CH196615A - Process for the production of a condensation product. - Google Patents
Process for the production of a condensation product.Info
- Publication number
- CH196615A CH196615A CH196615DA CH196615A CH 196615 A CH196615 A CH 196615A CH 196615D A CH196615D A CH 196615DA CH 196615 A CH196615 A CH 196615A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- condensation product
- pyridine
- water
- stearoylmethylamide
- Prior art date
Links
- 239000007859 condensation product Substances 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 6
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- WIVHXBTXQHIXTJ-UHFFFAOYSA-N 1-aminononadecan-2-one Chemical compound CCCCCCCCCCCCCCCCCC(=O)CN WIVHXBTXQHIXTJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000005711 Benzoic acid Substances 0.000 claims description 3
- 235000010233 benzoic acid Nutrition 0.000 claims description 3
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 3
- 238000005187 foaming Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000047 product Substances 0.000 claims description 2
- 239000004753 textile Substances 0.000 claims description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- XVMSFILGAMDHEY-UHFFFAOYSA-N 6-(4-aminophenyl)sulfonylpyridin-3-amine Chemical compound C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=N1 XVMSFILGAMDHEY-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines Kondensationsproduktes. Es wurde gefunden, dass man ein neues Kondensationsprodukt erhält, wenn man auf Stearoylmethylamid ein Mol des 3-Sulfochlo- rids der Benzoesäure in Gegenwart von Py- ridin einwirken lässt. Das neue Produkt bildet ein weisses Pulver, das sich in Wasser unter Bildung stark schäumender Lösungen löst und als Hilfsstoff in der Textilindustrie verwen det werden kann.
<I>Beispiel:</I> 3 Teile Stearoylmethylamid werden mit 4.4 Teilen Benzoesäure-3-sulfochlorid in 30 Teilen Pyridin während 1 Stunde auf 80-90 erhitzt, wonach sich eine Probe in Wasser klar auflöst. Nach weitgehender Entfernung des Pyridins im Vakuum wird der helle, fiüs- sige Rückstand mit 400 Teilen Wasser auf genommen, mit verdünnter Sodalösung neu tralisiert und das Reaktionsprodukt mit Na triumchlorid ausgesalzen. Dasselbe wird ab gesaugt und getrocknet.
Process for the production of a condensation product. It has been found that a new condensation product is obtained if one mole of the 3-sulfochloride of benzoic acid is allowed to act on stearoylmethylamide in the presence of pyridine. The new product forms a white powder that dissolves in water to form strongly foaming solutions and can be used as an auxiliary in the textile industry.
<I> Example: </I> 3 parts of stearoylmethylamide are heated with 4.4 parts of benzoic acid 3-sulfochloride in 30 parts of pyridine to 80-90 for 1 hour, after which a sample dissolves clearly in water. After extensive removal of the pyridine in vacuo, the pale, liquid residue is taken up in 400 parts of water, neutralized with dilute soda solution and the reaction product is salted out with sodium chloride. The same is sucked off and dried.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH196615T | 1936-11-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH196615A true CH196615A (en) | 1938-03-31 |
Family
ID=4440463
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH196615D CH196615A (en) | 1936-11-11 | 1936-11-11 | Process for the production of a condensation product. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH196615A (en) |
-
1936
- 1936-11-11 CH CH196615D patent/CH196615A/en unknown
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