CH200543A - Process for the production of a new dye preparation. - Google Patents
Process for the production of a new dye preparation.Info
- Publication number
- CH200543A CH200543A CH200543DA CH200543A CH 200543 A CH200543 A CH 200543A CH 200543D A CH200543D A CH 200543DA CH 200543 A CH200543 A CH 200543A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye preparation
- new
- production
- new dye
- preparation
- Prior art date
Links
- 238000002360 preparation method Methods 0.000 title claims description 8
- 238000000034 method Methods 0.000 title claims description 3
- 238000004519 manufacturing process Methods 0.000 title description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000004043 dyeing Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000004753 textile Substances 0.000 claims description 2
- -1 pyridine benzoic acid-sulfochloride Chemical compound 0.000 claims 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 239000005711 Benzoic acid Substances 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical class [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 1
- 150000004056 anthraquinones Chemical class 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/50—Amino-hydroxy-anthraquinones; Ethers and esters thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr. 196173. Verfahren zur Herstellung eines neuen Farbstoiipräparates. Es wurde gefunden, dass man ein neues, lösliches Farbstoffpräparat erhält, wenn man auf 1,5-p-Dianisoyl-diamino-4,
8-dioxyanthra- chinon in Gegenwart von Pyridiu Benzoe- säure-3-sulfochlorid einwirken lässt. Hier- durch werden die OH-Gruppen des Anthra- chinonderivates sulfobenzoyliert.
EMI0001.0015
entspricht, kann zum Färben oder Drucken von Textilien verwendet werden. <I>Beispiel:
</I> 53,8 Teile 1,5-p-Dianisoyl-diamino-4,8-di- oxyanthrachinon werden mit 500 Teilen Py- Das neue Farbstoffpräparat stellt ein braunes Pulver dar, das sich in Wasser mit braungelber Farbe unter Bildung einer Lö sung, aus welcher durch Alkalien der Aus gangsfarbstoff regeneriert wird, löst.
Das neue Farbstoffpräparat, das der Formel ridin verrührt. Dazu gibt man 66 Teile Benzoesäure-m-sulfochlorid, steigert die Tem peratur auf etwa 90 und hält bei 90 bis 95 , bis sich eine Probe in Wasser klar auflöst. Nach dem Abtreiben des Pyridins im Va kuum wird das Reaktionsprodukt durch Lö- sen in wenig Wasser und Fällen mit gesättig ter Kochsalzlösung in fester Form gewonnen.
<B> Additional patent </B> to main patent no. 196173. Process for the production of a new coloring agent preparation. It has been found that a new, soluble dye preparation is obtained if you click on 1,5-p-dianisoyl-diamino-4,
8-dioxyanthraquinone in the presence of Pyridiu benzoic acid 3-sulfochloride can act. As a result, the OH groups of the anthraquinone derivative are sulfobenzoylated.
EMI0001.0015
can be used for dyeing or printing textiles. <I> example:
</I> 53.8 parts of 1,5-p-dianisoyl-diamino-4,8-di-oxyanthraquinone with 500 parts of Py- The new dye preparation is a brown powder that turns brownish-yellow in water to form a Lö solution, from which the starting dye is regenerated by alkalis, dissolves.
The new dye preparation that mixes the formula ridin. 66 parts of benzoic acid-m-sulfochloride are added, the temperature is increased to about 90 and held at 90 to 95 until a sample dissolves clearly in water. After the pyridine has been driven off in a vacuum, the reaction product is obtained in solid form by dissolving it in a little water and precipitating it with saturated sodium chloride solution.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH196173T | 1935-10-01 | ||
| CH200543T | 1935-10-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH200543A true CH200543A (en) | 1938-10-15 |
Family
ID=25722827
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH200543D CH200543A (en) | 1935-10-01 | 1935-10-01 | Process for the production of a new dye preparation. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH200543A (en) |
-
1935
- 1935-10-01 CH CH200543D patent/CH200543A/en unknown
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