CA2331602C - Procede de fabrication d'un materiau actif pour electrode positive d'une batterie secondaire - Google Patents

Procede de fabrication d'un materiau actif pour electrode positive d'une batterie secondaire Download PDF

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Publication number: CA2331602C
Authority: CA; Canada
Prior art keywords: transition metal; positive electrode; lithium; group; compound
Prior art date: 1992-11-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA002331602A

Other languages

English (en)

Other versions

CA2331602A1 (fr

Inventor

Soichiro Kawakami

Shinya Mishina

Naoya Kobayashi

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Canon Inc

Original Assignee

Canon Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1992-11-30

Filing date

1993-11-26

Publication date

2002-09-10

1992-11-30 Priority claimed from JP4320559A external-priority patent/JP2771406B2/ja

1992-11-30 Priority claimed from JP32056092A external-priority patent/JP3487556B2/ja

1992-11-30 Priority claimed from JP4320558A external-priority patent/JP3067426B2/ja

1992-11-30 Priority claimed from JP4320557A external-priority patent/JP2943127B2/ja

1992-12-24 Priority claimed from JP34456392A external-priority patent/JP3423338B2/ja

1993-04-05 Priority claimed from JP07834293A external-priority patent/JP3530544B2/ja

1993-11-26 Application filed by Canon Inc filed Critical Canon Inc

1993-11-26 Priority claimed from CA002110097A external-priority patent/CA2110097C/fr

