CH200525A - Process for the preparation of an acidic wool azo dye. - Google Patents

Process for the preparation of an acidic wool azo dye.

Info

Publication number
CH200525A
CH200525A CH200525DA CH200525A CH 200525 A CH200525 A CH 200525A CH 200525D A CH200525D A CH 200525DA CH 200525 A CH200525 A CH 200525A
Authority
CH
Switzerland
Prior art keywords
sep
wool
azo dye
preparation
acidic
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH200525A publication Critical patent/CH200525A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28—Amino naphthols
    • C09B29/30—Amino naphtholsulfonic acid
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/34—Monoazo dyes prepared by diazotising and coupling from other coupling components
    • C09B29/36—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
    • C09B29/3604—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
    • C09B29/3647—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms
    • C09B29/3652—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles
    • C09B29/366—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles containing hydroxy-1,2-diazoles, e.g. pyrazolone

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Paper (AREA)

Description

  

  Verfahren zur- Herstellung eines sauren     Wollazofarbstoffes.     
EMI0001.0002     
  
    Vorliegendes <SEP> Patent <SEP> bezieht <SEP> sich <SEP> auf <SEP> ein
<tb>  Verfahren <SEP> zur <SEP> Herstellung <SEP> eines <SEP> sauren
<tb>  Wollazofarbstoffes-,dadurch <SEP> gekennzeichnet,
<tb>  dass <SEP> man <SEP> diazotiertes <SEP> 1-(N-Acetyl-isopropyl  amino)-4-am#inobenzal <SEP> in <SEP> sodaalkalischem
<tb>  Medium <SEP> mit <SEP> 1-(2'-Chlor-5'-sulfophenyl)-6  methyl-5-pyrazolan <SEP> kuppelt.
<tb>  



  Der <SEP> so <SEP> erhaltene <SEP> Farbstoff <SEP> bildet <SEP> nach
<tb>  dem <SEP> Trocknen <SEP> ein <SEP> zitronengelbes <SEP> wasserIös  liahes <SEP> Pulver <SEP> und <SEP> färbt <SEP> Wolle <SEP> und <SEP> Seide <SEP> in
<tb>  wasch- <SEP> und <SEP> lichtechten, <SEP> lebhaften <SEP> .grünstichig  gelben <SEP> Tönen <SEP> von <SEP> sehr <SEP> gutem <SEP> Egalisi@erver  mögen.
<tb>  



  <I>Beispiel:</I>
<tb>  1,9,2 <SEP> Teile <SEP> 1-(N-Acetyl-:isopTopylamina)  4-aminoibenzol <SEP> werden <SEP> wie <SEP> üblich <SEP> diazotiert.
<tb>  Die <SEP> erhaltene <SEP> Diazolösung <SEP> kuppelt <SEP> man <SEP> in
<tb>  sodaalikalis,chem <SEP> Medium <SEP> mit <SEP> <B>26</B> <SEP> Teilen) <SEP> 1-(2'  Chlor- <SEP> 5'-sulfophenyl)-,3i-methyl--5 <SEP> -pyrazolon.            Nach        beendeter        Kupplung        wird        der        gebildete          Farbstoff        abgesohieden        und    .getrocknet.



  Process for the preparation of an acidic wool azo dye.
EMI0001.0002
  
    The present <SEP> patent <SEP>, <SEP> refers to <SEP>
<tb> Process <SEP> for the <SEP> production <SEP> of an <SEP> acidic
<tb> wool azo dye - characterized by <SEP>,
<tb> that <SEP> one <SEP> diazotized <SEP> 1- (N-acetyl-isopropyl amino) -4-am # inobenzal <SEP> in <SEP> soda-alkaline
<tb> Medium <SEP> with <SEP> 1- (2'-chloro-5'-sulfophenyl) -6 methyl-5-pyrazolane <SEP> couples.
<tb>



