CH130321A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH130321A CH130321A CH130321DA CH130321A CH 130321 A CH130321 A CH 130321A CH 130321D A CH130321D A CH 130321DA CH 130321 A CH130321 A CH 130321A
- Authority
- CH
- Switzerland
- Prior art keywords
- azo dye
- preparation
- dye
- red
- naphthylamide
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title description 3
- 238000002360 preparation method Methods 0.000 title description 3
- 239000000975 dye Substances 0.000 claims description 4
- CPICBCWZPCRRHM-UHFFFAOYSA-N 3,5-dichloro-2,4-dimethylaniline Chemical compound ClC=1C(=C(C(=C(C1)N)C)Cl)C CPICBCWZPCRRHM-UHFFFAOYSA-N 0.000 claims description 2
- 150000008049 diazo compounds Chemical class 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000007900 aqueous suspension Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung eines Azofarbstoffes. Gegenstand der vorliegenden Erfindung ist ein Verfahren zur Darstellung eines Azo- farbstoffes, den man durch Kupplung der Dir.zoverbindung von 1.3-Dirnethyl-4-amino- 2.6-dichlorbenzol mit 2-Oxyriaphtalin-3-car- bonsäure-c,-naphtylamid erhält.
Beispiel: Die aus<B>19</B> kg 1.3-Dimethyl-4-amino- I . 6-dichlorbenzol in üblicher Weise darge stellte Diazoverbindung lässt man unter Rüh ren in eine wässerige Suspension von S 1 kg 2-Oxynaphtalin-3-c arbunsärire-a-naphtylamid, bereitet durch Auflösen desselben in Natron lauge und Wiederausfällen mit verdünnter Essigsäure, einlaufen. Der Farbstoff scheidet sich als roter Niederschlag aus. Er wird filtriert, gewaschen und getrocknet.
Der Farbstoff soll besonders als Entwick lungsfarbstoff verwendet werden. Er gibt ein blaustichiges Rot und besitzt die wichtige Eigenschaft, dass er zur Erzeugung von ganz hervorragend lichtechten und laugenkoch- echten blaustichig-roten Tönen dienen kann.
Process for the preparation of an azo dye. The present invention relates to a process for the preparation of an azo dye which is obtained by coupling the Dir.zo compound of 1,3-dimethyl-4-amino-2,6-dichlorobenzene with 2-oxyriaphthalene-3-carboxylic acid-c, -naphthylamide .
Example: The one from <B> 19 </B> kg of 1,3-dimethyl-4-amino-I. 6-dichlorobenzene in the usual way presented diazo compound is allowed to run into an aqueous suspension of S 1 kg of 2-oxynaphthalene-3-carbunsärire-a-naphthylamide, prepared by dissolving it in sodium hydroxide solution and reprecipitating it with dilute acetic acid, with stirring. The dye separates out as a red precipitate. It is filtered, washed and dried.
The dye should be used especially as a developing dye. It gives a bluish red and has the important property that it can be used to produce very excellent lightfast and caustic-blue-tinged red tones.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE130321X | 1926-07-09 | ||
| CH127528T | 1927-07-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH130321A true CH130321A (en) | 1928-11-30 |
Family
ID=25710901
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH130321D CH130321A (en) | 1926-07-09 | 1927-07-08 | Process for the preparation of an azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH130321A (en) |
-
1927
- 1927-07-08 CH CH130321D patent/CH130321A/en unknown
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