CH206366A - Process for the preparation of a nitrogen compound. - Google Patents
Process for the preparation of a nitrogen compound.Info
- Publication number
- CH206366A CH206366A CH206366DA CH206366A CH 206366 A CH206366 A CH 206366A CH 206366D A CH206366D A CH 206366DA CH 206366 A CH206366 A CH 206366A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- nitrogen compound
- phenylchloroacetonitrile
- lorylanilide
- chcl
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 229910017464 nitrogen compound Inorganic materials 0.000 title claims description 3
- 150000002830 nitrogen compounds Chemical class 0.000 title claims description 3
- FFDGPVCHZBVARC-UHFFFAOYSA-N N,N-dimethylglycine Chemical compound CN(C)CC(O)=O FFDGPVCHZBVARC-UHFFFAOYSA-N 0.000 claims description 6
- WZSOEUAQKKEHFE-UHFFFAOYSA-N 2-chloro-2-phenylacetonitrile Chemical compound N#CC(Cl)C1=CC=CC=C1 WZSOEUAQKKEHFE-UHFFFAOYSA-N 0.000 claims description 2
- 230000000844 anti-bacterial effect Effects 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 239000000645 desinfectant Substances 0.000 claims description 2
- 230000000855 fungicidal effect Effects 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- NNICRUQPODTGRU-UHFFFAOYSA-N mandelonitrile Chemical compound N#CC(O)C1=CC=CC=C1 NNICRUQPODTGRU-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung einer Stichstoffverbindnng. Gegenstand des vorliegenden Patentes ist ein Verfahren zur Darstellung einer .Stick stoffverbindung, dadurch gekennzeichnet, daB man Dimethylaminoessigsäurelorylanilid mit Phenylchloracetonitril der Formel C,H,-CHCl-CN umsetzt.
Dae Endprodukt, eine halbfeste Masse, besitzt gute fungieide und bacteri- cide Eigenschaften und kann als Desinfek tionsmittel verwendet werden.
<I>Beispiel:</I> 12 Teile Dimethylaminoessigsäureloryl- anilid werden in 50 Teilen Benzol gelöst und mit -6 Teilen Phenylchloraoetonitril, aus Mandelsäurenitril in bekannter Weise dar- gestellt, zugesetzt. Nach zirka 20 Stunden wird mit Petroläther gefällt, die Fällung mit dem gleichen Lösungsmittel gut ausgewaschen und die neue Verbindung im Vakuum ge trocknet. Sie ist in Wasser trüb löslich.
Method for the representation of a nitrogen compound. The subject of the present patent is a process for the preparation of a stick material compound, characterized in that dimethylaminoacetic acid lorylanilide is reacted with phenylchloroacetonitrile of the formula C, H, -CHCl-CN.
The end product, a semi-solid mass, has good fungicidal and bactericidal properties and can be used as a disinfectant.
<I> Example: </I> 12 parts of dimethylaminoacetic acid eylanilide are dissolved in 50 parts of benzene and -6 parts of phenylchloraoetonitrile, prepared from mandelonitrile in a known manner, are added. After about 20 hours, it is precipitated with petroleum ether, the precipitate is washed out well with the same solvent and the new compound is dried in vacuo. It is cloudyly soluble in water.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH723275X | 1937-12-27 | ||
| CH206366T | 1937-12-27 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH206366A true CH206366A (en) | 1939-07-31 |
Family
ID=25724293
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH206366D CH206366A (en) | 1937-12-27 | 1937-12-27 | Process for the preparation of a nitrogen compound. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH206366A (en) |
-
1937
- 1937-12-27 CH CH206366D patent/CH206366A/en unknown
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