  The <SEP> thus <SEP> obtained <SEP> dye <SEP> reproduces <SEP>
<tb> <SEP> drying <SEP> a <SEP> lemon yellow <SEP> water-soluble <SEP> powder <SEP> and <SEP> colors <SEP> wool <SEP> and <SEP> silk <SEP> in
<tb> wash- <SEP> and <SEP> lightfast, <SEP> lively <SEP> .green-tinged yellow <SEP> tones <SEP> by <SEP> very <SEP> good <SEP> Egalisi @ er ability.
<tb>



  <I> Example: </I>
<tb> 1,9,2 <SEP> parts <SEP> 1- (N-Acetyl-: isopTopylamina) 4-aminoibenzol <SEP> are <SEP> diazotized <SEP> as usual <SEP>.
<tb> The <SEP> received <SEP> diazo solution <SEP> is coupled <SEP> to <SEP> in
<tb> sodaalikalis, chem <SEP> medium <SEP> with <SEP> <B> 26 </B> <SEP> parts) <SEP> 1- (2 'chloro- <SEP> 5'-sulfophenyl) -, 3i-methyl - 5 <SEP> -pyrazolone. After the coupling has ended, the dye formed is boiled off and dried.

 

Claims (1)

EMI0001.0012 PATENTANSPRUCH: <tb> Verfahren <SEP> zur <SEP> Herstellung <SEP> eins <SEP> sauren <tb> Wollazofarbstoffes, <SEP> dadurch <SEP> gekennzeichnet, <tb> dass, <SEP> man <SEP> diazotiertes <SEP> 1-(N-Aoetyl-i.s,opropyl amino@)-4-aminobenzo1 <SEP> in <SEP> sodaalkalischem <tb> Medium <SEP> mit <SEP> 1-(2'-Chlor-5'-sulfophenyl-3 methyl-5-pyrazolon <SEP> kuppelt. <tb> Der <SEP> so <SEP> erhaltene <SEP> Farbstoff <SEP> bildet <SEP> nach <tb> ,dem <SEP> Trocknen <SEP> ein <SEP> zitronengelbes <SEP> wasserlös liches <SEP> Pulver <SEP> und <SEP> färbt <SEP> Wolle <SEP> und <SEP> Seide <SEP> in <tb> wasch- <SEP> und <SEP> lichtechten, <SEP> lebhaften <SEP> grünstiehig gelben <SEP> Tönen, <SEP> von <SEP> sehr <SEP> gutem <SEP> Egalisierver mögen. EMI0001.0012 PATENT CLAIM: <tb> Method <SEP> for <SEP> production <SEP> one <SEP> acidic <tb> wool azo dye, <SEP> characterized by <SEP>, <tb> that, <SEP> one <SEP> diazotized <SEP> 1- (N-aoetyl-i.s, opropyl amino @) - 4-aminobenzo1 <SEP> in <SEP> soda-alkaline <tb> Medium <SEP> with <SEP> 1- (2'-chloro-5'-sulfophenyl-3 methyl-5-pyrazolone <SEP> couples. <tb> The <SEP> <SEP> obtained in this way <SEP> dye <SEP> reproduces <SEP> <tb>, <SEP> drying <SEP> a <SEP> lemon yellow <SEP> water-soluble <SEP> powder <SEP> and <SEP> colors <SEP> wool <SEP> and <SEP> silk <SEP> in <tb> wash <SEP> and <SEP> lightfast, <SEP> lively <SEP> greenish yellow <SEP> tones, <SEP> of <SEP> very <SEP> good <SEP> equalizing ability.
CH200525D 1935-10-02 1936-09-17 Process for the preparation of an acidic wool azo dye. CH200525A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE200525X 1935-10-02
CH195654T 1936-09-17

Publications (1)

Publication Number Publication Date
CH200525A true CH200525A (en) 1938-10-15

Family

ID=25722775

Family Applications (1)

Application Number Title Priority Date Filing Date
CH200525D CH200525A (en) 1935-10-02 1936-09-17 Process for the preparation of an acidic wool azo dye.

Country Status (1)

Country Link
CH (1) CH200525A (en)

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