CH393311A - Verfahren zur Herstellung von gereinigtes Pyrethrin enthaltenden Zusammensetzungen - Google Patents

Verfahren zur Herstellung von gereinigtes Pyrethrin enthaltenden Zusammensetzungen

Info

Publication number: CH393311A
Authority: CH; Switzerland
Prior art keywords: pyrethrin; parts; pyrethrins; hydrocarbons; cinerin
Prior art date: 1959-03-06

Application number

CH247860A

Other languages

German (de)

English (en)

Inventor

August Goldberg Alan

John Smith Harold

Original Assignee

Kenya Pyrethrum Board

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1959-03-06

Filing date

1960-03-04

Publication date

1965-06-15

1960-03-04 Application filed by Kenya Pyrethrum Board filed Critical Kenya Pyrethrum Board

1965-06-15 Publication of CH393311A publication Critical patent/CH393311A/de

Links

VQXSOUPNOZTNAI-UHFFFAOYSA-N Pyrethrin I Natural products CC(=CC1CC1C(=O)OC2CC(=O)C(=C2C)CC=C/C=C)C VQXSOUPNOZTNAI-UHFFFAOYSA-N 0.000 title claims description 58
VJFUPGQZSXIULQ-XIGJTORUSA-N pyrethrin II Chemical compound CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VJFUPGQZSXIULQ-XIGJTORUSA-N 0.000 title claims description 53
HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 title claims description 51
239000000203 mixture Substances 0.000 title claims description 16
238000000034 method Methods 0.000 title claims description 11
229930195733 hydrocarbon Natural products 0.000 claims description 34
150000002430 hydrocarbons Chemical class 0.000 claims description 34
ROVGZAWFACYCSP-VUMXUWRFSA-N pyrethrin I Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-VUMXUWRFSA-N 0.000 claims description 33
VMORCWYWLVLMDG-YZGWKJHDSA-N Pyrethrin-II Natural products CC(=O)OC(=C[C@@H]1[C@H](C(=O)O[C@H]2CC(=O)C(=C2C)CC=CC=C)C1(C)C)C VMORCWYWLVLMDG-YZGWKJHDSA-N 0.000 claims description 29
239000007788 liquid Substances 0.000 claims description 28
239000000284 extract Substances 0.000 claims description 27
VXSIXFKKSNGRRO-MXOVTSAMSA-N [(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate;[(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-3-[(e)-3-methoxy-2-methyl-3-oxoprop-1-enyl Chemical class CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1.CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VXSIXFKKSNGRRO-MXOVTSAMSA-N 0.000 claims description 26
229940070846 pyrethrins Drugs 0.000 claims description 26
239000002728 pyrethroid Substances 0.000 claims description 26
240000004460 Tanacetum coccineum Species 0.000 claims description 19
ROVGZAWFACYCSP-MQBLHHJJSA-N [2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-MQBLHHJJSA-N 0.000 claims description 19
229940015367 pyrethrum Drugs 0.000 claims description 19
229930193529 cinerin Natural products 0.000 claims description 16
FMTFEIJHMMQUJI-UHFFFAOYSA-N Cinerin I Natural products C1C(=O)C(CC=CC)=C(C)C1OC(=O)C1C(C)(C)C1C=C(C)C FMTFEIJHMMQUJI-UHFFFAOYSA-N 0.000 claims description 14
FMTFEIJHMMQUJI-DFKXKMKHSA-N cinerin I Chemical compound C1C(=O)C(C\C=C/C)=C(C)[C@H]1OC(=O)[C@H]1C(C)(C)[C@@H]1C=C(C)C FMTFEIJHMMQUJI-DFKXKMKHSA-N 0.000 claims description 14
FMTFEIJHMMQUJI-NJAFHUGGSA-N 102130-98-3 Natural products CC=CCC1=C(C)[C@H](CC1=O)OC(=O)[C@@H]1[C@@H](C=C(C)C)C1(C)C FMTFEIJHMMQUJI-NJAFHUGGSA-N 0.000 claims description 13
239000011347 resin Substances 0.000 claims description 11
229920005989 resin Polymers 0.000 claims description 11
LTNDZDRYUXNFCU-NEWSRXKRSA-N Cinerin II Natural products CC=CCC1=C(C)[C@H](CC1=O)OC(=O)[C@@H]2[C@@H](C=C(C)OC(=O)C)C2(C)C LTNDZDRYUXNFCU-NEWSRXKRSA-N 0.000 claims description 10
