CA2435593C - Method and device for deionizing cooling media for fuel cells - Google Patents

Method and device for deionizing cooling media for fuel cells Download PDF

Info

Publication number: CA2435593C
Authority: CA; Canada
Prior art keywords: deionization; fuel cell; cell; cooling circuit; cooling
Prior art date: 2001-02-02
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA2435593A

Other languages

English (en)

French (fr)

Other versions

CA2435593A1 (en

Inventor

Claudius Kormann

Andreas Fischer

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

BASF SE

Original Assignee

BASF SE

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2001-02-02

Filing date

2002-02-01

Publication date

2010-06-22

2002-02-01 Application filed by BASF SE filed Critical BASF SE

2002-08-15 Publication of CA2435593A1 publication Critical patent/CA2435593A1/en

2010-06-22 Application granted granted Critical

2010-06-22 Publication of CA2435593C publication Critical patent/CA2435593C/en

2022-02-01 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

239000000446 fuel Substances 0.000 title claims abstract description 58
238000001816 cooling Methods 0.000 title claims abstract description 50
238000000034 method Methods 0.000 title claims abstract description 19
239000002826 coolant Substances 0.000 claims abstract description 40
239000012141 concentrate Substances 0.000 claims abstract description 33
238000002242 deionisation method Methods 0.000 claims abstract description 21
239000012528 membrane Substances 0.000 claims description 44
150000002500 ions Chemical class 0.000 claims description 39
238000009296 electrodeionization Methods 0.000 claims description 38
239000011347 resin Substances 0.000 claims description 26
229920005989 resin Polymers 0.000 claims description 26
150000001450 anions Chemical class 0.000 claims description 20
150000001768 cations Chemical class 0.000 claims description 20
238000011144 upstream manufacturing Methods 0.000 claims 1
238000012856 packing Methods 0.000 description 24
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 7
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
239000001257 hydrogen Substances 0.000 description 6
229910052739 hydrogen Inorganic materials 0.000 description 6
239000001301 oxygen Substances 0.000 description 6
229910052760 oxygen Inorganic materials 0.000 description 6
239000007789 gas Substances 0.000 description 5
230000008929 regeneration Effects 0.000 description 5
238000011069 regeneration method Methods 0.000 description 5
238000002485 combustion reaction Methods 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
239000003570 air Substances 0.000 description 3
239000007795 chemical reaction product Substances 0.000 description 3
230000007797 corrosion Effects 0.000 description 3
238000005260 corrosion Methods 0.000 description 3
238000000909 electrodialysis Methods 0.000 description 3
239000003792 electrolyte Substances 0.000 description 3
-1 hydroxyl ions Chemical class 0.000 description 3
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
239000007798 antifreeze agent Substances 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
239000000470 constituent Substances 0.000 description 2
238000010612 desalination reaction Methods 0.000 description 2
238000009792 diffusion process Methods 0.000 description 2
238000010494 dissociation reaction Methods 0.000 description 2
230000005593 dissociations Effects 0.000 description 2
230000005684 electric field Effects 0.000 description 2
239000003112 inhibitor Substances 0.000 description 2
