CH206367A - Process for the preparation of a nitrogen compound. - Google Patents
Process for the preparation of a nitrogen compound.Info
- Publication number
- CH206367A CH206367A CH206367DA CH206367A CH 206367 A CH206367 A CH 206367A CH 206367D A CH206367D A CH 206367DA CH 206367 A CH206367 A CH 206367A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- nitrogen compound
- rhodanide
- dimethyldodecylamine
- chloroethylene
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims description 4
- 229910017464 nitrogen compound Inorganic materials 0.000 title claims description 3
- 150000002830 nitrogen compounds Chemical class 0.000 title claims description 3
- VFFDVELHRCMPLY-UHFFFAOYSA-N dimethyldodecyl amine Natural products CC(C)CCCCCCCCCCCN VFFDVELHRCMPLY-UHFFFAOYSA-N 0.000 claims description 3
- YWFWDNVOPHGWMX-UHFFFAOYSA-N n,n-dimethyldodecan-1-amine Chemical compound CCCCCCCCCCCCN(C)C YWFWDNVOPHGWMX-UHFFFAOYSA-N 0.000 claims description 3
- 230000000844 anti-bacterial effect Effects 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 239000000645 desinfectant Substances 0.000 claims description 2
- 230000000855 fungicidal effect Effects 0.000 claims description 2
- 238000009736 wetting Methods 0.000 claims description 2
- 239000000080 wetting agent Substances 0.000 claims description 2
- -1 chloroethylene rhodanide Chemical compound 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- PBLNBZIONSLZBU-UHFFFAOYSA-N 1-bromododecane Chemical compound CCCCCCCCCCCCBr PBLNBZIONSLZBU-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C331/00—Derivatives of thiocyanic acid or of isothiocyanic acid
- C07C331/02—Thiocyanates
- C07C331/12—Thiocyanates having sulfur atoms of thiocyanate groups bound to carbon atoms of hydrocarbon radicals substituted by nitrogen atoms, not being part of nitro or nitroso groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C331/00—Derivatives of thiocyanic acid or of isothiocyanic acid
- C07C331/02—Thiocyanates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung einer Stickstoffverbindung. Gegenstand des vorliegenden Patentes ist ein Verfahren zur Darstellung einer Stiek- e,toffverbindung, dadurch gekennzeichnet, dass man Dimethyldodecylamin mit a,ss-Chlor- äthylenrhodanid umsetzt. Das Endprodukt, eine klebrige, hellbraune Masse, hat ;gute netzende, fungicide und bactericide Eigen schaften und kann als Netzmittel und als Desinfektionsmittel verwendet werden.
<I>Beispiel:</I> 31,8 Teile Dimethyldode@cylamin - in bekannter Weise aus Dodecylbromid und Dimethylaminlösung bei 40 bis 60 dar- gestellt - werden in 80 Teilen Benzol mit 16,5 Teilen a,ss-Chloräthylenrhodanid 8 Stun- den bei<B>50'</B> gerührt.
Durch Zusatz von Petroläther erhält man eine harzige Fällung, welche durch Abgiessen und Erwärmen im Vakuum auf<B>50'</B> von den organischen Lö- sungs- bezw. Fällungsmitteln befreit wird. Der Rückstand ist eine klebrige, hellbraune Masse, die in Wasser klar löslich ist.
Process for the preparation of a nitrogen compound. The subject matter of the present patent is a process for the preparation of a substance compound, characterized in that dimethyldodecylamine is reacted with α, ß-chloroethylene rhodanide. The end product, a sticky, light brown mass, has good wetting, fungicidal and bactericidal properties and can be used as a wetting agent and as a disinfectant.
<I> Example: </I> 31.8 parts of dimethyldodecylamine - prepared in a known manner from dodecyl bromide and dimethylamine solution at 40 to 60 - are in 80 parts of benzene with 16.5 parts of α, ß-chloroethylene rhodanide for 8 hours stirred at <B> 50 '</B>.
By adding petroleum ether, a resinous precipitate is obtained, which by pouring and heating in vacuo to <B> 50 '</B> from the organic solution or. Precipitants is freed. The residue is a sticky, light brown mass that is clearly soluble in water.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH848003X | 1937-12-27 | ||
| CH723275X | 1937-12-27 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH206367A true CH206367A (en) | 1939-07-31 |
Family
ID=33030474
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH206367D CH206367A (en) | 1937-12-27 | 1937-12-27 | Process for the preparation of a nitrogen compound. |
Country Status (2)
| Country | Link |
|---|---|
| CH (1) | CH206367A (en) |
| FR (1) | FR848003A (en) |
-
1937
- 1937-12-27 CH CH206367D patent/CH206367A/en unknown
-
1938
- 1938-12-24 FR FR848003D patent/FR848003A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR848003A (en) | 1939-10-20 |
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