1994-05-31 Publication of CA2331602A1 publication Critical patent/CA2331602A1/fr

2002-09-10 Publication of CA2331602C publication Critical patent/CA2331602C/fr

2002-09-10 Application granted granted Critical

2013-11-26 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

239000007774 positive electrode material Substances 0.000 title claims abstract description 91
238000004519 manufacturing process Methods 0.000 title claims description 38
229910052744 lithium Inorganic materials 0.000 claims abstract description 314
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims abstract description 266
238000006243 chemical reaction Methods 0.000 claims abstract description 86
238000000034 method Methods 0.000 claims description 220
239000000463 material Substances 0.000 claims description 187
150000001875 compounds Chemical class 0.000 claims description 138
-1 transition metal salt Chemical class 0.000 claims description 127
229910052723 transition metal Inorganic materials 0.000 claims description 122
150000003624 transition metals Chemical class 0.000 claims description 108
239000007789 gas Substances 0.000 claims description 86
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 73
239000002904 solvent Substances 0.000 claims description 73
229910052751 metal Inorganic materials 0.000 claims description 69
239000002184 metal Substances 0.000 claims description 69
229910052799 carbon Inorganic materials 0.000 claims description 63
229910052719 titanium Inorganic materials 0.000 claims description 61
229910001868 water Inorganic materials 0.000 claims description 60
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 59
239000000203 mixture Substances 0.000 claims description 56
239000012298 atmosphere Substances 0.000 claims description 53
230000008569 process Effects 0.000 claims description 50
150000003839 salts Chemical class 0.000 claims description 50
229910052759 nickel Inorganic materials 0.000 claims description 48
239000000843 powder Substances 0.000 claims description 47
229920005989 resin Polymers 0.000 claims description 44
239000011347 resin Substances 0.000 claims description 44
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 43
150000002736 metal compounds Chemical class 0.000 claims description 40
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 35
239000004743 Polypropylene Substances 0.000 claims description 33
229920001155 polypropylene Polymers 0.000 claims description 33
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 31
239000004020 conductor Substances 0.000 claims description 31
239000002994 raw material Substances 0.000 claims description 31
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 29
229910052710 silicon Inorganic materials 0.000 claims description 28
239000010703 silicon Substances 0.000 claims description 27
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 26
239000013078 crystal Substances 0.000 claims description 26
239000007788 liquid Substances 0.000 claims description 26
229910052760 oxygen Inorganic materials 0.000 claims description 26
239000001301 oxygen Substances 0.000 claims description 26
150000003623 transition metal compounds Chemical class 0.000 claims description 25
239000002253 acid Substances 0.000 claims description 24
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 24
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 23
229910052731 fluorine Inorganic materials 0.000 claims description 23
239000011737 fluorine Substances 0.000 claims description 23
239000013081 microcrystal Substances 0.000 claims description 23
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 20
239000004698 Polyethylene Substances 0.000 claims description 20
150000004820 halides Chemical class 0.000 claims description 20
229920000573 polyethylene Polymers 0.000 claims description 20
239000003513 alkali Substances 0.000 claims description 19
229910052739 hydrogen Inorganic materials 0.000 claims description 18
238000002156 mixing Methods 0.000 claims description 18
239000001257 hydrogen Substances 0.000 claims description 17
229910052757 nitrogen Inorganic materials 0.000 claims description 17
229910052802 copper Inorganic materials 0.000 claims description 16
238000005507 spraying Methods 0.000 claims description 14
150000004703 alkoxides Chemical class 0.000 claims description 13
229910052717 sulfur Inorganic materials 0.000 claims description 13
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 12
229910052796 boron Inorganic materials 0.000 claims description 12
238000002844 melting Methods 0.000 claims description 12
239000011593 sulfur Substances 0.000 claims description 12
229910052720 vanadium Inorganic materials 0.000 claims description 12
239000000654 additive Substances 0.000 claims description 11
230000000996 additive effect Effects 0.000 claims description 11
229910052782 aluminium Inorganic materials 0.000 claims description 11
238000010574 gas phase reaction Methods 0.000 claims description 11
229910052742 iron Inorganic materials 0.000 claims description 11
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 10
238000001816 cooling Methods 0.000 claims description 10
239000011133 lead Substances 0.000 claims description 10
230000008018 melting Effects 0.000 claims description 10
229910052708 sodium Inorganic materials 0.000 claims description 10
239000011734 sodium Substances 0.000 claims description 10
239000011135 tin Substances 0.000 claims description 10
229910052718 tin Inorganic materials 0.000 claims description 10
ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 9
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 9
150000002894 organic compounds Chemical class 0.000 claims description 9
229910000314 transition metal oxide Inorganic materials 0.000 claims description 9
239000012159 carrier gas Substances 0.000 claims description 8
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 7
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 7
