22

Publications (1)

Publication Number	Publication Date
CA2308932A1 true CA2308932A1 (fr)	2000-11-22

Family

ID=7908924

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA 2308932 Abandoned CA2308932A1 (fr)	1999-05-22	2000-05-18	Processus de production de granules d'agent de surface

Country Status (3)

Country	Link
CA (1)	CA2308932A1 (fr)
DE (1)	DE19923627A1 (fr)
WO (1)	WO2000071657A1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6900170B2 (en)	2001-05-15	2005-05-31	Unilever Home Products And Care Usa, A Division Of Conopco, Inc.	Granular composition
US6911423B2 (en)	2001-05-15	2005-06-28	Unilever Home & Personal Care Usa, Division Of Conopco, Inc.	Granular composition
US7208458B2 (en)	2003-09-27	2007-04-24	Clariant Produkte (Deutschland) Gmbh	Surfactant composition comprising fatty alcohol alkoxylates and amorphous silica

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6096694A (ja) *	1983-10-31	1985-05-30	ライオン株式会社	粒状洗剤組成物
JPH07133497A (ja) *	1993-11-11	1995-05-23	Lion Corp	高嵩密度粒状洗剤の製造方法
DE19753310A1 (de) *	1997-12-02	1999-06-10	Henkel Kgaa	Rohstoff-Compounds mit hohem Schüttgewicht

1999
- 1999-05-22 DE DE1999123627 patent/DE19923627A1/de not_active Withdrawn
2000
- 2000-05-13 WO PCT/EP2000/004328 patent/WO2000071657A1/fr not_active Ceased
- 2000-05-18 CA CA 2308932 patent/CA2308932A1/fr not_active Abandoned

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6900170B2 (en)	2001-05-15	2005-05-31	Unilever Home Products And Care Usa, A Division Of Conopco, Inc.	Granular composition
US6911423B2 (en)	2001-05-15	2005-06-28	Unilever Home & Personal Care Usa, Division Of Conopco, Inc.	Granular composition
US7208458B2 (en)	2003-09-27	2007-04-24	Clariant Produkte (Deutschland) Gmbh	Surfactant composition comprising fatty alcohol alkoxylates and amorphous silica

Also Published As

Publication number	Publication date
WO2000071657A1 (fr)	2000-11-30
DE19923627A1 (de)	2000-11-23

Legal Events

Date	Code	Title	Description
2002-08-22	FZDE	Dead

Publication	Publication Date	Title
US5616550A (en)	1997-04-01	Process for the continuous production of a granular detergent
AU647681B2 (en)	1994-03-24	Detergent compositions
US5518649A (en)	1996-05-21	Particulate detergent composition or component comprising zeolite MAP ASA carrier
US5354493A (en)	1994-10-11	Process for the production of surfactant-containing granulates
JPH0649879B2 (ja)	1994-06-29	洗剤組成物、その成分、およびその製造方法
EP2841553B1 (fr)	2018-02-21	Procédé de production d'un granule de détergent, granule de détergent et composition détergente comprenant ce granule
WO2011061044A1 (fr)	2011-05-26	Granulés de détergent
CA2164107C (fr)	2000-10-03	Compositions detergentes granulaires renfermant une zeolite; methode de preparation
KR19980701494A (ko)	1998-05-15	무정형 알칼리 실리케이트 화합물
EP2870229B1 (fr)	2019-08-07	Procédé de production d'un granule de détergent, granule de détergent et composition détergente comprenant ce granule
EP2123744B1 (fr)	2010-05-12	Fabrication de granules de détergent par neutralisation sèche
JPH0617098A (ja)	1994-01-25	洗剤組成物及びその製造法
EP0925354B1 (fr)	2004-08-11	Procede de preparation de compositions detergentes a masse volumique en vrac elevee
EP3030641B1 (fr)	2017-12-27	Procédé de production d'un granule détergent, granule détergent et composition détergente comprenant ce granule
CA2308932A1 (fr)	2000-11-22	Processus de production de granules d'agent de surface
CA2308910A1 (fr)	2000-11-22	Processus de production de granules d'agent de surface
CA2248635C (fr)	2006-05-16	Compositions detergentes a base de particules d'aluminosilicate contenant des cogranules de zeolite map et un silicate de metal alcalin
JPH08504864A (ja)	1996-05-28	粒状の洗浄剤および／または清浄化剤
JP4373546B2 (ja)	2009-11-25	洗剤物品
JP2000503055A (ja)	2000-03-14	粒状洗剤／洗浄剤またはその成分の製造法
KR100334733B1 (ko)	2002-05-04	고밀도분말세제의 제조방법
EP1076686B1 (fr)	2004-03-03	Procede de fabrication d'un produit detergent non particulaire dispersible dans l'eau obtenu a partir de particules de detergent de faible densite
CA2293969A1 (fr)	2000-07-14	Adjuvant en granules pour objets sous forme de detergent
JP2003516467A (ja)	2003-05-13	圧縮粒子の製造法
CA2300604A1 (fr)	2000-09-11	Pastilles de detergent renfermant une combinaison de surfactant et d'agent renforcateur

CA2308932A1 - Processus de production de granules d'agent de surface - Google Patents

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Applications Claiming Priority (2)

Publications (1)

Family

ID=7908924

Family Applications (1)

Country Status (3)

Cited By (3)

Family Cites Families (3)

Cited By (3)

Also Published As

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