CA2597630C - Composition et procede de preparation de revetements de protection sur des substrats metalliques - Google Patents

Composition et procede de preparation de revetements de protection sur des substrats metalliques Download PDF

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Publication number
CA2597630C
CA2597630C CA2597630A CA2597630A CA2597630C CA 2597630 C CA2597630 C CA 2597630C CA 2597630 A CA2597630 A CA 2597630A CA 2597630 A CA2597630 A CA 2597630A CA 2597630 C CA2597630 C CA 2597630C
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CA
Canada
Prior art keywords
glycol
grams
water
compound
compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CA2597630A
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English (en)
Other versions
CA2597630A1 (fr
Inventor
Craig A. Matzdorf
William C. Nickerson, Jr.
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
US Department of Navy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/076,106 external-priority patent/US20060180247A1/en
Priority claimed from US11/058,715 external-priority patent/US20100032060A1/en
Priority claimed from US11/116,166 external-priority patent/US20060240191A1/en
Priority claimed from US11/116,165 external-priority patent/US7811391B2/en
Application filed by US Department of Navy filed Critical US Department of Navy
Publication of CA2597630A1 publication Critical patent/CA2597630A1/fr
Application granted granted Critical
Publication of CA2597630C publication Critical patent/CA2597630C/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/82—After-treatment
    • C23C22/83—Chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C21/00—Alloys based on aluminium
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/73—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
    • C23C22/77—Controlling or regulating of the coating process
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2222/00—Aspects relating to chemical surface treatment of metallic material by reaction of the surface with a reactive medium
    • C23C2222/10—Use of solutions containing trivalent chromium but free of hexavalent chromium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Paints Or Removers (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

Cette invention concerne une solution aqueuse acide utilisée pour traiter des substrats métalliques pour améliorer la liaison adhésive et la protection contre la corrosion de la surface métallique, laquelle solution comprend des quantités efficaces de composés chrome trivalent hydrosolubles, des fluorozirconates, des quantités efficaces d'au moins un inhibiteur de corrosion tel que le benzotriazole, des composés fluorométalliques, des composés zinc, des agents épaississants, des tensioactifs et au moins environ 0,001 mole par litre de la solution acide d'un composé polyhydroxy et/ou carboxylique comme agent stabilisant pour la solution aqueuse.
CA2597630A 2005-02-15 2005-11-14 Composition et procede de preparation de revetements de protection sur des substrats metalliques Expired - Lifetime CA2597630C (fr)

Applications Claiming Priority (9)

Application Number Priority Date Filing Date Title
US11/076,106 2005-02-15
US11/058,715 2005-02-15
US11/076,106 US20060180247A1 (en) 2005-02-15 2005-02-15 Process for preparing chromium conversion coatings for iron and iron alloys
US11/058,715 US20100032060A1 (en) 2005-02-15 2005-02-15 Process for preparing chromium conversion coatings for magnesium alloys
US11/116,166 US20060240191A1 (en) 2005-04-21 2005-04-21 Composition and process for preparing chromium-zirconium coatings on metal substrates
US11/116,166 2005-04-21
US11/116,165 US7811391B2 (en) 2005-04-21 2005-04-21 Composition and process for preparing protective coatings on metal substrates
US11/116,165 2005-04-21
PCT/US2005/041587 WO2006088521A2 (fr) 2005-02-15 2005-11-14 Composition et procede de preparation de revetements de protection sur des substrats metalliques

Publications (2)

Publication Number Publication Date
CA2597630A1 CA2597630A1 (fr) 2006-08-24
CA2597630C true CA2597630C (fr) 2015-09-29

Family

ID=36916893

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2597630A Expired - Lifetime CA2597630C (fr) 2005-02-15 2005-11-14 Composition et procede de preparation de revetements de protection sur des substrats metalliques

Country Status (10)

Country Link
EP (1) EP1863952B1 (fr)
JP (1) JP5060964B2 (fr)
KR (1) KR20080000564A (fr)
AU (1) AU2005327548A1 (fr)
BR (1) BRPI0519981B1 (fr)
CA (1) CA2597630C (fr)
DK (1) DK1863952T3 (fr)
ES (1) ES2411429T3 (fr)
MX (1) MX2007009801A (fr)
WO (1) WO2006088521A2 (fr)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110020237A (ko) * 2008-04-25 2011-03-02 헨켈 아게 운트 코 카게아아 아연 도금 강을 처리하기 위한 3가 크롬 부동태화제
US8591670B2 (en) 2008-05-07 2013-11-26 Bulk Chemicals, Inc. Process and composition for treating metal surfaces using trivalent chromium compounds
DE102009028025A1 (de) * 2009-07-27 2011-02-03 Henkel Ag & Co. Kgaa Mehrstufiges Verfahren zur Behandlung von Metalloberflächen vor einer Tauchlackierung
EP2711444A1 (fr) 2012-09-20 2014-03-26 Coventya SAS Solution aqueuse alcaline pour améliorer la résistance à la corrosion d'un revêtement de conversion Cr(III), procédé de production d'un tel revêtement et son utilisation
US10156016B2 (en) 2013-03-15 2018-12-18 Henkel Ag & Co. Kgaa Trivalent chromium-containing composition for aluminum and aluminum alloys
CN107109659B (zh) * 2014-12-26 2020-05-05 迪普索股份公司 锌或锌合金基材用3价铬化成处理液和化成被膜
US10435806B2 (en) 2015-10-12 2019-10-08 Prc-Desoto International, Inc. Methods for electrolytically depositing pretreatment compositions
JP7399080B2 (ja) * 2017-05-12 2023-12-15 ケメオン サーフェス テクノロジー， エルエルシー ｐＨ安定な三価クロムコーティング液
EP3746580A1 (fr) * 2018-01-30 2020-12-09 PRC-Desoto International, Inc. Systèmes et procédés de traitement d'un substrat métallique
JP7118402B2 (ja) * 2018-04-26 2022-08-16 奥野製薬工業株式会社 アルミニウム合金の陽極酸化皮膜用封孔処理液、濃縮液及び封孔処理方法
SG11202107824XA (en) * 2019-02-21 2021-08-30 Mec Co Ltd Adhesive composition, method for producing surface-treated metal member, and method for producing metal-resin composite body
MX2022007699A (es) * 2019-12-20 2022-07-19 Atotech Deutschland Gmbh & Co Kg Composicion de pasivacion y metodo para depositar una capa de pasivacion que comprende cromo sobre un sustrato recubierto de zinc o de zinc-niquel.
WO2022167624A1 (fr) * 2021-02-05 2022-08-11 Atotech Deutschland GmbH & Co. KG Procédé de dépôt de couche de passivation comprenant du chrome sur un revêtement comprenant du zinc
EP4423312A1 (fr) * 2021-10-27 2024-09-04 PRC-Desoto International, Inc. Compositions, systèmes et procédés de traitement d'un substrat