229910000037 hydrogen sulfide Inorganic materials 0.000 claims description 7
229910052738 indium Inorganic materials 0.000 claims description 7
APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims description 7
150000004678 hydrides Chemical class 0.000 claims description 6
238000006460 hydrolysis reaction Methods 0.000 claims description 6
229910052749 magnesium Inorganic materials 0.000 claims description 6
239000011777 magnesium Substances 0.000 claims description 6
239000007787 solid Substances 0.000 claims description 6
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 5
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 4
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 4
229910052791 calcium Inorganic materials 0.000 claims description 4
239000011575 calcium Substances 0.000 claims description 4
239000000460 chlorine Substances 0.000 claims description 4
229910052801 chlorine Inorganic materials 0.000 claims description 4
229910052804 chromium Inorganic materials 0.000 claims description 4
229910052748 manganese Inorganic materials 0.000 claims description 4
229910052698 phosphorus Inorganic materials 0.000 claims description 4
POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 claims description 3
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 3
229910002651 NO3 Inorganic materials 0.000 claims description 3
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 3
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 3
230000005587 bubbling Effects 0.000 claims description 3
125000005609 naphthenate group Chemical group 0.000 claims description 3
150000007524 organic acids Chemical class 0.000 claims description 3
239000011574 phosphorus Substances 0.000 claims description 3
229910052700 potassium Inorganic materials 0.000 claims description 3
239000011591 potassium Substances 0.000 claims description 3
229910052787 antimony Inorganic materials 0.000 claims description 2
WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 2
238000000889 atomisation Methods 0.000 claims description 2
229910052788 barium Inorganic materials 0.000 claims description 2
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 2
229910052797 bismuth Inorganic materials 0.000 claims description 2
JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 2
150000001728 carbonyl compounds Chemical class 0.000 claims description 2
BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims 1
206010011416 Croup infectious Diseases 0.000 claims 1
229910019142 PO4 Inorganic materials 0.000 claims 1
150000003863 ammonium salts Chemical class 0.000 claims 1
201000010549 croup Diseases 0.000 claims 1
WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
239000010452 phosphate Substances 0.000 claims 1
239000008151 electrolyte solution Substances 0.000 abstract description 117
239000007773 negative electrode material Substances 0.000 abstract description 75
229910052725 zinc Inorganic materials 0.000 abstract description 75
239000011701 zinc Substances 0.000 abstract description 75
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract description 61
150000002500 ions Chemical class 0.000 abstract description 50
239000003792 electrolyte Substances 0.000 abstract description 43
210000001787 dendrite Anatomy 0.000 abstract description 41
QELJHCBNGDEXLD-UHFFFAOYSA-N nickel zinc Chemical compound [Ni].[Zn] QELJHCBNGDEXLD-UHFFFAOYSA-N 0.000 abstract description 22
ZRXYMHTYEQQBLN-UHFFFAOYSA-N [Br].[Zn] Chemical compound [Br].[Zn] ZRXYMHTYEQQBLN-UHFFFAOYSA-N 0.000 abstract description 5
230000001747 exhibiting effect Effects 0.000 abstract description 5
HTQOEHYNHFXMJJ-UHFFFAOYSA-N oxosilver zinc Chemical compound [Zn].[Ag]=O HTQOEHYNHFXMJJ-UHFFFAOYSA-N 0.000 abstract 1
239000010408 film Substances 0.000 description 287
239000000243 solution Substances 0.000 description 149
229920000642 polymer Polymers 0.000 description 125
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 104
239000010410 layer Substances 0.000 description 97
230000000052 comparative effect Effects 0.000 description 96
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 94
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 78
238000000576 coating method Methods 0.000 description 73
239000010936 titanium Substances 0.000 description 64
239000011888 foil Substances 0.000 description 57
239000011248 coating agent Substances 0.000 description 54
229910052786 argon Inorganic materials 0.000 description 52
238000004544 sputter deposition Methods 0.000 description 48
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 39
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 38
238000006116 polymerization reaction Methods 0.000 description 38
239000000178 monomer Substances 0.000 description 36
VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 34
238000002360 preparation method Methods 0.000 description 34
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 31
229910001416 lithium ion Inorganic materials 0.000 description 31
239000004065 semiconductor Substances 0.000 description 30
CONKBQPVFMXDOV-QHCPKHFHSA-N 6-[(5S)-5-[[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]methyl]-2-oxo-1,3-oxazolidin-3-yl]-3H-1,3-benzoxazol-2-one Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C[C@H]1CN(C(O1)=O)C1=CC2=C(NC(O2)=O)C=C1 CONKBQPVFMXDOV-QHCPKHFHSA-N 0.000 description 29
HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 29
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 29
238000010438 heat treatment Methods 0.000 description 28
229910044991 metal oxide Inorganic materials 0.000 description 27
150000004706 metal oxides Chemical class 0.000 description 27
239000010935 stainless steel Substances 0.000 description 27
229910001220 stainless steel Inorganic materials 0.000 description 27
RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 description 26
238000012360 testing method Methods 0.000 description 26
NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 24
