CH174899A - Process for the production of a new vat dye. - Google Patents
Process for the production of a new vat dye.Info
- Publication number
- CH174899A CH174899A CH174899DA CH174899A CH 174899 A CH174899 A CH 174899A CH 174899D A CH174899D A CH 174899DA CH 174899 A CH174899 A CH 174899A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- new
- vat dye
- dye
- new vat
- Prior art date
Links
- 239000000984 vat dye Substances 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 4
- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 claims description 2
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- 229960000583 acetic acid Drugs 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B7/00—Indigoid dyes
- C09B7/10—Bis-thionapthene indigos
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. <B>172735.</B> Verfahren zur Herstellung eines neuen Küpenfarbstoffes. Es wurde gefunden, dass man einen neuen Küpenfarbstoff erhält, wenn man 4. 6-Dimethyl-5. 7-dibrom-3-oxythionaplithen mit dem 2-(p-Dimethylamino-)-anil des 5- Chl(>r-7-methyl-3-oxythionaphi-hens kondeyl- siert.
Der neue Farbstoff der Formel.
EMI0001.0012
stellt ein rotviolettes Pulver dar, das sich in konzentrierter Schwefelsäure mit grüner Farbe löst und Baumwolle aus grüngelb gefärbter Küpe in beuehechten, reinen, vio letten Tönen färbt.
<I>Beispiel:</I> <B>336</B> Teile 4.6-Dimethyl-5.7-dibrom- 3-oxythiona,phthen und<B>330,5</B> Teile 2-(p- Dimethy,lamino)-anil des 5-Chlor-7-metliyl- 3-oxythionaplithens werden mit 4000 Volum- teilen Eisessig auf dem Wasserbade erhitzt, bis die Kondensation beendigt ist. Dann wird filtriert, gewaselien und getroaknet.
Additional patent to main patent no. <B> 172735. </B> Process for the production of a new vat dye. It has been found that a new vat dye is obtained if 4. 6-dimethyl-5. 7-dibromo-3-oxythionaplithen condensed with 2- (p-dimethylamino-) - anil des 5-Chl (> r-7-methyl-3-oxythionaphi-hens.
The new dye in the formula.
EMI0001.0012
is a red-violet powder that dissolves in concentrated sulfuric acid with a green color and dyes cotton from a green-yellow vat in blue, pure, violet tones.
<I> Example: </I> <B> 336 </B> parts 4.6-dimethyl-5.7-dibromo-3-oxythiona, phthene and <B> 330.5 </B> parts 2- (p-dimethy, lamino) -anil of 5-chloro-7-methyl-3-oxythionaplithene are heated with 4000 parts by volume of glacial acetic acid in a water bath until the condensation has ended. Then it is filtered, washed and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH174899T | 1933-09-22 | ||
| CH172735T | 1933-09-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH174899A true CH174899A (en) | 1935-01-31 |
Family
ID=25719267
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH174899D CH174899A (en) | 1933-09-22 | 1933-09-22 | Process for the production of a new vat dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH174899A (en) |
-
1933
- 1933-09-22 CH CH174899D patent/CH174899A/en unknown
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