CH235705A - Process for the production of a sulfur dye. - Google Patents
Process for the production of a sulfur dye.Info
- Publication number
- CH235705A CH235705A CH235705DA CH235705A CH 235705 A CH235705 A CH 235705A CH 235705D A CH235705D A CH 235705DA CH 235705 A CH235705 A CH 235705A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- sulfur
- dye
- sulfur dye
- way
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 239000000988 sulfur dye Substances 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 3
- 239000011593 sulfur Substances 0.000 claims description 3
- 229910052717 sulfur Inorganic materials 0.000 claims description 3
- 240000007817 Olea europaea Species 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000000835 fiber Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 235000013311 vegetables Nutrition 0.000 claims description 2
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 2
- NGDNCZPCIZNCQS-UHFFFAOYSA-N ctk3j8699 Chemical compound Cl=S NGDNCZPCIZNCQS-UHFFFAOYSA-N 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B49/00—Sulfur dyes
- C09B49/04—Sulfur dyes from amino compounds of the benzene, naphthalene or anthracene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. 231495. Verfahren zur Herstellung eines Schwefelfarbstoffes. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines Schwefel farbstoffes, dadurch gekennzeichnet, dass man 1.5 - Di - p - toluido - anthrächinon mit einem schwefelnden Mittel behandelt und die dabei erhaltene Rohschmelze unter Verwendung von Schwefelalkali aufschliesst.
Der so erhaltene Farbstoff ist ein dunkles Pulver und färbt die pflanzliche Faser in echten braunstickig oliven Tönen, insbeson dere von einer sehr guten Lichtechtheit.
<I>Beispiel:</I> Zu einer Schmelze von 12 Teilen Schwe fel in 150 Teilen Chlorschwefel werden all mählich 40 Teile 1.5 - Di - p - toluidö - anthra- chinon bei 70 bis 80 eingetragen. Man heizt langsam auf 150 , kocht 1 Stunde unter Rüekfluss und destilliert dann bis zur Trockne. Dann wird die Temperatur auf 270 erhöht und 8 Stunden bei dieser Tem peratur gehalten. Durch Nachbehandlung mit Schwefelnatrium und Lauge wird der Farb stoff in üblicher Weise aufgeschlossen.
Additional patent to main patent no. 231495. Process for the production of a sulfur dye. The present patent relates to a process for the production of a sulfur dye, characterized in that 1,5 - di - p - toluido - anthraquinone is treated with a sulphurizing agent and the resulting crude melt is broken down using alkali sulfur.
The dye obtained in this way is a dark powder and dyes the vegetable fiber in real brownish olive tones, in particular very good lightfastness.
<I> Example: </I> To a melt of 12 parts of sulfur in 150 parts of chlorosulphur, 40 parts of 1.5 - di - p - toluidö - anthraquinone at 70 to 80 are gradually added. The mixture is slowly heated to 150, refluxed for 1 hour and then distilled to dryness. Then the temperature is increased to 270 and kept at this temperature for 8 hours. After treatment with sodium sulphide and lye, the dye is broken down in the usual way.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE235705X | 1941-12-18 | ||
| CH231495T | 1944-03-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH235705A true CH235705A (en) | 1944-12-15 |
Family
ID=25727597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH235705D CH235705A (en) | 1941-12-18 | 1942-12-21 | Process for the production of a sulfur dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH235705A (en) |
-
1942
- 1942-12-21 CH CH235705D patent/CH235705A/en unknown
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