229920000620 organic polymer Polymers 0.000 description 24
239000003960 organic solvent Substances 0.000 description 24
238000005229 chemical vapour deposition Methods 0.000 description 23
239000002131 composite material Substances 0.000 description 23
WZFUQSJFWNHZHM-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)CC(=O)N1CC2=C(CC1)NN=N2 WZFUQSJFWNHZHM-UHFFFAOYSA-N 0.000 description 22
229920001577 copolymer Polymers 0.000 description 22
238000001035 drying Methods 0.000 description 22
235000019441 ethanol Nutrition 0.000 description 22
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 21
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 21
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 21
238000004132 cross linking Methods 0.000 description 21
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 20
239000010949 copper Substances 0.000 description 20
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 20
229920002554 vinyl polymer Polymers 0.000 description 20
XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 19
238000005268 plasma chemical vapour deposition Methods 0.000 description 19
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 19
HMUNWXXNJPVALC-UHFFFAOYSA-N 1-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C(CN1CC2=C(CC1)NN=N2)=O HMUNWXXNJPVALC-UHFFFAOYSA-N 0.000 description 18
YJLUBHOZZTYQIP-UHFFFAOYSA-N 2-[5-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1,3,4-oxadiazol-2-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1=NN=C(O1)CC(=O)N1CC2=C(CC1)NN=N2 YJLUBHOZZTYQIP-UHFFFAOYSA-N 0.000 description 18
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 18
BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 18
WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 17
239000011521 glass Substances 0.000 description 17
229920006254 polymer film Polymers 0.000 description 17
238000011156 evaluation Methods 0.000 description 16
SXAMGRAIZSSWIH-UHFFFAOYSA-N 2-[3-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1,2,4-oxadiazol-5-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1=NOC(=N1)CC(=O)N1CC2=C(CC1)NN=N2 SXAMGRAIZSSWIH-UHFFFAOYSA-N 0.000 description 15
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 15
YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical class CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 15
239000011810 insulating material Substances 0.000 description 15
239000011159 matrix material Substances 0.000 description 15
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 14
150000003983 crown ethers Chemical class 0.000 description 14
238000007599 discharging Methods 0.000 description 14
150000004767 nitrides Chemical class 0.000 description 14
239000007858 starting material Substances 0.000 description 14
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 14
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 14
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 13
238000005566 electron beam evaporation Methods 0.000 description 13
239000011800 void material Substances 0.000 description 13
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
238000007598 dipping method Methods 0.000 description 12
230000000694 effects Effects 0.000 description 12
XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical group FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 12
239000012535 impurity Substances 0.000 description 12
238000001182 laser chemical vapour deposition Methods 0.000 description 12
239000000377 silicon dioxide Substances 0.000 description 12
238000004381 surface treatment Methods 0.000 description 12
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 11
UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 11
BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 11
125000003118 aryl group Chemical group 0.000 description 11
230000015572 biosynthetic process Effects 0.000 description 11
238000010894 electron beam technology Methods 0.000 description 11
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 11
229910052697 platinum Inorganic materials 0.000 description 11
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238000007906 compression Methods 0.000 description 1
238000010276 construction Methods 0.000 description 1
238000011109 contamination Methods 0.000 description 1
229940120693 copper naphthenate Drugs 0.000 description 1
PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 description 1
SEVNKWFHTNVOLD-UHFFFAOYSA-L copper;3-(4-ethylcyclohexyl)propanoate;3-(3-ethylcyclopentyl)propanoate Chemical compound [Cu+2].CCC1CCC(CCC([O-])=O)C1.CCC1CCC(CCC([O-])=O)CC1 SEVNKWFHTNVOLD-UHFFFAOYSA-L 0.000 description 1
239000007822 coupling agent Substances 0.000 description 1
239000013039 cover film Substances 0.000 description 1
125000004122 cyclic group Chemical group 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
QDGONURINHVBEW-UHFFFAOYSA-N dichlorodifluoroethylene Chemical group FC(F)=C(Cl)Cl QDGONURINHVBEW-UHFFFAOYSA-N 0.000 description 1
YKLVAJZBWVTOGT-YCBFMBTMSA-N didodecyl (2s)-2-aminopentanedioate;hydrochloride Chemical compound Cl.CCCCCCCCCCCCOC(=O)CC[C@H](N)C(=O)OCCCCCCCCCCCC YKLVAJZBWVTOGT-YCBFMBTMSA-N 0.000 description 1
229960004132 diethyl ether Drugs 0.000 description 1
238000004455 differential thermal analysis Methods 0.000 description 1
238000009792 diffusion process Methods 0.000 description 1
MGNHOGAVECORPT-UHFFFAOYSA-N difluorosilicon Chemical compound F[Si]F MGNHOGAVECORPT-UHFFFAOYSA-N 0.000 description 1
VIXPKJNAOIWFMW-UHFFFAOYSA-M dihexadecyl(dimethyl)azanium;bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCC VIXPKJNAOIWFMW-UHFFFAOYSA-M 0.000 description 1
239000002612 dispersion medium Substances 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000009826 distribution Methods 0.000 description 1
125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
238000002848 electrochemical method Methods 0.000 description 1
238000003487 electrochemical reaction Methods 0.000 description 1
