CH367917A - Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form - Google Patents

Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form

Info

Publication number: CH367917A
Authority: CH; Switzerland
Prior art keywords: pigment; water; organic solvent; production; solvent
Prior art date: 1958-08-07

Application number

CH6266758A

Other languages

German (de)

English (en)

Inventor

Hans Dr Gaertner

Christoph Dr Frey

Rudolf Dr Mory

Original Assignee

Ciba Geigy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1958-08-07

Filing date

1958-08-07

Publication date

1963-03-15

1958-08-07 Application filed by Ciba Geigy filed Critical Ciba Geigy

1958-08-07 Priority to CH6266758A priority Critical patent/CH367917A/de

1959-08-06 Priority to ES0251312A priority patent/ES251312A1/es

1963-03-15 Publication of CH367917A publication Critical patent/CH367917A/de

Links

239000000049 pigment Substances 0.000 title claims description 25
238000000034 method Methods 0.000 title claims description 17
PPSZHCXTGRHULJ-UHFFFAOYSA-N dioxazine Chemical compound O1ON=CC=C1 PPSZHCXTGRHULJ-UHFFFAOYSA-N 0.000 title claims description 4
238000004519 manufacturing process Methods 0.000 title claims description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 11
239000003960 organic solvent Substances 0.000 claims description 10
239000002904 solvent Substances 0.000 claims description 8
239000000975 dye Substances 0.000 claims description 7
239000002270 dispersing agent Substances 0.000 claims description 5
238000000227 grinding Methods 0.000 claims description 5
239000002245 particle Substances 0.000 claims description 2
DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims 1
230000001419 dependent effect Effects 0.000 claims 1
-1 aliphatic alcohols Chemical class 0.000 description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
238000009826 distribution Methods 0.000 description 3
238000001035 drying Methods 0.000 description 3
239000000758 substrate Substances 0.000 description 3
YZVWKHVRBDQPMQ-UHFFFAOYSA-N 1-aminopyrene Chemical compound C1=C2C(N)=CC=C(C=C3)C2=C2C3=CC=CC2=C1 YZVWKHVRBDQPMQ-UHFFFAOYSA-N 0.000 description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 description 2
NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
239000002253 acid Substances 0.000 description 2
238000005054 agglomeration Methods 0.000 description 2
230000002776 aggregation Effects 0.000 description 2
239000006185 dispersion Substances 0.000 description 2
150000002170 ethers Chemical class 0.000 description 2
BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
238000003801 milling Methods 0.000 description 2
239000000843 powder Substances 0.000 description 2
RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
BCHZICNRHXRCHY-UHFFFAOYSA-N 2h-oxazine Chemical compound N1OC=CC=C1 BCHZICNRHXRCHY-UHFFFAOYSA-N 0.000 description 1
OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
OXEUETBFKVCRNP-UHFFFAOYSA-N 9-ethyl-3-carbazolamine Chemical compound NC1=CC=C2N(CC)C3=CC=CC=C3C2=C1 OXEUETBFKVCRNP-UHFFFAOYSA-N 0.000 description 1
RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 description 1
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 1
239000005662 Paraffin oil Substances 0.000 description 1
239000002202 Polyethylene glycol Substances 0.000 description 1
KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
150000001408 amides Chemical class 0.000 description 1
239000012736 aqueous medium Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
239000007859 condensation product Substances 0.000 description 1
235000014113 dietary fatty acids Nutrition 0.000 description 1
HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 1
150000005125 dioxazines Chemical class 0.000 description 1
MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical class CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 description 1
229940043264 dodecyl sulfate Drugs 0.000 description 1
238000010410 dusting Methods 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
229930195729 fatty acid Natural products 0.000 description 1
239000000194 fatty acid Substances 0.000 description 1
150000004665 fatty acids Chemical class 0.000 description 1
238000011010 flushing procedure Methods 0.000 description 1
235000019253 formic acid Nutrition 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000002609 medium Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000000203 mixture Substances 0.000 description 1
125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical class C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 1
125000005608 naphthenic acid group Chemical group 0.000 description 1
229920001223 polyethylene glycol Polymers 0.000 description 1
229920000915 polyvinyl chloride Polymers 0.000 description 1
239000004800 polyvinyl chloride Substances 0.000 description 1
230000001376 precipitating effect Effects 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000000344 soap Substances 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
239000007787 solid Substances 0.000 description 1
238000001694 spray drying Methods 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
UGNWTBMOAKPKBL-UHFFFAOYSA-N tetrachloro-1,4-benzoquinone Chemical compound ClC1=C(Cl)C(=O)C(Cl)=C(Cl)C1=O UGNWTBMOAKPKBL-UHFFFAOYSA-N 0.000 description 1
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1
238000010626 work up procedure Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B19/00—Oxazine dyes
- C09B19/02—Bisoxazines prepared from aminoquinones

