CH193263A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH193263A CH193263A CH193263DA CH193263A CH 193263 A CH193263 A CH 193263A CH 193263D A CH193263D A CH 193263DA CH 193263 A CH193263 A CH 193263A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- production
- acidic
- wool dye
- wool
- Prior art date
Links
- 210000002268 wool Anatomy 0.000 title claims description 7
- 230000002378 acidificating effect Effects 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000000975 dye Substances 0.000 claims description 12
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B17/00—Azine dyes
- C09B17/04—Azine dyes of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. 189649. Verfahren zur Herstellung eines sauren Wollfarbstoffes. Gegenstand vorliegenden Patentes ist ein Verfahren zur Herstellung eines sauren Wollfarbstoffes, das dadurch gekennzeichnet ist, dass man den Farbstoff der Formel:
EMI0001.0004
mit einem sulfonierenden Mittel behandelt. Der neue Farbstoff, der zwei Sulfogrup- pen im Molekül enthält, löst sich in konzen trierter Schwefelsäure mit grüner, in Wasser mit blauer Farbe und färbt Wolle in blauen Tönen von guten Echtheitseigenschaften.
Beispiel: Der Farbstoff der Formel
EMI0001.0009
wird zwecks Sulfonierung in der fünffachen Menge 32 % igen Oleums mehrere Stunden er hitzt, bis eine Probe in verdünnter Natrium acetatlösung klar löslich ist. Die Aufarbei tung erfolgt in üblicher Weise durch Aus giessen auf Eis, Filtrieren und Überführung in das Natronsalz. Der erhaltene Farbstoff enthält zwei Sulfogruppen im Molekül.
Er löst sich in konzentrierter Schwefelsäure mit grüner, in Wasser mit blauer Farbe und färbt Wolle in blauen Tönen von guten Echtheits eigenschaften.
Additional patent to main patent No. 189649. Process for the production of an acidic wool dye. The present patent relates to a process for the preparation of an acidic wool dye, which is characterized in that the dye of the formula:
EMI0001.0004
treated with a sulfonating agent. The new dye, which contains two sulfo groups in the molecule, dissolves in concentrated sulfuric acid with a green color and in water with a blue color and dyes wool in blue shades with good fastness properties.
Example: The dye of the formula
EMI0001.0009
is for the purpose of sulfonation in five times the amount of 32% oleum for several hours he heated until a sample in dilute sodium acetate solution is clearly soluble. The processing is carried out in the customary manner by pouring out onto ice, filtering and converting into the sodium salt. The dye obtained contains two sulfo groups in the molecule.
It dissolves in concentrated sulfuric acid with green color, in water with blue color and dyes wool in blue shades with good fastness properties.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH189649T | 1936-04-11 | ||
| CH193263T | 1936-04-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH193263A true CH193263A (en) | 1937-09-30 |
Family
ID=25721843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH193263D CH193263A (en) | 1936-04-11 | 1936-04-11 | Process for the production of an acidic wool dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH193263A (en) |
-
1936
- 1936-04-11 CH CH193263D patent/CH193263A/en unknown
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