238000009713 electroplating Methods 0.000 description 1
XTLNYNMNUCLWEZ-UHFFFAOYSA-N ethanol;propan-2-one Chemical compound CCO.CC(C)=O XTLNYNMNUCLWEZ-UHFFFAOYSA-N 0.000 description 1
229940031098 ethanolamine Drugs 0.000 description 1
MASNVFNHVJIXLL-UHFFFAOYSA-N ethenyl(ethoxy)silicon Chemical compound CCO[Si]C=C MASNVFNHVJIXLL-UHFFFAOYSA-N 0.000 description 1
NKSJNEHGWDZZQF-UHFFFAOYSA-N ethenyl(trimethoxy)silane Chemical compound CO[Si](OC)(OC)C=C NKSJNEHGWDZZQF-UHFFFAOYSA-N 0.000 description 1
BITPLIXHRASDQB-UHFFFAOYSA-N ethenyl-[ethenyl(dimethyl)silyl]oxy-dimethylsilane Chemical compound C=C[Si](C)(C)O[Si](C)(C)C=C BITPLIXHRASDQB-UHFFFAOYSA-N 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
SBRXLTRZCJVAPH-UHFFFAOYSA-N ethyl(trimethoxy)silane Chemical compound CC[Si](OC)(OC)OC SBRXLTRZCJVAPH-UHFFFAOYSA-N 0.000 description 1
229920001038 ethylene copolymer Polymers 0.000 description 1
239000004744 fabric Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
150000002221 fluorine Chemical class 0.000 description 1
150000002222 fluorine compounds Chemical class 0.000 description 1
229920001973 fluoroelastomer Polymers 0.000 description 1
ZHPNWZCWUUJAJC-UHFFFAOYSA-N fluorosilicon Chemical compound [Si]F ZHPNWZCWUUJAJC-UHFFFAOYSA-N 0.000 description 1
230000008014 freezing Effects 0.000 description 1
238000007710 freezing Methods 0.000 description 1
229910052733 gallium Inorganic materials 0.000 description 1
YEJRWHAVMIAJKC-UHFFFAOYSA-N gamma-butyrolactone Natural products O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 1
229910052732 germanium Inorganic materials 0.000 description 1
GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
YBMRDBCBODYGJE-UHFFFAOYSA-N germanium oxide Inorganic materials O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 description 1
239000003365 glass fiber Substances 0.000 description 1
229910052735 hafnium Inorganic materials 0.000 description 1
230000020169 heat generation Effects 0.000 description 1
UBIJTWDKTYCPMQ-UHFFFAOYSA-N hexachlorophosphazene Chemical compound ClP1(Cl)=NP(Cl)(Cl)=NP(Cl)(Cl)=N1 UBIJTWDKTYCPMQ-UHFFFAOYSA-N 0.000 description 1
229910000042 hydrogen bromide Inorganic materials 0.000 description 1
229920001477 hydrophilic polymer Polymers 0.000 description 1
230000002209 hydrophobic effect Effects 0.000 description 1
229920001600 hydrophobic polymer Polymers 0.000 description 1
230000006698 induction Effects 0.000 description 1
150000002484 inorganic compounds Chemical class 0.000 description 1
229910010272 inorganic material Inorganic materials 0.000 description 1
PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
239000010416 ion conductor Substances 0.000 description 1
230000010220 ion permeability Effects 0.000 description 1
238000010884 ion-beam technique Methods 0.000 description 1
229910052741 iridium Inorganic materials 0.000 description 1
229910000049 iron hydride Inorganic materials 0.000 description 1
235000014413 iron hydroxide Nutrition 0.000 description 1
RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
229910052746 lanthanum Inorganic materials 0.000 description 1
229910052745 lead Inorganic materials 0.000 description 1
238000003754 machining Methods 0.000 description 1
239000011565 manganese chloride Substances 0.000 description 1
235000002867 manganese chloride Nutrition 0.000 description 1
SGGOJYZMTYGPCH-UHFFFAOYSA-L manganese(2+);naphthalene-2-carboxylate Chemical compound [Mn+2].C1=CC=CC2=CC(C(=O)[O-])=CC=C21.C1=CC=CC2=CC(C(=O)[O-])=CC=C21 SGGOJYZMTYGPCH-UHFFFAOYSA-L 0.000 description 1
238000005259 measurement Methods 0.000 description 1
230000007246 mechanism Effects 0.000 description 1
239000002609 medium Substances 0.000 description 1
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
229910052753 mercury Inorganic materials 0.000 description 1
229910000000 metal hydroxide Inorganic materials 0.000 description 1
150000004692 metal hydroxides Chemical class 0.000 description 1
VMTCKFAPVIWNOF-UHFFFAOYSA-N methane tetrahydrofluoride Chemical compound C.F.F.F.F VMTCKFAPVIWNOF-UHFFFAOYSA-N 0.000 description 1
UNRFQJSWBQGLDR-UHFFFAOYSA-N methane trihydrofluoride Chemical compound C.F.F.F UNRFQJSWBQGLDR-UHFFFAOYSA-N 0.000 description 1
125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
239000004570 mortar (masonry) Substances 0.000 description 1
PHQOGHDTIVQXHL-UHFFFAOYSA-N n'-(3-trimethoxysilylpropyl)ethane-1,2-diamine Chemical compound CO[Si](OC)(OC)CCCNCCN PHQOGHDTIVQXHL-UHFFFAOYSA-N 0.000 description 1
MQWFLKHKWJMCEN-UHFFFAOYSA-N n'-[3-[dimethoxy(methyl)silyl]propyl]ethane-1,2-diamine Chemical compound CO[Si](C)(OC)CCCNCCN MQWFLKHKWJMCEN-UHFFFAOYSA-N 0.000 description 1
GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 description 1
125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
125000005487 naphthalate group Chemical group 0.000 description 1
UIEKYBOPAVTZKW-UHFFFAOYSA-L naphthalene-2-carboxylate;nickel(2+) Chemical compound [Ni+2].C1=CC=CC2=CC(C(=O)[O-])=CC=C21.C1=CC=CC2=CC(C(=O)[O-])=CC=C21 UIEKYBOPAVTZKW-UHFFFAOYSA-L 0.000 description 1
GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
229920001220 nitrocellulos Polymers 0.000 description 1
GVGCUCJTUSOZKP-UHFFFAOYSA-N nitrogen trifluoride Chemical compound FN(F)F GVGCUCJTUSOZKP-UHFFFAOYSA-N 0.000 description 1
239000004745 nonwoven fabric Substances 0.000 description 1
229920006284 nylon film Polymers 0.000 description 1
MCCIMQKMMBVWHO-UHFFFAOYSA-N octadecanoic acid;titanium Chemical compound [Ti].CCCCCCCCCCCCCCCCCC(O)=O.CCCCCCCCCCCCCCCCCC(O)=O.CCCCCCCCCCCCCCCCCC(O)=O.CCCCCCCCCCCCCCCCCC(O)=O MCCIMQKMMBVWHO-UHFFFAOYSA-N 0.000 description 1
125000005447 octyloxy group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])O* 0.000 description 1
150000002902 organometallic compounds Chemical class 0.000 description 1
229910052762 osmium Inorganic materials 0.000 description 1
235000006408 oxalic acid Nutrition 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
