CH193254A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH193254A CH193254A CH193254DA CH193254A CH 193254 A CH193254 A CH 193254A CH 193254D A CH193254D A CH 193254DA CH 193254 A CH193254 A CH 193254A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- production
- acidic
- blue
- wool dye
- Prior art date
Links
- 210000002268 wool Anatomy 0.000 title claims description 6
- 230000002378 acidificating effect Effects 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000000975 dye Substances 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 3
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B17/00—Azine dyes
- C09B17/04—Azine dyes of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr. 189649. verfahren zur Herstellung eines sauren Wollfarbstoffes. Gegenstand vorliegenden Patentes ist ein Verfahren zur Herstellung eines sauren Wollfarbstoffes, das dadurch gekennzeich net ist, dass man den Farbstoff der Formel:
EMI0001.0003
mit. einem sulfonierenden Mittel behandelt.
Der neue Farbstoff, der zwei Sulfogrup- pen im Molekül enthält, löst sich in konzen trierter Schwefelsäure grün, in Wasser blau und färbt Wolle in blauen Tönen von guter Licht- und Alkaliechtheit und gutem Egali- sierungsvermögen. <I>Beispiel:</I> Zwecks Sulfonierung wird der Farbstoff der Formel:
EMI0001.0010
mit der fünffachen Menge 32%igen Oleums mehrere Stunden auf<B>80'</B> erhitzt, bis sich eine Probe in verdünnter Natriumacetat- lösung ohne Rückstand löst.
Die Aufarbei tung und Überführung in das Natriumsalz erfolgt in üblicher Weise. Der Farbstoff ent hält zwei Sulfogruppen im Molekül. Er löst sich in konzentrierter Schwefelsäure grün, in Wasser blau und färbt Wolle in blauen Tönen von guter Licht- und Alkaliechtheit und gutem Egalisierungsvermögen.
<B> Additional patent </B> to main patent no. 189649. Process for the production of an acidic wool dye. The subject of the present patent is a process for the preparation of an acidic wool dye, which is characterized in that the dye of the formula:
EMI0001.0003
With. treated with a sulfonating agent.
The new dye, which contains two sulfo groups in the molecule, dissolves green in concentrated sulfuric acid, blue in water and dyes wool in blue shades of good lightfastness and alkali fastness and good leveling properties. <I> Example: </I> For the purpose of sulfonation, the dye of the formula:
EMI0001.0010
heated to <B> 80 '</B> for several hours with five times the amount of 32% oleum until a sample dissolves in dilute sodium acetate solution without residue.
The processing and conversion into the sodium salt is carried out in the usual way. The dye contains two sulfo groups in the molecule. It dissolves green in concentrated sulfuric acid, blue in water and dyes wool in blue shades of good lightfastness and alkali fastness and good leveling power.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH189649T | 1936-04-11 | ||
| CH193254T | 1936-04-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH193254A true CH193254A (en) | 1937-09-30 |
Family
ID=25721834
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH193254D CH193254A (en) | 1936-04-11 | 1936-04-11 | Process for the production of an acidic wool dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH193254A (en) |
-
1936
- 1936-04-11 CH CH193254D patent/CH193254A/en unknown
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