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4578122A (en) * 1984-11-14 1986-03-25 Omi International Corporation Non-peroxide trivalent chromium passivate composition and process
DE3521952A1 (de) * 1985-06-20 1987-01-02 Henkel Kgaa Waessrige zusammensetzungen fuer den hilite- und flux-prozess und ihre verwendung
DE3783173T2 (de) * 1986-07-23 1993-04-22 Fuji Photo Film Co Ltd Verfahren zur behandlung eines farbphotographischen silberhalogenidmaterials und farbentwickler.
JPH0225592A (ja) * 1988-07-14 1990-01-29 Fujitsu Ltd 陽極酸化皮膜の封孔処理方法
JPH07100873B2 (ja) * 1989-09-27 1995-11-01 日本パーカライジング株式会社 亜鉛系メッキ鋼板のクロメート塗布液
US5226976A (en) * 1991-04-15 1993-07-13 Henkel Corporation Metal treatment
DE19615664A1 (de) * 1996-04-19 1997-10-23 Surtec Produkte Und Systeme Fu Chrom(VI)freie Chromatschicht sowie Verfahren zu ihrer Herstellung
US6068710A (en) * 1996-11-27 2000-05-30 Henkel Corporation Aqueous composition and process for preparing metal substrate for cold forming
JP3391252B2 (ja) * 1998-03-26 2003-03-31 日本軽金属株式会社 電着塗装アルミ材の製造方法
JP2002075767A (ja) * 2000-08-31 2002-03-15 Sumitomo Special Metals Co Ltd 耐食性被膜を有する希土類系永久磁石およびその製造方法
EP1330498B1 (fr) * 2000-10-11 2006-05-24 Chemetall GmbH Procede pour enduire des surfaces metalliques avec une composition aqueuse, composition aqueuse et utilisation des substrats ainsi revetus
US6511532B2 (en) * 2000-10-31 2003-01-28 The United States Of America As Represented By The Secretary Of The Navy Post-treatment for anodized aluminum
US6527841B2 (en) * 2000-10-31 2003-03-04 The United States Of America As Represented By The Secretary Of The Navy Post-treatment for metal coated substrates
US6669764B1 (en) * 2000-10-31 2003-12-30 The United States Of America As Represented By The Secretary Of The Navy Pretreatment for aluminum and aluminum alloys
US6663700B1 (en) * 2000-10-31 2003-12-16 The United States Of America As Represented By The Secretary Of The Navy Post-treatment for metal coated substrates
JP2002212746A (ja) * 2001-01-11 2002-07-31 Okuno Chem Ind Co Ltd 未貫通穴を有する被めっき物への無電解ニッケルめっき方法
WO2003060019A1 (fr) * 2002-01-04 2003-07-24 University Of Dayton Pigments anticorrosion non toxiques a base de cobalt
JP3774415B2 (ja) * 2002-03-14 2006-05-17 ディップソール株式会社 亜鉛及び亜鉛合金めっき上に黒色の六価クロムフリー化成皮膜を形成するための処理溶液及び亜鉛及び亜鉛合金めっき上に黒色の六価クロムフリー化成皮膜を形成する方法。
JP2003306756A (ja) * 2002-04-18 2003-10-31 Jfe Steel Kk 溶融亜鉛めっき鋼板とその製造方法
JP2004083771A (ja) * 2002-08-28 2004-03-18 Nippon Hyomen Kagaku Kk 金属保護被膜形成用組成物
DE10310972A1 (de) * 2003-03-13 2004-09-23 Basf Ag Stickstoffhaltige Polymere für die Metalloberflächenbehandlung

Also Published As

Publication number Publication date
WO2006088521A3 (fr) 2007-10-18
EP1863952A4 (fr) 2010-01-13
DK1863952T3 (da) 2013-03-25
WO2006088521A2 (fr) 2006-08-24
BRPI0519981B1 (pt) 2016-03-08
EP1863952A2 (fr) 2007-12-12
BRPI0519981A2 (pt) 2009-08-18
JP5060964B2 (ja) 2012-10-31
ES2411429T3 (es) 2013-07-05
KR20080000564A (ko) 2008-01-02
AU2005327548A1 (en) 2006-08-24
MX2007009801A (es) 2007-10-03
EP1863952B1 (fr) 2013-03-06
CA2597630A1 (fr) 2006-08-24
JP2008537975A (ja) 2008-10-02

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