PVADDRMAFCOOPC-UHFFFAOYSA-N oxogermanium Chemical compound [Ge]=O PVADDRMAFCOOPC-UHFFFAOYSA-N 0.000 description 1
239000003973 paint Substances 0.000 description 1
229910052763 palladium Inorganic materials 0.000 description 1
KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 1
125000000864 peroxy group Chemical group O(O*)* 0.000 description 1
239000000088 plastic resin Substances 0.000 description 1
HZEBHPIOVYHPMT-UHFFFAOYSA-N polonium atom Chemical compound [Po] HZEBHPIOVYHPMT-UHFFFAOYSA-N 0.000 description 1
229920000747 poly(lactic acid) Polymers 0.000 description 1
229920000327 poly(triphenylamine) polymer Polymers 0.000 description 1
238000012643 polycondensation polymerization Methods 0.000 description 1
229920002530 polyetherether ketone Polymers 0.000 description 1
229920001601 polyetherimide Polymers 0.000 description 1
239000005020 polyethylene terephthalate Substances 0.000 description 1
229920000139 polyethylene terephthalate Polymers 0.000 description 1
229920000151 polyglycol Polymers 0.000 description 1
239000010695 polyglycol Substances 0.000 description 1
239000005518 polymer electrolyte Substances 0.000 description 1
239000002861 polymer material Substances 0.000 description 1
229920006380 polyphenylene oxide Polymers 0.000 description 1
229920000069 polyphenylene sulfide Polymers 0.000 description 1
229920001451 polypropylene glycol Polymers 0.000 description 1
229920002689 polyvinyl acetate Polymers 0.000 description 1
239000011118 polyvinyl acetate Substances 0.000 description 1
239000011148 porous material Substances 0.000 description 1
150000004032 porphyrins Chemical class 0.000 description 1
239000011698 potassium fluoride Substances 0.000 description 1
235000003270 potassium fluoride Nutrition 0.000 description 1
229910001414 potassium ion Inorganic materials 0.000 description 1
LUMVCLJFHCTMCV-UHFFFAOYSA-M potassium;hydroxide;hydrate Chemical compound O.[OH-].[K+] LUMVCLJFHCTMCV-UHFFFAOYSA-M 0.000 description 1
239000001294 propane Substances 0.000 description 1
238000004080 punching Methods 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000010992 reflux Methods 0.000 description 1
229910052702 rhenium Inorganic materials 0.000 description 1
229910052703 rhodium Inorganic materials 0.000 description 1
229910052707 ruthenium Inorganic materials 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
229930195734 saturated hydrocarbon Natural products 0.000 description 1
238000004062 sedimentation Methods 0.000 description 1
SPVXKVOXSXTJOY-UHFFFAOYSA-N selane Chemical compound [SeH2] SPVXKVOXSXTJOY-UHFFFAOYSA-N 0.000 description 1
229910000058 selane Inorganic materials 0.000 description 1
150000003346 selenoethers Chemical class 0.000 description 1
238000010008 shearing Methods 0.000 description 1
230000035939 shock Effects 0.000 description 1
229910052814 silicon oxide Inorganic materials 0.000 description 1
239000010944 silver (metal) Substances 0.000 description 1
239000011775 sodium fluoride Substances 0.000 description 1
235000013024 sodium fluoride Nutrition 0.000 description 1
239000012312 sodium hydride Substances 0.000 description 1
229910000104 sodium hydride Inorganic materials 0.000 description 1
239000001488 sodium phosphate Substances 0.000 description 1
229910000162 sodium phosphate Inorganic materials 0.000 description 1
238000005476 soldering Methods 0.000 description 1
239000007784 solid electrolyte Substances 0.000 description 1
IIACRCGMVDHOTQ-UHFFFAOYSA-M sulfamate Chemical compound NS([O-])(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-M 0.000 description 1
125000004434 sulfur atom Chemical group 0.000 description 1
SFZCNBIFKDRMGX-UHFFFAOYSA-N sulfur hexafluoride Chemical compound FS(F)(F)(F)(F)F SFZCNBIFKDRMGX-UHFFFAOYSA-N 0.000 description 1
229960000909 sulfur hexafluoride Drugs 0.000 description 1
239000002335 surface treatment layer Substances 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
OEIMLTQPLAGXMX-UHFFFAOYSA-I tantalum(v) chloride Chemical compound Cl[Ta](Cl)(Cl)(Cl)Cl OEIMLTQPLAGXMX-UHFFFAOYSA-I 0.000 description 1
229910052713 technetium Inorganic materials 0.000 description 1
PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 1
DPNGAWRBXKSTKZ-UHFFFAOYSA-J tetrabutylazanium tetrafluoride Chemical compound [F-].[F-].[F-].[F-].CCCC[N+](CCCC)(CCCC)CCCC.CCCC[N+](CCCC)(CCCC)CCCC.CCCC[N+](CCCC)(CCCC)CCCC.CCCC[N+](CCCC)(CCCC)CCCC DPNGAWRBXKSTKZ-UHFFFAOYSA-J 0.000 description 1
VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 1
LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 1
HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 1
150000003608 titanium Chemical class 0.000 description 1
230000001131 transforming effect Effects 0.000 description 1
FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 description 1
VOITXYVAKOUIBA-UHFFFAOYSA-N triethylaluminium Chemical compound CC[Al](CC)CC VOITXYVAKOUIBA-UHFFFAOYSA-N 0.000 description 1
125000003652 trifluoroethoxy group Chemical group FC(CO*)(F)F 0.000 description 1
ATVLVRVBCRICNU-UHFFFAOYSA-N trifluorosilicon Chemical compound F[Si](F)F ATVLVRVBCRICNU-UHFFFAOYSA-N 0.000 description 1
VKJKOXNPYVUXNC-UHFFFAOYSA-K trilithium;trioxido(oxo)-$l^{5}-arsane Chemical compound [Li+].[Li+].[Li+].[O-][As]([O-])([O-])=O VKJKOXNPYVUXNC-UHFFFAOYSA-K 0.000 description 1
MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 description 1
238000010792 warming Methods 0.000 description 1
238000003466 welding Methods 0.000 description 1
229910052724 xenon Inorganic materials 0.000 description 1
FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
239000004246 zinc acetate Substances 0.000 description 1
UGZADUVQMDAIAO-UHFFFAOYSA-L zinc hydroxide Chemical compound [OH-].[OH-].[Zn+2] UGZADUVQMDAIAO-UHFFFAOYSA-L 0.000 description 1
229910021511 zinc hydroxide Inorganic materials 0.000 description 1
229940007718 zinc hydroxide Drugs 0.000 description 1
DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1