SHCRDCOTRILILT-WOBDGSLYSA-N cinerin II Chemical compound CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C)C(=O)C1 SHCRDCOTRILILT-WOBDGSLYSA-N 0.000 claims description 10
239000008601 oleoresin Substances 0.000 claims description 9
238000004519 manufacturing process Methods 0.000 claims description 5
239000004215 Carbon black (E152) Substances 0.000 claims description 3
229930195735 unsaturated hydrocarbon Natural products 0.000 claims description 3
230000015556 catabolic process Effects 0.000 claims description 2
238000006731 degradation reaction Methods 0.000 claims description 2
238000005979 thermal decomposition reaction Methods 0.000 claims description 2
230000001419 dependent effect Effects 0.000 claims 1
239000003209 petroleum derivative Substances 0.000 claims 1
238000004821 distillation Methods 0.000 description 35
239000003921 oil Substances 0.000 description 25
239000012188 paraffin wax Substances 0.000 description 16
238000009835 boiling Methods 0.000 description 9
239000000126 substance Substances 0.000 description 9
229940057995 liquid paraffin Drugs 0.000 description 7
239000003208 petroleum Substances 0.000 description 7
241000196324 Embryophyta Species 0.000 description 6
238000000926 separation method Methods 0.000 description 5
239000000463 material Substances 0.000 description 4
241000238631 Hexapoda Species 0.000 description 3
239000004480 active ingredient Substances 0.000 description 3
238000001704 evaporation Methods 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
238000000354 decomposition reaction Methods 0.000 description 2
229940079593 drug Drugs 0.000 description 2
239000003814 drug Substances 0.000 description 2
238000006116 polymerization reaction Methods 0.000 description 2
239000007858 starting material Substances 0.000 description 2
BZKFMUIJRXWWQK-UHFFFAOYSA-N Cyclopentenone Chemical group O=C1CCC=C1 BZKFMUIJRXWWQK-UHFFFAOYSA-N 0.000 description 1
235000019728 animal nutrition Nutrition 0.000 description 1
150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
125000004369 butenyl group Chemical group C(=CCC)* 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
238000004140 cleaning Methods 0.000 description 1
239000006103 coloring component Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
239000000287 crude extract Substances 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000004459 forage Substances 0.000 description 1
238000005194 fractionation Methods 0.000 description 1
235000011389 fruit/vegetable juice Nutrition 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
230000000749 insecticidal effect Effects 0.000 description 1
238000006317 isomerization reaction Methods 0.000 description 1
239000003350 kerosene Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000002480 mineral oil Substances 0.000 description 1
235000010446 mineral oil Nutrition 0.000 description 1
230000003472 neutralizing effect Effects 0.000 description 1
235000019645 odor Nutrition 0.000 description 1
230000009965 odorless effect Effects 0.000 description 1
-1 pentadienyl chain Chemical group 0.000 description 1
229940048383 pyrethrum extract Drugs 0.000 description 1
230000006340 racemization Effects 0.000 description 1
238000007670 refining Methods 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
238000000526 short-path distillation Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000002904 solvent Substances 0.000 description 1
239000007921 spray Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1

