CH168024A - Process for the production of a new anthraquinone derivative. - Google Patents
Process for the production of a new anthraquinone derivative.Info
- Publication number
- CH168024A CH168024A CH168024DA CH168024A CH 168024 A CH168024 A CH 168024A CH 168024D A CH168024D A CH 168024DA CH 168024 A CH168024 A CH 168024A
- Authority
- CH
- Switzerland
- Prior art keywords
- anthraquinone derivative
- production
- new anthraquinone
- new
- green
- Prior art date
Links
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 title claims description 5
- 150000004056 anthraquinones Chemical class 0.000 title claims description 5
- 239000000975 dye Substances 0.000 claims description 5
- CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 claims description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 241001101998 Galium Species 0.000 description 1
- JLTDJTHDQAWBAV-UHFFFAOYSA-N N,N-dimethylaniline Chemical compound CN(C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-N 0.000 description 1
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/16—Amino-anthraquinones
- C09B1/20—Preparation from starting materials already containing the anthracene nucleus
- C09B1/26—Dyes with amino groups substituted by hydrocarbon radicals
- C09B1/32—Dyes with amino groups substituted by hydrocarbon radicals substituted by aryl groups
- C09B1/325—Dyes with no other substituents than the amino groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr. 166223. Verfahren zur Herstellung eines neuen Anthrachinonderivates. Es wurde gefunden, dass man ein neues Anthrachinonderivat erhält, wenn man 1-p Oxyäthylamino-4-bromanthrachinon mit 1.4- Diaminobenzol umsetzt, wobei 1 Mol 1.4-Dia- minobenzol mit einem Mol des Anthrachinon- derivates reagiert.
Der Farbstoff bildet ein dunkles Pulver, löst sich in organischen Lösungsmitteln mit grüner Farbe und färbt Acetatseide nach geeigneter Verpastung in grünen Tönen. <I>Beispiel:</I> 50 Teile 1-ss-Oxyäthylamino-4-bromanthra- chinon werden in 250 Teilen Dimethylanilin mit 75 Teilen 1.4-Diaminobenzol, 0,5 Teilen Kupferchlorür und 40 Teilen galiumacetat ca. 3 r/$ Stunden auf 110-120 erwärmt.
Nan fällt mit 350 Teilen Methylalkohol und erhält in vorzüglicher Reinheit ein Produkt, welches Acetatseide nach geeigneter Verpa- stung in reinen, grünen Tönen färbt.
<B> Additional patent </B> to main patent no. 166223. Process for the production of a new anthraquinone derivative. It has been found that a new anthraquinone derivative is obtained if 1-p oxyethylamino-4-bromoanthraquinone is reacted with 1,4-diaminobenzene, 1 mol of 1,4-diamino benzene reacting with one mole of the anthraquinone derivative.
The dye forms a dark powder, dissolves in organic solvents with a green color and, after suitable pasting, dyes acetate silk in green tones. <I> Example: </I> 50 parts of 1-ss-oxyethylamino-4-bromanthraquinone in 250 parts of dimethylaniline with 75 parts of 1,4-diaminobenzene, 0.5 part of copper chloride and 40 parts of galium acetate are approx. 3 hours heated to 110-120.
Nan falls with 350 parts of methyl alcohol and receives a product of excellent purity which, after suitable pasting, dyes acetate silk in pure, green tones.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH168024T | 1932-09-20 | ||
| CH166223T | 1934-02-06 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH168024A true CH168024A (en) | 1934-03-15 |
Family
ID=25718255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH168024D CH168024A (en) | 1932-09-20 | 1932-09-20 | Process for the production of a new anthraquinone derivative. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH168024A (en) |
-
1932
- 1932-09-20 CH CH168024D patent/CH168024A/en unknown
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