CH166086A - Process for the production of a new metal-containing dye. - Google Patents
Process for the production of a new metal-containing dye.Info
- Publication number
- CH166086A CH166086A CH166086DA CH166086A CH 166086 A CH166086 A CH 166086A CH 166086D A CH166086D A CH 166086DA CH 166086 A CH166086 A CH 166086A
- Authority
- CH
- Switzerland
- Prior art keywords
- containing dye
- production
- new metal
- sulfo
- dye
- Prior art date
Links
- 229910052751 metal Inorganic materials 0.000 title claims description 6
- 239000002184 metal Substances 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 7
- 239000000987 azo dye Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 229910052804 chromium Inorganic materials 0.000 claims description 2
- 239000011651 chromium Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 230000002378 acidificating effect Effects 0.000 claims 1
- 239000002253 acid Substances 0.000 description 2
- GRGSHONWRKRWGP-UHFFFAOYSA-N 2-amino-4-sulfobenzoic acid Chemical compound NC1=CC(S(O)(=O)=O)=CC=C1C(O)=O GRGSHONWRKRWGP-UHFFFAOYSA-N 0.000 description 1
- 150000001845 chromium compounds Chemical class 0.000 description 1
- GRWVQDDAKZFPFI-UHFFFAOYSA-H chromium(III) sulfate Chemical compound [Cr+3].[Cr+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GRWVQDDAKZFPFI-UHFFFAOYSA-H 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C09B45/16—Monoazo compounds containing chromium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. 163542. Verfahren zur Herstellung eines neuen metallhaltigen Farbstoffes. Es wurde gefunden, dass man einen neuen metallhaltigen Farbstoff erhalten kann, wenn man den Azofarbstoff aus diazotierter 4-Sulfo- 2-aminobenzol-l-karbonsäure und 1-(3'-Sulfo-) phenyl-3-inethyl-5-pyrazolon mit chromab gebenden Mitteln behandelt.
Der erhaltene metallhaltige Farbstoff stellt ein braungelbes Pulver dar, das sich in Wasser mit gelber Farbe löst und Wolle aus saurem Bade in gleichmässigen echten gelben Tönen färbt. <I>Beispiel:</I> 52,6 'feile des Azofarbstoffes aus diazo- tierter 4-Sulfo-2-aminobenzol-l-karborisäure und 1-(3'-Sulfo-)pheriyl-3-methyl-5-pyrazolon werden mit 300 Teilen Wasser und 120 Teilen einer 18 o/oigen Chromsulfatlösung mehrere Stunden unter Rückfluss zum Sieden erhitzt.
Die nach dem Abkühlen sich ab scheidende Chromverbindung wird abfiltriert und getrocknet.
Additional patent to main patent No. 163542. Process for the production of a new metal-containing dye. It has been found that a new metal-containing dye can be obtained by using the azo dye from diazotized 4-sulfo-2-aminobenzene-1-carboxylic acid and 1- (3'-sulfo) phenyl-3-ynethyl-5-pyrazolone treated with chromium donating agents.
The metal-containing dye obtained is a brown-yellow powder which dissolves in water with a yellow color and dyes wool from an acid bath in uniform, genuine yellow tones. <I> Example: </I> 52.6 'file of the azo dye from diazo- tated 4-sulfo-2-aminobenzene-1-carboric acid and 1- (3'-sulfo-) pheriyl-3-methyl-5-pyrazolone are refluxed for several hours with 300 parts of water and 120 parts of an 18% chromium sulfate solution.
The chromium compound which separates out after cooling is filtered off and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH166086T | 1932-07-20 | ||
| CH163542T | 1932-07-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH166086A true CH166086A (en) | 1933-12-15 |
Family
ID=25717803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH166086D CH166086A (en) | 1932-07-20 | 1932-07-20 | Process for the production of a new metal-containing dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH166086A (en) |
-
1932
- 1932-07-20 CH CH166086D patent/CH166086A/en unknown
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