Classifications

- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries

Landscapes

Battery Electrode And Active Subsutance (AREA)
Secondary Cells (AREA)

CA002331602A 1992-11-30 1993-11-26 Procede de fabrication d'un materiau actif pour electrode positive d'une batterie secondaire Expired - Fee Related CA2331602C (fr)

Applications Claiming Priority (13)

Application Number	Priority Date	Filing Date	Title
JP4320557A JP2943127B2 (ja)	1992-11-30	1992-11-30	二次電池
JP4-320559		1992-11-30
JP4320559A JP2771406B2 (ja)	1992-11-30	1992-11-30	二次電池
JP4-320557		1992-11-30
JP4320558A JP3067426B2 (ja)	1992-11-30	1992-11-30	リチウム二次電池と正極活物質の製造方法
JP4-320560		1992-11-30
JP4-320558		1992-11-30
JP32056092A JP3487556B2 (ja)	1992-11-30	1992-11-30	リチウム二次電池
JP34456392A JP3423338B2 (ja)	1992-12-24	1992-12-24	二次電池
JP4-344563		1992-12-24
JP07834293A JP3530544B2 (ja)	1992-09-14	1993-04-05	二次電池
JP5-078342		1993-04-05
CA002110097A CA2110097C (fr)	1992-11-30	1993-11-26	Batterie secondaire