238000012423 maintenance Methods 0.000 description 2
239000000203 mixture Substances 0.000 description 2
229910052605 nesosilicate Inorganic materials 0.000 description 2
150000004762 orthosilicates Chemical class 0.000 description 2
239000005518 polymer electrolyte Substances 0.000 description 2
229920005597 polymer membrane Polymers 0.000 description 2
239000000126 substance Substances 0.000 description 2
LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 2
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
229910000831 Steel Inorganic materials 0.000 description 1
BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
150000004703 alkoxides Chemical group 0.000 description 1
239000012080 ambient air Substances 0.000 description 1
230000002528 anti-freeze Effects 0.000 description 1
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
229910052794 bromium Inorganic materials 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
239000000460 chlorine Substances 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
239000008367 deionised water Substances 0.000 description 1
229910021641 deionized water Inorganic materials 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000003487 electrochemical reaction Methods 0.000 description 1
238000003411 electrode reaction Methods 0.000 description 1
239000003344 environmental pollutant Substances 0.000 description 1
125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
150000002334 glycols Chemical class 0.000 description 1
229910002804 graphite Inorganic materials 0.000 description 1
239000010439 graphite Substances 0.000 description 1
230000036571 hydration Effects 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000000463 material Substances 0.000 description 1
229910044991 metal oxide Inorganic materials 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
229910000510 noble metal Inorganic materials 0.000 description 1
239000002245 particle Substances 0.000 description 1
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 1
231100000719 pollutant Toxicity 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
239000013535 sea water Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
229910000077 silane Inorganic materials 0.000 description 1
150000004760 silicates Chemical class 0.000 description 1
125000006850 spacer group Chemical group 0.000 description 1
239000010959 steel Substances 0.000 description 1
UQMOLLPKNHFRAC-UHFFFAOYSA-N tetrabutyl silicate Chemical compound CCCCO[Si](OCCCC)(OCCCC)OCCCC UQMOLLPKNHFRAC-UHFFFAOYSA-N 0.000 description 1
SWQWONXMUXCEDF-UHFFFAOYSA-N tetrakis(2-ethylbutyl) silicate Chemical compound CCC(CC)CO[Si](OCC(CC)CC)(OCC(CC)CC)OCC(CC)CC SWQWONXMUXCEDF-UHFFFAOYSA-N 0.000 description 1
MQHSFMJHURNQIE-UHFFFAOYSA-N tetrakis(2-ethylhexyl) silicate Chemical compound CCCCC(CC)CO[Si](OCC(CC)CCCC)(OCC(CC)CCCC)OCC(CC)CCCC MQHSFMJHURNQIE-UHFFFAOYSA-N 0.000 description 1
ZUEKXCXHTXJYAR-UHFFFAOYSA-N tetrapropan-2-yl silicate Chemical compound CC(C)O[Si](OC(C)C)(OC(C)C)OC(C)C ZUEKXCXHTXJYAR-UHFFFAOYSA-N 0.000 description 1
ZQZCOBSUOFHDEE-UHFFFAOYSA-N tetrapropyl silicate Chemical compound CCCO[Si](OCCC)(OCCC)OCCC ZQZCOBSUOFHDEE-UHFFFAOYSA-N 0.000 description 1
BCLLLHFGVQKVKL-UHFFFAOYSA-N tetratert-butyl silicate Chemical compound CC(C)(C)O[Si](OC(C)(C)C)(OC(C)(C)C)OC(C)(C)C BCLLLHFGVQKVKL-UHFFFAOYSA-N 0.000 description 1
238000005809 transesterification reaction Methods 0.000 description 1
229910021642 ultra pure water Inorganic materials 0.000 description 1
239000012498 ultrapure water Substances 0.000 description 1