Classifications

- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/16—Ericaceae [Heath or Blueberry family], e.g. rhododendron, arbutus, pieris, cranberry or bilberry
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof

Landscapes

Life Sciences & Earth Sciences (AREA)
Health & Medical Sciences (AREA)
General Health & Medical Sciences (AREA)
Engineering & Computer Science (AREA)
Wood Science & Technology (AREA)
Natural Medicines & Medicinal Plants (AREA)
Dentistry (AREA)
Plant Pathology (AREA)
Agronomy & Crop Science (AREA)
Zoology (AREA)
Environmental Sciences (AREA)
Pest Control & Pesticides (AREA)
Biotechnology (AREA)
Microbiology (AREA)
Mycology (AREA)
Agricultural Chemicals And Associated Chemicals (AREA)
Compositions Of Macromolecular Compounds (AREA)
Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Medicines Containing Plant Substances (AREA)

CH247860A 1959-03-06 1960-03-04 Verfahren zur Herstellung von gereinigtes Pyrethrin enthaltenden Zusammensetzungen CH393311A (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GB7817/59A GB927892A (en)	1959-03-06	1959-03-06	Production of purified pyrethrum extract

Publications (1)

Publication Number	Publication Date
CH393311A true CH393311A (de)	1965-06-15

Family

ID=9840335

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH247860A CH393311A (de)	1959-03-06	1960-03-04	Verfahren zur Herstellung von gereinigtes Pyrethrin enthaltenden Zusammensetzungen

Country Status (3)

Country	Link
BE (1)	BE588295A (fr)
CH (1)	CH393311A (fr)
GB (1)	GB927892A (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5679662A (en) *	1995-06-06	1997-10-21	Thermo Trilogy Corporation	Synergistic use of azadirachtin and pyrethrum

1959
- 1959-03-06 GB GB7817/59A patent/GB927892A/en not_active Expired
1960
- 1960-03-04 CH CH247860A patent/CH393311A/de unknown
- 1960-03-04 BE BE588295A patent/BE588295A/fr unknown

Also Published As

Publication number	Publication date
GB927892A (en)	1963-06-06
BE588295A (fr)	1960-09-05

Publication	Publication Date	Title
DE60021279T2 (de)	2006-05-18	Reinigung von wässrigen lösungen von organischen säuren
DE4202657C2 (de)	1995-10-12	Pharmazeutisch wirksame Zusammensetzung aus Tanacetum parthenium sowie Verfahren zu deren Extraktion und mit der pharmazeutisch wirksamen Zusammensetzung hergestelltes Arzneimittel
DE69229480T2 (de)	2000-02-17	Verfahren zur herstellung hochreiner eicosapentaensäure oder ester davon
DE69614116T2 (de)	2002-03-14	Raffinieren von essbaren Ölen mit hohem natürlichem Carotin- und Vitamin-E-Gehalt
DE69533793T2 (de)	2005-12-22	Lösungsmittel-extraktionsverfahren
DE2363418C3 (de)	1985-08-01	Verfahren zur Extraktion und Isolierung von Fetten und Ölen pflanzlichen und tierischen Ursprungs im kritischen Druckbereich
DE2552311C3 (de)	1981-09-17	Verfahren zur Herstellung von Öl- und Fettfraktionen durch Umestern
EP0132570B1 (fr)	1986-12-03	Procédé de distillation de préservante d'acides gras
DE20221392U1 (de)	2005-12-15	Carnaubawachsoxidate
DE69304268T2 (de)	1997-03-06	Verfahren zur Entwässerung von Lösungsmitteln von ein Kohlenwasserstoff Entwachsungsverfahren
CH393311A (de)	1965-06-15	Verfahren zur Herstellung von gereinigtes Pyrethrin enthaltenden Zusammensetzungen
DE3112380C2 (de)	1985-04-11	Lagerstabiles Zitrusfruchtaroma-Konzentrat
DE602004008275T2 (de)	2008-05-08	Gaswaschverfahren und -vorrichtung
DE841505C (de)	1952-06-16	Verfahren zur Polymerisation eines ungesaettigten Alkohols, der ein ungesaettigtes Kohlenstoffatom direkt an die Carbinol-gruppe gebunden aufweist
DE1266748C2 (de)	1973-07-19	Verfahren zur Verhinderung der Verkrustung von Heizflaechen bei der kontinuierlichen Destillation von Phthalsaeureanhydrid
DE903852C (de)	1954-02-11	Verfahren zur kontinuierlichen Gewinnung reiner Harzsaeuren und reiner Fettsaeuren aus Talloel
DE3316523C2 (de)	1986-02-06	Verfahren und Vorrichtung zur Desodorierung und Entsäuerung von Fetten und Ölen
DE1519575B2 (de)	1976-02-05	Verfahren zur gleichzeitigen behandlung von wenigstens zwei verschiedenen rohoelen
DE19531806C1 (de)	1997-04-10	Verfahren zur schonenden Destillation von Fettsäuren
DE117626C (fr)
DE1468860A1 (de)	1969-06-26	Verfahren zur Entfernung wertvoller Produkte aus Mischungen,die aus der Reaktion zwischen Adipinsaeure und Ammoniak stammen
DE744284C (de)	1952-08-21	Verfahren zur Gewinnung von Phenolen aus OElen
DE552586C (de)	1932-06-15	Verfahren zur Gewinnung hochprozentiger oder reiner fester Kohlenwasserstoffe aus Teeren
DE665076C (de)	1938-09-16	Verfahren zur Gewinnung von Rotenon und ihm verwandten Insekticiden
DE566915C (de)	1933-01-02	Verfahren zur Gewinnung von Fettsaeuren aus den Oxydationsprodukten von Kohlenwasserstoffen