CH210974A - Process for the production of a new condensation product. - Google Patents

Process for the production of a new condensation product.

Info

Publication number
CH210974A
CH210974A CH210974DA CH210974A CH 210974 A CH210974 A CH 210974A CH 210974D A CH210974D A CH 210974DA CH 210974 A CH210974 A CH 210974A
Authority
CH
Switzerland
Prior art keywords
condensation product
production
new condensation
new
product
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH210974A publication Critical patent/CH210974A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines neuen Kondensationsproduktes.    Es     wurde    gefunden, dass man zu einem  neuen     Kondensationsprodukt        gelangt,    wenn  man     Stearinsäureamid    in Gegenwart einer  Säure mit dem Additionsprodukt von     Tiz-          methylamin    an     Methylolchloracetamid    um  setzt.  



  Die Umsetzung wird zweckmässig in     Ge-          genwart    eines Lösungsmittels, wie Alkohol,       Aceton,        Diogan,    Eisessig, vorgenommen. Als  Säure kann beispielsweise Salzsäure,     Schwe-          felsäure,    Essigsäure Anwendung finden.  



  Das neue Kondensationsprodukt, eine       weiche    Masse, deren wässerige     Lösungen     stark     kapillaraktiv        :sind,    kann als     Weich-          machungsmittel,    z. B. für Baumwolle und       'unstseide,    verwendet werden.         Beispiel:       5,6 Gewichtsteile     Stearinsäureamid    wer  den in 50     Volumteilen        Eisessig    gelöst.

   Nach  Zugabe von 5 Gewichtsteilen des Additions  produktes     aus        Methylolchloracetamid        und          Trimethylamin    wird die Lösung während  40 Stunden auf<B>90-100'</B> erhitzt. Nach dem  Abkühlen,     Filtrieren    und     Eindampfen        im       Vakuum wird eine weiche Masse erhalten,  deren wässerige Lösungen stark     kapillaraktiv     sind. Das neue Kondensationsprodukt kann  als     Weichmachungsmittel,    z. B. für Baum  wolle und     Kunstseide,    verwendet werden.



  Process for the production of a new condensation product. It has been found that a new condensation product is obtained if stearic acid amide is reacted in the presence of an acid with the addition product of tizmethylamine to methylolchloroacetamide.



  The reaction is expediently carried out in the presence of a solvent such as alcohol, acetone, Diogan, glacial acetic acid. Hydrochloric acid, sulfuric acid, acetic acid, for example, can be used as the acid.



  The new condensation product, a soft mass, the aqueous solutions of which are highly capillary-active, can be used as a plasticizer, e.g. B. for cotton and 'unstseilse be used. Example: 5.6 parts by weight of stearic acid amide who dissolved in 50 parts by volume of glacial acetic acid.

   After adding 5 parts by weight of the addition product of methylolchloracetamide and trimethylamine, the solution is heated to 90-100 'for 40 hours. After cooling, filtering and evaporation in vacuo, a soft mass is obtained, the aqueous solutions of which are highly capillary-active. The new condensation product can be used as a plasticizer, e.g. B. for cotton and rayon can be used.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Kondensationsproduktes, dadurch gekenn- zeichnet, dass man Stearinsäureamid in Ge genwart einer Säure mit dem Additions produkt von Trimethylamin an Methylol- ohloracetamid umsetzt. Das neue Kondensationsprodukt, eine weiche Masse, deren wässerige Lösungen stark kapil.laraktiv sind, kann als Weich- machungsmittels, z. B. für Baumwolle und Kunstseide, verwendet werden. PATENT CLAIM: Process for the production of a new condensation product, characterized in that stearic acid amide is reacted in the presence of an acid with the addition product of trimethylamine to methyloloroacetamide. The new condensation product, a soft mass, the aqueous solutions of which are strongly kapil.laraktiv, can be used as a plasticizer, e.g. B. for cotton and rayon can be used. UNTERANSPRUCH: Verfahren nach Patentanspruch, dadurch gekennzeichnet, dass man in Gegenwart eines Lösungsmittels arbeitet. SUBCLAIM: Process according to claim, characterized in that one works in the presence of a solvent.
CH210974D 1938-08-12 1938-08-12 Process for the production of a new condensation product. CH210974A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH210974T 1938-08-12
CH2279497X 1938-08-12

Publications (1)

Publication Number Publication Date
CH210974A true CH210974A (en) 1940-08-15

Family

ID=25724963

Family Applications (1)

Application Number Title Priority Date Filing Date
CH210974D CH210974A (en) 1938-08-12 1938-08-12 Process for the production of a new condensation product.

Country Status (1)

Country Link
CH (1) CH210974A (en)

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