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Pigments, Carbon Blacks, Or Wood Stains (AREA)
Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)

CH6266758A 1958-08-07 1958-08-07 Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form CH367917A (de)

Priority Applications (2)

Application Number	Priority Date	Filing Date	Title
CH6266758A CH367917A (de)	1958-08-07	1958-08-07	Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form
ES0251312A ES251312A1 (es)	1958-08-07	1959-08-06	Procedimiento para la preparaciën de pigmentos de dioxazina en forma finamente dispersada

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CH6266758A CH367917A (de)	1958-08-07	1958-08-07	Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form

Publications (1)

Publication Number	Publication Date
CH367917A true CH367917A (de)	1963-03-15

Family

ID=4524439

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH6266758A CH367917A (de)	1958-08-07	1958-08-07	Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form

Country Status (2)

Country	Link
CH (1)	CH367917A (es)
ES (1)	ES251312A1 (es)

1958
- 1958-08-07 CH CH6266758A patent/CH367917A/de unknown
1959
- 1959-08-06 ES ES0251312A patent/ES251312A1/es not_active Expired

Also Published As

Publication number	Publication date
ES251312A1 (es)	1960-02-16

Publication	Publication Date	Title
DE1181160B (de)	1964-11-12	Verfahren zur Herstellung feindisperser Farbstoffe oder Pigmente
CH629242A5 (de)	1982-04-15	Verfahren zur herstellung eines beta-phthalocyaninpigments.
DE2729892A1 (de)	1978-01-12	Festes pigmentpraeparat fuer druck- und lackierfarbensysteme
DE2160208C3 (de)	1979-09-13	Pigmentformierung
EP0176059A2 (de)	1986-04-02	Verfahren zur Herstellung von anwendungstechnisch verbesserten Verlackungsprodukten
DE1469724B2 (de)	1973-04-12	Verfahren zur herstellung von in organischen medien leicht dispergierbaren pigmentzubereitungen
DE2914299B2 (de)	1981-04-30	Pigmentpräparate, Verfahren zu ihrer Herstellung und ihre Verwendung
EP0033913B1 (de)	1985-03-20	Verfahren zur Herstellung von Pigmentpräparationen und ihre Verwendung
EP0028342B1 (de)	1983-10-12	Verwendung von veresterten Oxalkylaten als Präparationsmittel für Farbstoffe und entsprechende Farbstoffzubereitungen
CH522716A (de)	1972-06-30	Verfahren zur Herstellung einer Masse zur Pigmentierung eines organischen Mediums
CH367917A (de)	1963-03-15	Verfahren zur Herstellung von Dioxazin-Pigmenten in fein verteilter Form
EP0118394B1 (de)	1987-04-15	Dispersfarbstoffpräparate
DE2827264A1 (de)	1979-01-04	Pigmentzusammensetzungen
EP0180870B1 (de)	1990-03-07	Verfahren zur Herstellung hochkonzentrierter wässriger Presskuchen von Feststoffen
DE2646211A1 (de)	1977-04-21	Verfahren zum zerkleinern
DE3212408A1 (de)	1983-10-13	Feste farbstoffpraeparate von anionischen farbstoffen
DE60115213T2 (de)	2006-08-03	Verfahren zur herstellung kupferphthalocyaninpigment in der beta-phase
DE3045679C2 (es)	1988-12-08
DE4134079C2 (de)	1998-09-17	Pigmentpräparation, Verfahren zu ihrer Herstellung und ihre Verwendung
US2282527A (en)	1942-05-12	Pigment transfer
CH350058A (de)	1960-11-15	Verfahren zur Herstellung von weichkörnigen Küpenfarbstoff-Pigmenten
US3119706A (en)	1964-01-28	Process for conditioning pigments
DE3440487A1 (de)	1986-05-07	Verfahren zur herstellung hochkonzentrierter waessriger presskuchen von azodispersionsfarbstoffen
CH640559A5 (de)	1984-01-13	Verfahren zur herstellung von in wasser dispergierbaren pulverfoermigen zubereitungen von dispersionsfarbstoffen.
US2114713A (en)	1938-04-19	Process of dispersing pigments and products thereof