CH134848A - Process for the preparation of a water-insoluble azo dye. - Google Patents
Process for the preparation of a water-insoluble azo dye.Info
- Publication number
- CH134848A CH134848A CH134848DA CH134848A CH 134848 A CH134848 A CH 134848A CH 134848D A CH134848D A CH 134848DA CH 134848 A CH134848 A CH 134848A
- Authority
- CH
- Switzerland
- Prior art keywords
- water
- preparation
- azo dye
- insoluble azo
- mol
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 150000008049 diazo compounds Chemical class 0.000 claims description 3
- 239000000975 dye Substances 0.000 claims description 2
- 239000003973 paint Substances 0.000 claims description 2
- 229920000742 Cotton Polymers 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- OCISOSJGBCQHHN-UHFFFAOYSA-N 3-hydroxynaphthalene-1-carboxylic acid Chemical compound C1=CC=C2C(C(=O)O)=CC(O)=CC2=C1 OCISOSJGBCQHHN-UHFFFAOYSA-N 0.000 description 2
- WTASPHLDOOZONQ-UHFFFAOYSA-L O.[Al+3].S(=O)(=O)([O-])[O-].[Ba+2] Chemical compound O.[Al+3].S(=O)(=O)([O-])[O-].[Ba+2] WTASPHLDOOZONQ-UHFFFAOYSA-L 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Verfahren zur Darstellung eines wasserunlöslichen Azofarbstoffes. Gegenstand des vorliegenden Patentes ist ein Verfahren zur Darstellung eines wasser unlöslichen Azofarbstoffes, dadurch gekenn zeichnet, dass man 1 Mol 2.3-Oxynaphtoe- säure-5-chlor-2-toluidid (CHa = 1,NH = 2) mit 1 Mol der Diazoverbindung von Methyl- benzoylamino-as-m-gylindi n
EMI0001.0012
kuppelt.
<I>Beispiel:</I> 2,97 Gewichtsteile 2.3-Oxynaphtoesäure 5-chlor-2-toluidid werden mit Natronlauge in 300 Gewichtsteilen Wasser gelöst und<B>100</B> Teile Substrat, zum Beispiel Aluminium hydrat-Bariumsulfat zugegeben. Hierauf wird in bekannter Weise mit der Diazoverbindung aus 2,54 Grewichtsteilen Methylbenzoylamino- as-m-gylidin
EMI0001.0019
gekuppelt. Nach Beendigung der Kupplung wird gewaschen, filtriert und getrocknet. Man erhält einen blaustichigroten Lack. Der Farbstoff lässt sich in bekannter Weise auch auf der Faser kuppeln.
Process for the preparation of a water-insoluble azo dye. The present patent is a process for the preparation of a water-insoluble azo dye, characterized in that 1 mol of 2,3-oxynaphthoic acid 5-chloro-2-toluidide (CHa = 1, NH = 2) with 1 mol of the diazo compound of Methyl benzoylamino-as-m-gylindi n
EMI0001.0012
clutch.
<I> Example: </I> 2.97 parts by weight of 2,3-oxynaphthoic acid 5-chloro-2-toluidide are dissolved in 300 parts by weight of water with sodium hydroxide solution and <B> 100 </B> parts of substrate, for example aluminum hydrate barium sulfate, are added . Then in a known manner with the diazo compound from 2.54 parts by weight of methylbenzoylamino-as-m-gylidine
EMI0001.0019
coupled. After the coupling has ended, it is washed, filtered and dried. A bluish-tinged red paint is obtained. The dye can also be coupled to the fiber in a known manner.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE134848X | 1927-01-25 | ||
| CH134100T | 1928-01-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH134848A true CH134848A (en) | 1929-08-15 |
Family
ID=25712235
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH134848D CH134848A (en) | 1927-01-25 | 1928-01-17 | Process for the preparation of a water-insoluble azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH134848A (en) |
-
1928
- 1928-01-17 CH CH134848D patent/CH134848A/en unknown
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