Classifications

- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
- H01M8/04007—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids related to heat exchange
- H01M8/04029—Heat exchange using liquids
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells

Landscapes

Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Manufacturing & Machinery (AREA)
Sustainable Development (AREA)
Sustainable Energy (AREA)
Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Electrochemistry (AREA)
General Chemical & Material Sciences (AREA)
Fuel Cell (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Physical Or Chemical Processes And Apparatus (AREA)
Water Treatment By Electricity Or Magnetism (AREA)

CA2435593A 2001-02-02 2002-02-01 Method and device for deionizing cooling media for fuel cells Expired - Fee Related CA2435593C (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DE10104771A DE10104771A1 (de)	2001-02-02	2001-02-02	Verfahren und Vorrichtung zum Entionisieren von Kühlmedien für Brennstoffzellen
DE10104771.1		2001-02-02
PCT/EP2002/001074 WO2002063707A2 (de)	2001-02-02	2002-02-01	Verfahren und vorrichtung zum entionisieren von kühlmedien für brennstoffzellen

Publications (2)

Publication Number	Publication Date
CA2435593A1 CA2435593A1 (en)	2002-08-15
CA2435593C true CA2435593C (en)	2010-06-22

Family

ID=7672665

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA2435593A Expired - Fee Related CA2435593C (en)	2001-02-02	2002-02-01	Method and device for deionizing cooling media for fuel cells

Country Status (9)

Country	Link
US (2)	US7235319B2 (de)
EP (1)	EP1407506B1 (de)
JP (1)	JP4460832B2 (de)
AT (1)	ATE324675T1 (de)
CA (1)	CA2435593C (de)
DE (2)	DE10104771A1 (de)
ES (1)	ES2261653T3 (de)
PT (1)	PT1407506E (de)
WO (1)	WO2002063707A2 (de)

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DE102008054370A1 (de)	2008-12-08	2010-06-10	Robert Bosch Gmbh	Wartungsfreie und kontinuierliche Kühlmittelaufbereitung in Brennstoffzellenfahrzeugen mittels Elektro-Deionisation (EDI) mit vorteilhafter Ionenentnahme
DE102008044413B4 (de)	2008-12-08	2023-05-25	Robert Bosch Gmbh	Wartungsfreie und kontinuierliche Kühlmittelaufbereitung in Brennstoffzellenfahrzeugen mittels Elektro-Deionisation (EDI) in vorteilhafter Anordnung
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GB2505957B (en)	2012-09-18	2021-04-07	Intelligent Energy Ltd	Coolant fluid feed to fuel cell stacks
BR112019010016B1 (pt)	2016-11-23	2023-11-14	Basf Se	Composição de refrigerante, método para produzir composições de refrigerante, e, uso de uma composição de refrigerante
DE102017010040A1 (de)	2017-10-27	2019-05-02	Daimler Ag	Kühlkreislauf für wenigstens eine Brennstoffzelle
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2001
- 2001-02-02 DE DE10104771A patent/DE10104771A1/de not_active Withdrawn
2002
- 2002-02-01 US US10/466,562 patent/US7235319B2/en not_active Expired - Fee Related
- 2002-02-01 EP EP02716714A patent/EP1407506B1/de not_active Expired - Lifetime
- 2002-02-01 AT AT02716714T patent/ATE324675T1/de active
- 2002-02-01 PT PT02716714T patent/PT1407506E/pt unknown
- 2002-02-01 WO PCT/EP2002/001074 patent/WO2002063707A2/de not_active Ceased
- 2002-02-01 DE DE50206585T patent/DE50206585D1/de not_active Expired - Lifetime
- 2002-02-01 JP JP2002563550A patent/JP4460832B2/ja not_active Expired - Fee Related
- 2002-02-01 ES ES02716714T patent/ES2261653T3/es not_active Expired - Lifetime
- 2002-02-01 CA CA2435593A patent/CA2435593C/en not_active Expired - Fee Related
2007
- 2007-05-23 US US11/802,476 patent/US7976998B2/en not_active Expired - Fee Related

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Publication number	Publication date
US7976998B2 (en)	2011-07-12
EP1407506A2 (de)	2004-04-14
JP4460832B2 (ja)	2010-05-12
DE50206585D1 (de)	2006-06-01
US7235319B2 (en)	2007-06-26
WO2002063707A3 (de)	2004-01-22
EP1407506B1 (de)	2006-04-26
WO2002063707A2 (de)	2002-08-15
DE10104771A1 (de)	2002-08-08
US20070259237A1 (en)	2007-11-08
JP2004526280A (ja)	2004-08-26
ATE324675T1 (de)	2006-05-15
CA2435593A1 (en)	2002-08-15
US20040028963A1 (en)	2004-02-12
ES2261653T3 (es)	2006-11-16
PT1407506E (pt)	2006-08-31

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2014-03-17	MKLA	Lapsed	Effective date: 20140203

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