Related Parent Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002110097A Division CA2110097C (fr)	1992-11-30	1993-11-26	Batterie secondaire

Publications (2)

Publication Number	Publication Date
CA2331602A1 CA2331602A1 (fr)	1994-05-31
CA2331602C true CA2331602C (fr)	2002-09-10

Family

ID=27560977

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002331602A Expired - Fee Related CA2331602C (fr)	1992-11-30	1993-11-26	Procede de fabrication d'un materiau actif pour electrode positive d'une batterie secondaire

Country Status (1)

Country	Link
CA (1)	CA2331602C (fr)

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* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
TWI290781B (en)	2004-09-02	2007-12-01	Lg Chemical Ltd	Electrode active material with multi-element based oxide layers and preparation method thereof
CN115036565B (zh) *	2016-08-04	2025-02-28	松下知识产权经营株式会社	固体电解质材料和电池
CN106450498A (zh) *	2016-12-28	2017-02-22	珠海市至力电池有限公司	包胶式可充电锂离子扣式电池
CN110371948B (zh) *	2019-07-23	2023-02-10	中国科学院福建物质结构研究所	一种碳纳米材料及其制备方法和应用
CN111841627B (zh) *	2020-06-12	2023-06-27	青岛科技大学	一类二氧化硅基材料负载聚醚功能化离子液体催化剂及其制备方法
CN114068869B (zh) *	2021-11-23	2023-08-29	安徽大学	一种核-壳结构硅@氧化亚硅/碳负极材料及其制备方法与应用
CN114188542B (zh) *	2021-12-09	2024-01-26	中南大学	一种锌基mof负载二氧化钒纳米材料及其制备和应用
CN114988493A (zh) *	2022-04-27	2022-09-02	中国石油大学(华东)	一种镍铁双金属氢氧化物的制备方法、产品及其应用
CN115588731A (zh) *	2022-09-21	2023-01-10	苏州清陶新能源科技有限公司	一种固态锂离子电池用正极片、制备方法及固态锂电池
CN115621436A (zh) *	2022-09-26	2023-01-17	上海空间电源研究所	高熵阳离子无序盐岩结构正极材料、制备方法及电池
CN115411253B (zh) *	2022-09-26	2025-01-28	兴储世纪科技股份有限公司	碳包覆一维氟化亚铁正极材料及其制备方法和应用
CN115621051A (zh) *	2022-10-31	2023-01-17	无锡零一未来新材料技术研究院有限公司	一种聚三苯胺-碳源复合材料及其应用
CN115784321B (zh) *	2022-11-23	2024-02-09	广东邦普循环科技有限公司	一种改性镍钴锰酸锂正极材料及其制备方法
CN116365054B (zh) *	2023-06-01	2023-08-18	蓝固(常州)新能源有限公司	一种水系固态电解质浆料、固态电解质隔膜及二次电池
CN117326552B (zh) *	2023-09-28	2025-07-15	蜂巢能源科技股份有限公司	废旧石墨的回收方法、纯化石墨及其应用
CN117626340B (zh) *	2023-11-14	2025-03-14	齐齐哈尔大学	三维菊花状CoMoO4@Ni3V/NF异质结构催化剂及其制备方法和应用
CN121215668B (zh) *	2025-12-01	2026-02-17	潍坊科技学院	一种蒽-芘/多孔碳复合材料及其制备方法和应用

1993
- 1993-11-26 CA CA002331602A patent/CA2331602C/fr not_active Expired - Fee Related

Also Published As

Publication number	Publication date
CA2331602A1 (fr)	1994-05-31

Legal Events

Date	Code	Title	Description
2001-01-08	EEER	Examination request
2014-01-07	MKLA	Lapsed	Effective date: 20131126

Publication	Publication Date	Title
CA2110097C (fr)	2002-07-09	Batterie secondaire
CA2331602C (fr)	2002-09-10	Procede de fabrication d'un materiau actif pour electrode positive d'une batterie secondaire
JP3717085B2 (ja)	2005-11-16	二次電池用負極、該負極を有する二次電池及び電極の作製方法
EP0690517B1 (fr)	2003-10-01	Pile au lithium rechargeable
JP3530544B2 (ja)	2004-05-24	二次電池
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