CH297272A - Process for the preparation of a diammonium compound. - Google Patents

Process for the preparation of a diammonium compound.

Info

Publication number
CH297272A
CH297272A CH297272DA CH297272A CH 297272 A CH297272 A CH 297272A CH 297272D A CH297272D A CH 297272DA CH 297272 A CH297272 A CH 297272A
Authority
CH
Switzerland
Prior art keywords
preparation
diammonium compound
bis
diammonium
compound
Prior art date
Application number
Other languages
German (de)
Inventor
Ag J R Geigy
Original Assignee
Ag J R Geigy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ag J R Geigy filed Critical Ag J R Geigy
Publication of CH297272A publication Critical patent/CH297272A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung einer     Diammoniumverbindung.       Gegenstand vorliegenden Patentes ist ein  Verfahren zur     Herstellung    einer     Diammonium-          verbindung.    Das Verfahren ist dadurch ge  kennzeichnet, dass man auf     1.        Mol        1,10-Bis-          (ss-diä.t.liylamino-äthylmereapto)-delzan    2     Mol          :ltliyljodid    einwirken lässt.  



  Die erhaltene neue Verbindung, das     1,10-          Bis        -[ss        -(triäthylammonium)    -     äthylmercapt.o]-          dekan-dijodid,    schmilzt bei 130-132 . Sie soll  therapeutische Verwendung finden.  



       Beispiel:     8,09 Teile     1,10-Bis-(ss-diäthylamino-ätliyi-          inercapto)-dekan    in 70     Volumteilen    trockenem       Aeeton    werden mit 3,4     Volumteilen    Äthyl-         jodid    14 Stunden auf 50-60  erwärmt. Nach  Erkalten wird das Produkt     abgesaugt    und       gewünschtenfalls    aus     Aeeton    unter Zusatz  von wenig     abs.    Methanol umkristallisiert. Es  zeigt. einen Schmelzpunkt von     130-132 .  



  Process for the preparation of a diammonium compound. The present patent relates to a process for the production of a diammonium compound. The process is characterized in that 1,10-bis- (ss-diä.t.liylamino-äthylmereapto) -delzan is allowed to act on 1 mole: ethyl iodide.



  The new compound obtained, the 1,10-bis - [ss - (triäthylammonium) - äthylmercapt.o] - decane diiodide, melts at 130-132. It should find therapeutic use.



       Example: 8.09 parts of 1,10-bis- (ss-diethylamino-ätliyi- inercapto) -dekan in 70 parts by volume of dry acetone are heated with 3.4 parts by volume of ethyl iodide to 50-60 hours for 14 hours. After cooling, the product is filtered off with suction and, if desired, from acetone with the addition of a little abs. Recrystallized methanol. It shows. a melting point of 130-132.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung einer Diammo- niumverbindung, dadurch gekennzeichnet, dass man auf 1 Mol 1,10-Bis-(ss-diä.thylamino-äthyl- mercapto)-dekan 2 Mol Äthyljoclid einwirken lässt. Die erhaltene neue Verbindung, das 1,10- Bis -[ss -(triäthylammonium) - äthylmercapto]- dekan-dijodid, schmilzt bei 130-132 . Claim: Process for the production of a diammonium compound, characterized in that 1 mole of 1,10-bis- (ss-diä.thylamino-äthyl- mercapto) decane is allowed to act with 2 moles of ethyljoclide. The new compound obtained, the 1,10-bis - [ss - (triethylammonium) - äthylmercapto] - decane diiodide, melts at 130-132.
CH297272D 1950-12-12 1950-12-12 Process for the preparation of a diammonium compound. CH297272A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH297272T 1950-12-12
CH293565T 1950-12-12

Publications (1)

Publication Number Publication Date
CH297272A true CH297272A (en) 1954-03-15

Family

ID=25733370

Family Applications (1)

Application Number Title Priority Date Filing Date
CH297272D CH297272A (en) 1950-12-12 1950-12-12 Process for the preparation of a diammonium compound.

Country Status (1)

Country Link
CH (1) CH297272A (en)

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